1、Designation: E515 11Standard Practice forLeaks Using Bubble Emission Techniques1This standard is issued under the fixed designation E515; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the year of last revision. A number in parent
2、heses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice covers procedures for detecting or locatingleaks, or both, by bubble emission techniques. A quantitativemeasure is not practical. The nor
3、mal limit of sensitivity for thistest method is 4.5 3 1010mol/s (1 3 105Std cm3/s).21.2 Two techniques are described:1.2.1 Immersion technique, and1.2.2 Liquid application technique.NOTE 1Additional information is available in ASME Boiler andPressure Vessel Code, Section V, Article 10-Leak Testing,
4、and GuideE479.1.3 The values stated in SI units are to be regarded asstandard. No other units of measurement are included in thisstandard.1.4 This standard does not purport to address the safetyconcerns, if any, associated with its use. It is the responsibilityof the user of this standard to establi
5、sh appropriate safety andhealth practices and determine the applicability of regulatorylimitations prior to use.2. Referenced Documents2.1 ASTM Standards:3E479 Guide for Preparation of a Leak Testing SpecificationE543 Specification for Agencies Performing Nondestruc-tive TestingE1316 Terminology for
6、 Nondestructive Examinations2.2 Other Documents:SNT-TC-1A Recommended Practice for Personnel Qualifi-cation and Certification in Nondestructive Testing4ANSI/ASNT CP-189 ASNT Standard for Qualification andCertification of Nondestructive Testing Personnel4ASME Boiler and Pressure Vessel Code, Section
7、V, Article10-Leak Testing5NAS-410 Certification and Qualification of NondestructiveTest Personnel62.3 Military Standard:MIL-L-25567D Leak Detection Compound Oxygen Sys-tems73. Terminology3.1 DefinitionsFor definitions of terms used in this testmethod, see Terminology E1316, Section E.4. Summary of P
8、ractice4.1 The basic principle of this method consists of creating apressure differential across a leak and observing for bubbles ina liquid medium located on the low pressure side. Thesensitivity of the method is dependent on the pressure differ-ential, the gas used to create the differential, and
9、the liquid usedfor testing. As long as the pressure differential can be main-tained across the area to be tested, this method can be used.5. Basis of Application5.1 The following items are subject to contractual agree-ment between the parties using or referencing this test method:5.2 Personnel Quali
10、fications5.2.1 If specified in the contractual agreement. Personnelperforming examinations to this test method shall be qualifiedin accordance with a nationally or internationally recognizedNDT personnel qualification practice or standard such asANSI/ASNT CP-189, SNT-TC-1A, NAS-410, or similar docu-
11、ment and certified by the employer or certifying agency, asapplicable. The practice or standard used and its applicablerevision shall be identified in the contractual agreement.1This test method is under the jurisdiction of ASTM Committee E07 onNondestructive Testing and is the direct responsibility
12、 of Subcommittee E07.08 onLeak Testing Method.Current edition approved July 1, 2011. Published July 2011. Originally approvedin 1974. Last previous edition approved in 2005 as E515 - 05. DOI: 10.1520/E0515-11.2The gas temperature is referenced to 0C. To convert to another gas referencetemperature, T
13、ref, multiply the leak rate by (Tref+ 273)/273.3For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.4Available fro
14、mAmerican Society for Nondestructive Testing (ASNT), P.O. Box28518, 1711 Arlingate Ln., Columbus, OH 43228-0518, http:/www.asnt.org.5Available from American Society of Mechanical Engineers (ASME), ASMEInternational Headquarters, Three Park Ave., New York, NY 10016-5990, http:/www.asme.org.6Available
15、 from Aerospace Industries Association of America, Inc. (AIA), 1000Wilson Blvd., Suite 1700,Arlington, VA22209-3928, http:/www.aia-aerospace.org.7Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http:/dodssp.daps.dla.mil.1
16、Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.5.3 Qualification of Nondestructive AgenciesIf specifiedin the contractual agreement, NDT agencies shall be qualifiedand evaluated as described in Practice E543. The applicableedition of
17、 Practice E543 shall be specified in the contractualagreement.5.4 Re-examination of Repaired/Reworked ItemsRe-examination of repaired/reworked items is not addressed in thistest method, they shall be specified in the contractual agree-ment.6. Significance and Use6.1 The immersion technique is freque
18、ntly used to locateleaks in sealed containers. Leaks in a container can be seenindependently. Leak size can be approximated by the size ofthe bubble. It is not suitable for measurement of total systemleakage.6.2 The liquid film technique is widely applied to compo-nents and systems that can not easi
19、ly be immersed and is usedto rapidly locate leaks. An approximation of leak size can bemade based on the type of bubbles formed, but the technique isnot suitable for measuring leakage rate. It can be used with avacuum box to test vessels which cannot be pressurized orwhere only one side is accessibl
20、e.6.3 AccuracyThis practice is not intended to measureleakage rates, but to locate leaks on a go, no-go basis. Theiraccuracy for locating leaks of 4.5 3 1010mol/s (1 3 104Stdcm3/s)2and larger is 65 %.Accuracy for locating smaller leaksdepends upon the skill of the operator.6.4 RepeatabilityOn a go,
21、no-go basis, duplicate tests bythe same operator should not vary by more than 65 % for leaksof 4.5 3 109mol/s (1 3 104Std cm3/s).26.5 ReproducibilityOn a go, no-go basis, duplicate testsby other trained operators should not vary by more than 10 %for leaks of 4.5 3 109mol/s (1 3 104Std cm3/s)2and lar
22、ger.7. Interferences7.1 Surface contamination of the test specimen, if smallimmersed parts, in the form of grease, rust, weld slag, etc., maybe a source of bubbles giving false indication of leakage. Testspecimens should be thoroughly cleaned to avoid rejection ofacceptable items.7.2 Contaminated de
23、tection fluid or one that foams onapplication can cause spurious surface bubbles on the testspecimen.7.3 An excessive vacuum on the low-pressure side whenusing the vacuum differential technique may cause the detec-tion fluid to boil.7.4 If the component to be tested has parts made of stainlesssteel,
24、 nickel, or chromium alloys, the test fluid must have asulfur and halogen content of less than 10 ppm of each.7.5 Immediate application of high pressure may cause largeleaks to be missed in the liquid application technique.7.6 If the component to be tested has parts made ofpolyethylene or structural
25、 plastic, the test fluid must notpromote environmental stress cracking (E.S.C).7.7 If the test fluid is to be used on oxygen systems it mustmeet the requirements of MIL-L-25567D.8. Immersion Technique8.1 ApplicationThis technique is applicable to test speci-mens whose physical size allows immersion
26、in a container offluid when the test specimen can be sealed prior to the test.8.2 Techniques for Creating Pressure Differential:8.2.1 Pressurization of Test SpecimenSeal componentsand apply an elevated pressure, or if accessible, increase theinternal pressure for test purposes.8.2.2 Elevated-Tempera
27、ture Test FluidHeat the test fluidto a temperature not exceeding the maximum rated temperatureof the test specimen. This will cause expansion of the gasinside the test specimen, creating a pressure differential. Thistechnique is usually limited to use on very small parts.8.2.3 Vacuum TechniqueImmers
28、e the test specimen in thetest fluid and then place the test fluid container in the vacuumchamber. Reduce the pressure in the chamber to a point thatdoes not allow the test fluid to boil, thus creating a pressuredifferential. This technique is normally used on very smallparts.8.3 Test Fluids Used in
29、 Immersion TechniqueThe follow-ing test fluids may be used, provided they are not detrimentalto the component being tested:8.3.1 WaterShould be treated with a wetting agent up to13 by volume to reduce surface tension and promote bubblegrowth.8.3.2 Methyl Alcohol (Technical Grade), UndilutedNotsuitab
30、le for the heated-bath technique or the vacuum technique.8.3.3 Ethylene Glycol (Technical Grade), Undiluted.8.3.4 Mineral OilDegreasing of the test specimens maybe necessary. This is the most suitable fluid for the vacuumtechnique.8.3.5 Fluorocarbons or GlycerinFluorocarbons are notrecommended for s
31、tainless steel nuclear applications.8.4 Procedures:8.4.1 Pressurized Test Specimen:8.4.1.1 Specimens Sealed at Elevated PressuresPlace thetest specimen or area being tested in the selected test fluid andobserve for a minimum period of 2 min. Interpret as leakage astream of bubbles originating from a
32、 single point or two ormore bubbles that grow and then release from a single point.8.4.1.2 Very Small Specimens Sealed at Ambient or ReducedPressuresPlace the test specimen in a pressure chamber andexpose to an elevated pressure. The actual pressure is depen-dent on the specimens. Place the specimen
33、 in the selected testfluid within 2 min after removal from the pressure chamber andobserve for a minimum period of 2 min. Interpret as leakage astream of bubbles originating from a single point.8.4.2 Elevated Temperature Test Fluid Place the testspecimen in the test fluid which is stabilized and mai
34、ntained atan elevated temperature at a temperature dependent on thespecimen. Observe for a stream of bubbles originating from asingle point or two or more bubbles that grow and then releasefrom a single point. Interpret either as indicating leakage. Thetime of observation shall be dependent on the i
35、nternal volumeof the specimen and the case materials of the enclosure. Dwelltime must be sufficient to allow a pressure increase to apressure dependent on the specimen.E515 1128.4.3 Vacuum TechniquePlace the test specimen in acontainer of the selected test fluid and place the container in avacuum ch
36、amber with viewing ports. Reduce the pressure inthe vacuum chamber and observe for a stream of bubblesoriginating from a single point or two or more bubbles thatgrow and then release from a single point. The amount ofvacuum used will be dependent on the test fluid and should bethe maximum obtainable
37、 without the test fluid boiling. Thistechnique is also applicable to unsealed components or speci-men sections by use of the apparatus shown in Fig. 1.9. Liquid Application Technique9.1 ApplicationThis technique is applicable to any testspecimen on which a pressure differential can be created across
38、the area to be examined. An example of this technique is theapplication of leak-test solutions to pressurized gas-line joints.It is most useful on piping systems, pressure vessels, tanks,spheres, pumps, or other large apparatus on which the immer-sion techniques are impractical.9.2 Location of Bubbl
39、e Test FluidApply the test liquid tothe low-pressure side of the area to be examined and thenexamine the area for bubbles in the fluid. Take care in applyingthe fluid to prevent formation of bubbles. Flow the solution onthe test area. Joints must be completely coated. The pressuredifferential should
40、 be created before the fluid is applied, toprevent clogging of small leaks.9.3 Type of Bubble Test FluidA solution of commercialleak-testing fluids may be used. The use of soap buds orhousehold detergents and water is not considered a satisfactoryleak-test fluid for a bubble test, because of lack of
41、 sensitivitydue to masking by foam. The fluid should be capable of beingapplied free of bubbles so that a bubble appears only at a leak.The fluid selected should not bubble except in response toleakage.9.4 Vacuum TechniquePlace a vacuum box (see Fig. 2)over the bubble test fluid. In testing equipmen
42、t, such as storagetank floors and roofs, place the vacuum box over a section ofthe weld seam and evacuate to 3 psi 20.68 kPa (or what theapplicable standard requires) and hold for a minimum time of15 s.10. Keywords10.1 bubble leak testing; film solution leak test; immersionleak test; leak testing; v
43、acuum box leak testingFIG. 1 Vacuum Chamber TechniqueE515 113ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such p
44、atent rights, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited e
45、ither for revision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fai
46、r hearing you shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this sta
47、ndard may be obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).FIG. 2 Vacuum BoxE515 114
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