1、Designation: E 662 09An American National StandardStandard Test Method forSpecific Optical Density of Smoke Generated by SolidMaterials1This standard is issued under the fixed designation E 662; the number immediately following the designation indicates the year oforiginal adoption or, in the case o
2、f revision, the year of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon () indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the Department of Defense.1. Scope1.1 This fire-tes
3、t-response standard covers determination ofthe specific optical density of smoke generated by solidmaterials and assemblies mounted in the vertical position inthicknesses up to and including 1 in. (25.4 mm).1.2 Measurement is made of the attenuation of a light beamby smoke (suspended solid or liquid
4、 particles) accumulatingwithin a closed chamber due to nonflaming pyrolytic decom-position and flaming combustion.1.3 Results are expressed in terms of specific optical densitywhich is derived from a geometrical factor and the measuredoptical density, a measurement characteristic of the concentra-ti
5、on of smoke.1.4 This test method is intended for use in research anddevelopment and not as a basis for ratings for regulatorypurposes.1.5 This standard measures and describes the response ofmaterials, products, or assemblies to heat and flame undercontrolled conditions, but does not by itself incorp
6、orate allfactors required for fire hazard or fire risk assessment of thematerials, products or assemblies under actual fire conditions.1.6 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It is theresponsibility of the user of this standard to est
7、ablish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.1.7 The values stated in inch-pound units are to be regardedas standard. Values stated in parentheses are for informationonly.2. Referenced Documents2.1 ASTM Standards:2D 2843 Test
8、 Method for Density of Smoke from the Burn-ing or Decomposition of PlasticsE 176 Terminology of Fire Standards3. Terminology3.1 DefinitionsFor definitions of terms found in this testmethod refer to Terminology E 176.4. Summary of Test Method4.1 This test method employs an electrically heated radiant
9、-energy source mounted within an insulated ceramic tube andpositioned so as to produce an irradiance level of 2.2 Btu/sft2(2.5 W/cm2) averaged over the central 1.5-in. (38.1-mm)diameter area of a vertically mounted specimen facing theradiant heater. The nominal 3 by 3-in. (76.2 by 76.2-mm)specimen i
10、s mounted within a holder which exposes an areameasuring 2916 by 2916 in. (65.1 by 65.1 mm). The holder isable to accommodate specimens up to 1 in. (25.4 mm) thick.This exposure provides the nonflaming condition of the test.4.2 For the flaming condition, a six-tube burner is used toapply a row of eq
11、uidistant flamelets across the lower edge ofthe exposed specimen area and into the specimen holdertrough. This application of flame in addition to the specifiedirradiance level from the heating element constitutes theflaming combustion exposure.4.3 The test specimens are exposed to the flaming andno
12、nflaming conditions within a closed chamber. A photometricsystem with a vertical light path is used to measure the varyinglight transmission as smoke accumulates. The light transmit-tance measurements are used to calculate specific opticaldensity of the smoke generated during the time period to reac
13、hthe maximum value.35. Significance and Use5.1 This test method provides a means for determining thespecific optical density of the smoke generated by specimens ofmaterials and assemblies under the specified exposure condi-tions. Values determined by this test are specific to thespecimen or assembly
14、 in the form and thickness tested and are1This test method is under the jurisdiction of ASTM Committee E05 on FireStandards and is the direct responsibility of Subcommittee E05.21 on Smoke andCombustion Products.Current edition approved March 1, 2009. Published April 2009. Originallyapproved in 1979
15、. Last previous edition approved in 2006 as E 662 061.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3Additi
16、onal parameters, such as the maximum rate of smoke accumulation, timeto a fixed optical density level, or a smoke obscuration index provide potentiallyuseful information. See Appendix X1.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United State
17、s.not to be considered inherent fundamental properties of thematerial tested. Thus, it is likely that closely repeatable orreproducible experimental results are not to be expected fromtests of a given material when specimen thickness, density, orother variables are involved.5.2 The photometric scale
18、 used to measure smoke by thistest method is similar to the optical density scale for humanvision. However, physiological aspects associated with visionare not measured by this test method. Correlation with mea-surements by other test methods has not been established.45.3 At the present time no basi
19、s is provided for predictingthe density of smoke generated by the materials upon exposureto heat and flame under other fire conditions.5.4 The test method is of a complex nature and the dataobtained are sensitive to variations which in other test methodsmight be considered to be insignificant (see S
20、ection 6). Aprecision statement based on the results of a roundrobin test bya prior draft version of this test method is given in 14.15.5 In this procedure, the specimens are subjected to one ormore specific sets of laboratory test conditions. If different testconditions are substituted or the end-u
21、se conditions arechanged, it is not always possible by or from this test methodto predict changes in the fire-test-response characteristicsmeasured. Therefore, the results are valid only for the fire testexposure conditions described in this procedure.6. Limitations6.1 If during the test of one or m
22、ore of the three replicatesamples there occurs such unusual behavior as (1) the speci-men falling out of the holder, (2) melted material overflowingthe sample holder trough, (3) self-ignition in the pyrolysismode, (4) extinguishment of the flame tiplets (even for a shortperiod of time), or (5) a spe
23、cimen being displaced from thezone of controlled irradiance, then an additional three samplesof the identical preconditioned materials shall be tested in thetest mode in which the unusual behavior occurred. Dataobtained from the improper tests noted above shall not beincorporated in the averaged dat
24、a but the occurrence shall bereported. The test method is not suitable if more than three ofthe six replicates tested show these characteristics.6.2 The test method has proven sensitive to small variationsin sample geometry, surface orientation, thickness (eitheroverall or individual layer), weight,
25、 and composition. It is,therefore, critical that the replicate samples be cut, sawed, orblanked to identical sample areas, 3 by 3, +0, 0.03 in. (76.2by 76.2, +0, 0.8 mm), and that records be kept of therespective weights with the individual test data. It is feasiblethat evaluation of the obtained da
26、ta together with the individualweights will assist in assessing the reasons for any observedvariability in measurements. Preselection of samples withidentical thickness or weight, or both, are potential methods toreduce the variability but are likely to not be truly indicative ofthe actual variabili
27、ty to be expected from the material asnormally supplied.6.3 The results of the test apply only to the thickness of thespecimen as tested. There is no common mathematical formulato calculate the specific optical density of one thickness of amaterial when the specific optical density of another thickn
28、essof the same material is known.6.4 The test method is sensitive to small variations of theposition of the specimen and radiometer relative to the radiantheat source.6.5 It is critical to clean the test chamber, and to removeaccumulated residues from the walls when changing from onetest material to
29、 another, to ensure that chemical or physicalrecombination with the effluents or residues produced does notaffect the data obtained. Even when testing the same material,excessive accumulations of residue shall not be permitted tobuild up since ruggedness tests have indicated that suchaccumulations s
30、erve as additional insulators tending to reducenormally expected condensation of the aerosol, thereby raisingthe measured specific optical density.6.6 With resilient samples, take extreme care to ensure thateach replicate sample in its aluminum foil wrapper is installedso that each protrudes identic
31、ally through the front sampleholder opening. Unequal protrusion will subject the samples todifferent effective irradiances and to slightly different ignitionexposures. Excessive protrusion of specimens has the potentialto cause drips or for the specimen to sag onto the burner,clogging the flame jets
32、 and thereby invalidating the test.6.7 The measurements obtained have also proven sensitiveto small differences in conditioning (see Section 9). Manymaterials such as carpeting and thick sections of wood,plastics, or plywood require long periods to attain equilibrium(constant weight) even in a force
33、d-draft humidification cham-ber.7. Apparatus7.1 Fig. 1 shows examples of the test apparatus, with adetailed description contained in the remainder of Section 7and in Annex A2. The apparatus shall include the following:7.1.1 Test ChamberAs shown in Fig. 1, the test chambershall be fabricated from lam
34、inated panels5to provide insidedimensions of 36 by 24 by 36 618 in. (914 by 610 by 914 63 mm) for width, depth, and height, respectively. The interiorsurfaces shall consist of porcelain enameled metal, or equiva-lent coated metal resistant to chemical attack and corrosion,and suitable for periodic c
35、leaning. Sealed windows shall beprovided to accommodate a vertical photometric system. Allother chamber penetrations shall be sealed. When all openingsare closed, the chamber shall be capable of developing andmaintaining positive pressure during test periods, in accor-dance with 11.11.7.1.2 Radiant
36、Heat FurnaceAs shown in Fig. 2,anelectric furnace with a 3-in. (76.2-mm) diameter opening shall4Other test methods for measuring smoke available at the time of the publica-tions referenced have been reviewed and summarized in “The Control of Smoke inBuilding FiresAState of theArt Review.” Materials
37、Research and Standards,Vol42, April 1971, pp. 1623 and “A Report on Smoke Test Methods,” ASTMStandardization News, August 1976, pp. 1826.5Commercially available panels of porcelain-enameled steel (interior surface)permanently laminated to an asbestos-magnesia core and backed with galvanizedsteel (ex
38、terior surface), total thickness316 in. (9.6 mm), have been found suitable.E662092be used to provide a constant irradiance on the specimensurface. The furnace shall be located along the centerlineequidistant between the front and back of the chamber, with theopening facing toward and about 12 in. (3
39、05 mm) from theright wall. The centerline of the furnace shall be about 734 in.(195 mm) above the chamber floor. The furnace control systemshall maintain the required irradiance level, under steady-stateconditions with the chamber door closed, of 2.20 6 0.04Btu/ft2s (2.50 6 0.05 W/cm2) for 20 min. T
40、he control systemshall consist of an autotransformer or alternative controldevice, and a voltmeter or other means for monitoring theelectrical input. Where line voltage fluctuations exceed 62.5 ,a constant voltage transformer is required to maintain theprescribed irradiance level.APhotomultiplier tu
41、be housing NFlowmeter shutoff valvesBChamber OSample mover knobCBlow-out panel (in floor of chamber) PLight source switchDHinged door with window QLight source voltage jacksEExhaust vent control RLine switchFRadiometer output jacks SBase cabinetGTemperature (wall) indicator TIndicating lampsHAutotra
42、nsformer UMicrophotometer (photomultiplier)IFurnace switch VOptical system rodsJVoltmeter (furnace) WOptical system floor windowKFuse holder (furnace) XExhaust vent damperLRadiometer air flowmeter YInlet vent damperMGas and air (burner) flowmeter ZAccess portsFIG. 1 Smoke Density Chamber AssemblyE66
43、20937.1.3 Specimen HolderSpecimen holders shall conform inshape and dimension to that shown in Fig. 3 and be fabricatedto expose a 2916 by 2916-in. (65.1 by 65.1-mm) specimen area.Also shown in Fig. 3 are the spring and rods for retaining thespecimen within the holders.7.1.4 Framework for Support of
44、 Furnace and SpecimenHolderThe furnace and specimen supporting frameworkshall be constructed essentially in accordance with Fig. 4.7.1.5 Photometric SystemThe photometric system shallconsist of a light source and photodetector, oriented verticallyto reduce measurement variations resulting from strat
45、ificationof the smoke generated by materials under test. The systemshall be as shown in Figs. 5 and 6 and include the following:7.1.5.1 The light source shall be an incandescent lampoperated at a fixed voltage in a circuit powered by a constant-voltage transformer. The light source shall be mounted
46、in asealed and light-tight box. This box shall contain the necessaryoptics to provide a collimated light beam passing verticallythrough the chamber. The light source shall be maintained at anoperating voltage required to provide a brightness temperatureof 2200 6 100K.AStainless steel tube GStainless
47、 steel spacersBFront insulating ring HStainless steel reflectors (3)CCeramic tube JCenter insulating diskDHeater/plate 525 W KInsulating spacer ringEStainless steel mounting screw LRear insulating diskFInsulating gasket MSheet metal screw (2)PHeater leads/porcelain beadsFIG. 2 Furnace SectionE662094
48、FIG. 3 Details of Specimen Holder and Pilot BurnerFIG. 4 Furnace SupportE6620957.1.5.2 The photodetector shall be a photomultiplier tube,with an S-4 spectral sensitivity response and a dark current lessthan 109A. A set of nine gelatin compensating filters varyingfrom 0.1 to 0.9 neutral density are m
49、ounted one or more asrequired in the optical measuring system to correct for differ-ences in the luminous sensitivity of the photomultiplier tube.These filters also provide correction for light source or photo-multiplier aging and reduction in light transmission, throughdiscolored or abraded optical windows. An additional criterionfor selection of photomultiplier tubes requires a minimumsensitivity equivalent to that required to give a full scalereading with only the No. 5 compensating filter in the lightpath.Alight-tig
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