ASTM E2470-2009(2015) Standard Specification for Polyester Grade Ethylene Glycol《聚酯级乙二醇的标准规格》.pdf

1、Designation: E2470 09 (Reapproved 2015)Standard Specification forPolyester Grade Ethylene Glycol1This standard is issued under the fixed designation E2470; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision.

2、A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope*1.1 This specification covers polyester grade ethylene gly-col.1.2 Review the current Materials Safety Data Sheets(MSDS) for detailed in

3、formation concerning toxicity, first aidprocedures, handling and safety precautions.1.3 The following applies to all specified limits in thisstandard; for purposes of determining conformance with thisstandard, an observed value or a calculated value shall berounded off “to the nearest unit” in the l

4、ast right-hand digitused in expressing the specification limit, in accordance withthe rounding-off method of Practice E29.1.4 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.5 The following safety hazards caveat pertains only

5、to thetest methods portion, Section 5, described in this specification:This standard does not purport to address all of the safetyconcerns, if any, associated with its use. It is the responsibilityof the user of this standard to establish appropriate safety andhealth practices and determine the appl

6、icability of regulatorylimitations prior to use.2. Referenced Documents2.1 ASTM Standards:2D482 Test Method for Ash from Petroleum ProductsD1078 Test Method for Distillation Range of Volatile Or-ganic LiquidsD1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)D1722 Test Method for Wa

7、ter Miscibility of Water-SolubleSolventsD4052 Test Method for Density, Relative Density, and APIGravity of Liquids by Digital Density MeterE29 Practice for Using Significant Digits in Test Data toDetermine Conformance with SpecificationsE202 Test Methods for Analysis of Ethylene Glycols andPropylene

8、 GlycolsE300 Practice for Sampling Industrial ChemicalsE1064 Test Method for Water in Organic Liquids by Coulo-metric Karl Fischer TitrationE1615 Test Method for Iron in Trace Quantities Using theFerroZine MethodE2193 Test Method for Ultraviolet Transmittance of Mono-ethylene Glycol (Ultraviolet Spe

9、ctrophotometric Method)E2313 Test Method for Aldehydes in Mono-, Di-, andTriethylene Glycol (Spectrophotometric Method)E2409 Test Method for Glycol Impurities in Mono-, Di-, Tri-and Tetraethylene Glycol and in Mono- and DipropyleneGlycol(Gas Chromatographic Method)E2469 Test Method for Chloride in M

10、ono-, Di- and Tri-ethylene Glycol by Ion ChromatographyE2679 Test Method for Acidity in Mono-, Di-, Tri- andTetraethylene Glycol byNon-Aqueous PotentiometricTitrationE2680 Test Method for Appearance of Clear, TransparentLiquids (Visual Inspection Procedure)3. Requirements3.1 Polyester grade ethylene

11、 glycol shall conform to thespecification chemical and physical requirements (see Table 1).4. Sampling4.1 Sample ethylene glycol in accordance with the appro-priate sections of Practice E300 for liquid samples.5. Test Methods5.1 Test each composite sample for chemical and physicalrequirements using

12、the test methods specified in 3.1. Many ofthese test methods, along with alternative test methods andtechnologies, can be found in Test Methods E202. In case of adispute, test methods identified in 3.1 of this specification shallbe the preferred test methods.1This specification is under the jurisdic

13、tion of ASTM Committee E15 onIndustrial and Specialty Chemicals and is the direct responsibility of SubcommitteeE15.02 on Product Standards.Current edition approved June 1, 2015. Published June 2015. Originallyapproved in 2009. Last previous edition approved in 2009 as E2470-09. DOI:10.1520/E2470-09

14、R15.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.*A Summary of Changes section appears at the end of this

15、standardCopyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States16. Packaging, Package Markings, and Transportation6.1 The packaging, labeling, and transportation of commer-cial quantities shall conform to applicable federal, state, andlocal r

16、egulation. Conformance is the responsibility of themanufacturer and the shipper.7. Keywords7.1 ethylene glycol; polyester gradeSUMMARY OF CHANGESSubcommittee E15.02 has identified the location of selected changes to this standard since the last issue(E2470-07) that may impact the use of this standar

17、d.(1) Replaced two test methods within the specification with testmethods that have been recently adopted by E15 and reflectnewer technologies used in the industry.(2) Section 2, Referenced Documents, was revised.(3) Table 1 was revised.(4) Added Summary of Changes section.ASTM International takes n

18、o position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the riskof infringement of such rights, are entirely their own respon

19、sibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standardsand should be addressed

20、to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you shouldmake your views known to the ASTM Committee on Standards, at the ad

21、dress shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone)

22、, 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the Copyright Clearance Center, 222Rosewood Drive, Danvers, MA 01923, Tel: (978) 646-2600; http:/ 1 Chemical and Physical Specification R

23、equirementsSpecification Requirements min max ASTM Test MethodAcidity as Acetic Acid, % mass (m/m) 0.002 E2679Aldehydes as Acetaldehyde, ug/g not reported E2313Appearance, Clear & Free from Suspended Matter pass E2680Chloride as Cl, ug/g 0.2 E2469Color, platinum cobalt 5 D1209GlycolsEthylene glycol,

24、 % mass (m/m)Diethylene glycol, % mass (m/m)99.90.05E2409Iron, ug/g 0.1 E1615Ultraviolet Transmittanceat 220 nm, %Tat 250 nm, %Tat 275 nm, %Tat 350 nm, %T70909498E2193Water, % mass (m/m) 0.05 E1064Typical Properties min max ASTM Test MethodAsh, % mass (m/m) 0.004 D482Distillation RangeInitial Boiling Point, CDry Point, C196200D1078Relative Density at20/20 Cor25/25 C1.1151or1.11291.1156or1.1134D4052Water Miscibility miscible D1722E2470 09 (2015)2