ASTM E285-1980(2002) Standard Test Method for Oxyacetylene Ablation Testing of Thermal Insulation Materials《热绝缘材料的氧乙炔烧蚀试验方法》.pdf

1、Designation: E 285 80 (Reapproved 2002)Standard Test Method forOxyacetylene Ablation Testing of Thermal InsulationMaterials1This standard is issued under the fixed designation E 285; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision,

2、the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 This test method covers the screening of ablative mate-rials to determine the relative thermal insulation

3、 effectivenesswhen tested as a flat panel in an environment of a steady flowof hot gas provided by an oxyacetylene burner.1.2 This test method should be used to measure and describethe properties of materials, products, or assemblies in responseto heat and flame under controlled laboratory condition

4、s andshould not be used to describe or appraise the fire hazard ofmaterials, products, or assemblies under actual fire conditions.However, results of this test method may be used as elementsof a fire risk assessment which takes into account all of thefactors which are pertinent to an assessment of t

5、he fire hazardof a particular end use.1.3 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory li

6、mitations prior to use.1.4 The values stated in SI units are to be regarded as thestandard.2. Referenced Documents2.1 ASTM Standards:D 792 Test Methods for Density and Specific Gravity (Rela-tive Density) of Plastics by Displacement22.2 Federal Standards:3BB-A-106a Acetylene, Technical, DissolvedBB-

7、O-925a Oxygen, Technical, Gas and Liquid3. Summary of Test Method3.1 Hot combustion gases are directed along the normal tothe specimen until burn-through is achieved. The erosion rateof the material is determined by dividing the original thicknessby the time to burn-through. The insulating effective

8、ness isdetermined from back-face temperature measurements. Insula-tion index numbers are computed by dividing the times fortemperature changes of 80, 180, and 380C, from the initialambient temperature, by the original thickness. The insulation-to-density performance is computed by dividing the insul

9、ationindex by the density of the panel.3.2 The general characteristics of the oxyacetylene heatsource are:3.2.1 Heat Flux835 W/cm2(cold-wall calorimeter).3.2.2 Velocity210 m/s (cold, unreacted gases).3.2.3 Neutral flame conditions.4. Significance and Use4.1 This test method is intended to screen the

10、 most obviouspoor materials from further consideration. Since the combus-tion gases more closely resemble the environment generated inrocket motors, this test method is more applicable to screeningmaterials for nozzles and motor liners than for aerodynamicheating.4.2 The environment for any specific

11、 high-temperature ther-mal protection problem is peculiar to that particular applica-tion. The conditions generated by the oxyacetylene heat sourcein this test method represent only one set of conditions; they donot simulate any specific application. Thus, the test resultscannot be used to predict d

12、irectly the behavior of materials forspecific environments, nor can they be used for design pur-poses. However, over a number of years, the test has beenuseful in determining the relative merit of materials, particu-larly in weeding out obviously poor materials from moreadvanced data-generation prog

13、rams. It has also been consid-ered for use as a production quality-control test for rocketinsulation materials.4.3 The tester is cautioned to use prudence in extending theusefulness of the test method beyond its original intent,namely, screening. For situations having environments widelydifferent fr

14、om those of the test, the user is urged to modify theoxyacetylene burner conditions to suit his requirements orperhaps change to a different heat-generating device thatprovides better simulation.5. Apparatus5.1 GeneralThe apparatus shall consist of an oxyacety-lene burner, a specimen holder, and mea

15、ns for measuring the1This test method is under the jurisdiction of ASTM Committee E21 on SpaceSimulation and Applications of Space Technology and is the direct responsibility ofSubcommittee E21.08 on Thermal Protection.Current edition approved Dec. 8, 1980. Published February 1981. Originallypublish

16、ed as E 285 65T. Last previous edition E 285 70.2Annual Book of ASTM Standards, Vol 08.01.3Available from Standardization Documents Order Desk, Bldg. 4 Section D, 700Robbins Ave., Philadelphia, PA 19111-5098, Attn: NPODS.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshoh

17、ocken, PA 19428-2959, United States.time to burn-through and for recording the back-face tempera-ture history of the specimen. Auxiliary apparatus all consist ofa calorimetric device to measure heat-transfer rate as specifiedin 5.5.5.2 Heat SourceThe hot-gas source shall consist of awelding torch wi

18、th suitable storage for acetylene and oxygen,together with suitable manifolds, flow regulators, and flow andpressure indicators, as shown schematically in Fig. 1.5.2.1 TorchThe torch shall be a Victor Model 3154andshall be mounted so that the flame can be made to contact thespecimen in less than12 s

19、 from the time of actuation.NOTE 1Both a solenoid-powered mechanism and a hand-operatedsystem of levers and push rods have been found to be adequate for thispurpose.5.2.2 Torch TipThe tip shall be a Victor welding nozzle,Type 4, No. 7, equipped with a water jacket to minimizedamage to the tip (Note

20、2).4Details of the water jacket areshown in Figs. 2 and 3 and the torch tip is shown in Fig. 4.NOTE 2Proprietary designation cannot be avoided because of thebroad spectrum of heat flux and flame patterns produced by competitivetorch tips of similar size. The Victor torch tip was selected on the basi

21、s ofpopularity, reproducibility of test results, and the relatively high heat fluxit produces.5.2.3 Fuel Storage and ManifoldA minimum of threeacetylene cylinders shall be tapped simultaneously through amanifold and suitable pressure regulators. Cylinders shall bestored in an upright position and he

22、ld at room temperature forat least 1 h, or until at equilibrium with room temperature,before using. The complete bank of cylinders shall be changedwhen the gage reads 0.7 MPa (100 psi). Acetylene storagetanks shall be protected by a check valve against accidentalbackflow from the torch. The acetylen

23、e shall be maintained at294.2 K (70F) when possible (Note 3). The purity of acetylenegas shall conform with Federal Specification BB-A-106a. Theminimum acetylene content shall be 98 %.NOTE 3If this is not possible, the flow rate shall be corrected to 294.2K in accordance with the flow rate specified

24、 in 5.2.7. The gas temperatureshall not be allowed to exceed 299 K (79F) or go below 289 K (61F).Flow rates are corrected to 294.2 K because most manufacturers use thistemperature as standard for calibration charts.5.2.4 Oxygen StorageA minimum of one oxygen tankshall be tapped through suitable pres

25、sure regulators. Theoxygen shall be maintained at 294.2 K when possible (Note 4).The purity of oxygen gas shall conform with Federal Specifi-cation BB-O-925a. The minimum oxygen content shall be99.5 %.5.2.5 Safety WallThe acetylene and oxygen storage areashall be isolated from the torch and the oper

26、ating area by asuitable safety wall. For convenience, a two-stage regulatorshall be located in the storage space and a single-stage pressureregulator located in the operating area.5.2.6 Pressure RegulatorsThe regulators for the oxygenand the acetylene shall be capable of supplying the flow ofgases s

27、pecified in 5.2.7.5.2.7 FlowmetersThe flowmeters for the acetylene andthe oxygen shall be capable of supplying an accurate flow ofgases.5A variation of 65 % in gas flow rate due to instrumen-tation inaccuracies shall be permissible. The total flow rate ofunreacted gases shall be 6.37 standard m3/h (

28、294.2 K, 0.1 MPa)(225 standard ft3/h (70.0F, 14.7 psia), and the volume ratio ofoxygen to acetylene shall be 1.20, which corresponds toessentially a neutral (oxygen-free) atmosphere.NOTE 4Flowmeter and pressure-gage settings are not specified be-cause they will vary with the size and brand of flowme

29、ter used. Consultmanufacturers instructions and calibration charts that are furnished withthe flowmeters.5.2.8 Flow-Pressure GagesSuitable pressure gages shallbe located at the exit (downstream) side of the flowmeters tomonitor metered gas pressure. These gages shall be capable ofsupplying pressure

30、measurements to maintain an accurate flowof gases in accordance with the specifications stated in 5.2.7.NOTE 5Pressure gages graduated 0 to 50 psig for oxygen and 0 to 30psig for acetylene, both in 1-psig increments, have been found to besuitable.5.2.9 Temperature-Measuring DevicesGas temperaturessh

31、all be measured with thermocouples, thermistors, or othersuitable devices located at the exit (downstream) side of theflowmeters. Accuracy shall be within 61.0K(61.8 F).5.2.10 Piping, Hoses, and Needle ValvesAny combina-tion of piping, tubing, hoses, and needle valves may beemployed that have suffic

32、ient flow capacity to allow the fueland oxidant to flow and be controlled at the specified flowrates.4Victor Equipment Co., 2800 Airport Rd., Denton, TX 76207.5Fischer-Porter Meter size 4, Fig. 1735, float shape BSVT, equivalent capacity3.35 standard ft3/min air, has been found satisfactory for this

33、 purpose.FIG. 1 Schematic Diagram of Gas SystemE 28525.3 Specimen HolderThe specimen and the calorimetershall be supported in a suitable fixture arranged in such afashion that it can be moved to align and set the distance andangle (see 8.4 for specifications) between the specimen, orcalorimeter, and

34、 the torch tip (Note 7). The back surface of thespecimen shall be unobstructed by the holder for a distance of25.4 mm (1.00 in.) out from the center of the specimen. Onlymaterials with a thermal conductivity of 0.2 W/mK (1.4Btuin./hft2F) or less shall contact the back of the specimen.The front surfa

35、ce of the specimen shall be unobstructed for adistance of 48.0 mm (1.89 in.) out from the center of thespecimen. The total area of contact with front and backsurfaces shall not exceed 52.0 cm2(8.06 in.2).NOTE 6A lathe bed with the specimen holder mounted on the toolcarriage has been found to be adeq

36、uate for the purpose. Water cooling ofthe holder is recommended to prolong service life.5.4 Back-Face Temperature MeasurementThe back-facetemperature history shall be measured with a No. 28 AWGgage Chromel-Alumel thermocouple.NOTE 7For soft specimens, it shall be permissible to attach a thincopper d

37、isk, no larger than 10 mm (0.39 in.) in diameter, to thethermocouple junction.5.4.1 Thermocouple MountingA spring-loaded, two-holeceramic support rod no larger than 3.2 mm (18 in.) in diametershall be used to maintain good contact between the thermo-couple and the back surface of the specimen.5.4.2

38、Temperature RecorderThe thermocouple emf shallbe recorded as back-face temperature, in degrees Celsius, as afunction of time during the test. The response time of therecorder shall be1sorless for full-scale deflection and thechart speed shall be at least 12 m/s (approximately 8 in./min).The recorder

39、 shall be equipped with a suitable auxiliary timingpen to indicate the starting time of the test.5.4.3 Starting SwitchAn electric switch shall be installedon the torch mechanism to actuate the timing pen on thetemperature recorder and the electric clock for the erosion ratemeasurement.5.5 Calorimete

40、rThe cold wall heat flux of the hot-gassource shall be measured by using a calorimetric device.5.6 Burn-Through DetectorA device such as a mirror,photocell, or direct visual means shall be used to detectburn-through of the specimen for termination of the test.5.6.1 TimerAn electric time clock, 0 to

41、1000 s graduatedin 0.1-s increments, shall be used to measure the time toFIG. 2 Details of Water Jacket for Oxyacetylene TorchFIG. 3 Assembly of Water Jacket for Oxyacetylene TorchE 2853burn-through of the specimen.6. Test Specimen6.1 The test specimen shall be a square, flat panel 6.35 60.41 mm (0.

42、250 6 0.016 in.) thick.6.2 The dimensions of length and width shall both be 101.6+ 0.0, 0.71 mm (4.000 +0.000, 0.028 in.).6.3 Five replicates of each type of specimen shall be tested.6.4 The thickness and density of the specimen shall bemeasured before the test.6.4.1 The density shall be measured in

43、 accordance with TestMethods D 792. If the immersing fluid is known to haveadverse effects on the specimen, the density shall be deter-mined by a simple weight-to-volume calculation wherein thevolume is determined by scaling the specimen.6.4.2 The thickness at the point of flame impingement shallbe

44、determined with suitable micrometer calipers or equivalent.Reasonable care shall be taken to avoid depressing softspecimens.7. Calibration7.1 Temperature recorders should be calibrated at frequentintervals using known reference voltages. The frequency ofcalibration and exact procedure are not given

45、here because ofthe large variety of recorders and standard voltage devices onthe market. A general procedure found to be satisfactory,however, consists of connecting a potentiometer to the inputside of the recorder. Various input voltages are set on thepotentiometer and the recorder is adjusted to r

46、ead thesevoltages.7.2 The heat flux should be measured at the start of eachtesting day and at any time during testing when there is asuspicion of faulty torch operation, such as an irregularlyshaped flame or an unusual color or noise in the flame. Thetorch tip should be replaced if the heat flux is

47、outside thespecifications listed below.7.2.1 Mount the calorimeter in the specimen holder andconnect the thermocouple leads to the temperature recorder.Align the center of the calorimeter with the center line of thetorch (Note 8) and set the correct distance between thecalorimeter face and the end o

48、f the torch tip. Make heat-fluxmeasurements at on-axis positions of 19.00 and 25.40 6 0.30mm (0.748 and 1.000 6 0.012 in.).NOTE 8A metal rod, thin enough to slide into the torch port has beenfound to be suitable for aligning the central axes of the copper cylinder (ofthe calorimeter) and the torch t

49、ip. Absolute alignment is difficult becauseof the uncertainty of the exact location of the axis of the hot gas withrespect to the axis of the torch tip. Moreover, since the torch port has avariable inside diameter, the aligning tool cannot be rigidly held in placeto locate the axis. Best results have been obtained by inserting the tool intothe torch port and slowly rotating the tool so that its free end describes acircle. Alignment adjustments are then made until the circle described isconcentric with the copper cylinder of the calorimet