ASTM E675-2002(2007) 431 Standard Specification for Interchangeable Taper-Ground Stopcocks And Stoppers《可互换的圆锥接地旋塞阀和栓塞的标准规范》.pdf

1、Designation: E 675 02 (Reapproved 2007)Standard Specification forInterchangeable Taper-Ground Stopcocks And Stoppers1This standard is issued under the fixed designation E 675; the number immediately following the designation indicates the year oforiginal adoption or, in the case of revision, the yea

2、r of last revision. A number in parentheses indicates the year of last reapproval. Asuperscript epsilon (e) indicates an editorial change since the last revision or reapproval.1. Scope1.1 The specification provides standard dimensional re-quirements for obtaining, within practical limits, interchang

3、e-ability in stopcocks and stoppers for ordinary laboratory andindustrial applications. It covers dimensional interchangeabil-ity of the ground surfaces only and does not involve designcharacteristics of the item except where specified.NOTE 1The dimensions pertaining to stopcocks and stoppers wereta

4、ken from the Commercial Standard CS 21 of the U.S. Department ofCommerce.NOTE 2Although glass is the most commonly used material forstopcocks and stoppers, other materials may be used as specified.Stopcocks and stoppers constructed from glass should conform to Speci-fications E 438 and E 671.2. Refe

5、renced Documents2.1 ASTM Standards:2E 438 Specification for Glasses in Laboratory ApparatusE 671 Specification for Maximum Permissible Thermal Re-sidual Stress in Annealed Glass Laboratory ApparatusE 920 Specification for Commercially Packaged LaboratoryApparatusE 921 Specification for Export Packag

6、ed Laboratory Appa-ratusE 1133 Practice for Performance Testing of Packaged Labo-ratory Apparatus for United States Government Procure-mentsE 1157 Specification for Sampling and Testing of ReusableLaboratory Glassware2.2 U.S. Department of Commerce Standard:CS 21 Interchangeable Taper-Ground Joints,

7、 Stopcocks,Stoppers, and Spherical-Ground Joints33. Requirements for Single Straight-Bore Taper-GroundStopcocks3.1 The designations and dimensions for single straight-bore stopcocks shall be as shown in Fig. 1 and Table 1.3.2 TaperAll straight-bore stopcocks shall have a taper of1 6 0.006 mm of diam

8、eter per 10 mm of length (1 to 10).3.3 Master GagesDimensions and tolerances for mastergages shall be as shown in Fig. 2 and Fig. 3, and Table 2 andTable 3. Overall diameter of ring gage shall be approximatelytwice the diameter of the bore at the reference line in thewindow, but not less than 25 mm.

9、3.3.1 Plug GagePlug shall have two short axial lines1806 0.5 apart intersecting the reference line for checkinglocation of bore hole. In addition to the two axial lines 180apart intersecting the reference line on the 4 and 6-mm plugs,two additional axial lines shall be provided on each of theseplugs

10、 for checking the location of the bore hole of T-bore and120-deg bore stopcocks. These two additional axial lines shallbe placed 90 and 120 (6 0.5) from one of the first two axiallines.3.3.2 Ring GageThe central milled recess, or window,shall be placed approximately midway between the ends of therin

11、g gage. Width of recess measured parallel with the axis shallbe approximately one fourth of the length of the ring, and thewidth of the opening at the inner surface of ring, measuredperpendicular to the axis, shall not exceed one fourth of thelength of the ring. Reference line in recess shall be pla

12、cedapproximately midway between ends of ring gage.3.3.3 Fit of Product in Working Gages The product (bothinner and outer members) shall fit the corresponding workinggages so that the centerline through the bore corresponds withthe reference line on the gage within 6 0.3 mm for 1, 112 , and2-mm bores

13、;6 0.5 mm for 3 and 4-mm bores; and 6 1.0 mmfor 5-mm and larger bores.1This specification is under the jurisdiction of ASTM Committee E41 onLaboratory Apparatus and is the direct responsibility of Subcommittee E41.01 onApparatus.Current edition approved Nov. 1, 2007. Published January 2008. Original

14、lyapproved in 1979. Last previous edition approved in 2002 as E 675 02.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe AST

15、M website.3Discontinued 1979U.S. Department of Commerce, Washington, DC 20234.1Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.4. Requirements for Single Oblique-Bore Stopcocks4.1 Design, dimensions, and tolerances for 1, 112 ,2,3,and

16、4-mm oblique-bore stopcocks shall be as shown in Fig. 4 andTable 4.4.2 TaperAll single oblique-bore stopcocks shall have ataper of 1 6 0.006 mm of diameter per 10 mm of length (1 to10).4.3 Master GagesThe dimensions and tolerances for mas-ter gages shall be as shown in Fig. 5 and Fig. 6 and Table 5

17、andTable 6. The overall diameter of the ring gage shall beapproximately twice the diameter of the bore at its midpoint,but not less than 25 mm.4.3.1 Plug GageThe upper circumferential reference lineshall be the gaging point. Each reference line shall have a shortaxial line intersecting it, the two a

18、xial lines being on oppositesides of the plug and in the same plane running through the axis(180 6 0.5 apart) for checking location of bore holes.4.3.2 Ring GageThe width of the milled recesses, orwindows, measured parallel with the axis shall be approxi-mately one fourth of the length of the ring,

19、and the width of theopening at the inner surface of ring, measured perpendicular tothe axis, shall not exceed one fourth of the length of the ring.The recesses shall be so placed that the reference lines fallapproximately midway in the recess.4.3.3 Fit of Product in Working Gages The product (bothin

20、ner and outer members) shall fit the corresponding workinggages so that the centerlines through the openings correspondwith the reference lines on the gages within 6 0.3 mm for 1,112 , and 2-mm bores, and 6 0.5 mm for 3 and 4-mm bores.5. Requirements for Double Oblique-Bore (Three-Way)Stopcocks5.1 D

21、esign, dimensions, and tolerances for 1, 112 ,2,3,and4-mm, three-way bore stopcocks shall be as shown in Fig. 7and Table 7.FIG. 1 StopcockTABLE 1 Single Straight-Bore StopcocksStopcockDesignationDiameter of Plugat Center-Lineof Bore, mmDLength ofShell, 60.5mmEDiameter ofBore Hole inPlug, mmF1-MA720

22、1112 3112 12 30 11221 0317 4 341 4520 562 4 6825 52 810 35 56 10AMicro size.FIG. 2 Master Plug Gage for Single Straight-Bore StopcocksFIG. 3 Master Ring Gage for Single Straight-Bore StopcocksE 675 02 (2007)25.2 TaperAll double oblique-bore stopcocks shall have ataper of 1 6 0.006 mm of diameter per

23、 10 mm of length (1 to10).5.3 Master GagesDimensions and tolerances for mastergages shall be as shown in Fig. 8 and Fig. 9 and Table 8 andTable 9. The overall diameter of the ring gage shall beapproximately twice the diameter of the bore at the referenceline in the central window.5.3.1 Plug GageThe

24、central circumferential referenceline shall be the gaging point. A short axial reference line shallintersect each of the circumferential reference lines. The axialline intersecting the central circumferential reference line shallbe on the opposite side of the plug from the other two axiallines. All

25、three axial lines shall be in the same plane runningthrough the axis (180 6 0.5) to check the location of the boreholes.5.3.2 Ring GageThe width of the milled recesses, orwindows, measured parallel with the axis shall be approxi-mately one fourth of the length of the ring, and the width of theopenin

26、g at the inner surface of ring, measured perpendicular tothe axis, shall not exceed one fourth of the length of the ring.The recesses shall be so placed that the reference lines fallapproximately midway in the recesses.5.3.3 Fit of Product in Working Gages The product (bothinner and outer members) s

27、hall fit the corresponding workinggages so that the centerlines through the openings correspondwith the reference lines on the gage within 6 0.3 mm for 1, 112, and 2-mm bores, and 6 0.5 mm for 3 and 4-mm bores.6. Requirements for T-Bore and 120-deg Bore Stopcocks6.1 These stopcocks are designated by

28、 the nominal boresize. With the exception of the bore sizes, the dimensions andtolerances for 1, 112 , and 2-mm T-bore and 120-deg borestopcocks shall be the same as for the 4-mm single straight-bore stopcocks. Dimensions and tolerances for 3 and 4-mmT-bore and 120-deg bore stopcocks shall be the sa

29、me as for the6-mm single-bore stopcocks. (See Table 1.)6.2 TaperAll T-bore and 120-deg bore stopcocks shallhave a taper of 1 6 0.006 mm of diameter per 10 mm of length(1 to 10).6.3 Master Gages:6.3.1 Plug GageThe 4-mm single straight-bore gage shallbe used for 1, 112 , and 2-mm T-bore and 120-deg bo

30、re, and6-mm single straight-bore gage for 3 and 4-mm T-bore and120-deg bore stopcocks.6.3.2 Ring GageTo check diameter at the centerline of thebore, the 4-mm single straight-bore ring gage shall be used forthe 1, 112 , and 2-mm sizes; and the 6-mm single straight-borering gage for the 3 and 4-mm siz

31、es of T-bore and 120-deg borestopcocks.6.3.3 Ring Gage for Locating Position of Bores for T-Boreand 120-deg BoreThe length of the ring gage shall be 25 61.0 mm for all sizes. The outside diameter of the rings shall beapproximately twice the diameter at the centerline of the bore.The inside diameter

32、at the large end of the tapered portion shallbe equal to the diameter at the centerline of the bore of the plug(product) 60.1 mm. Four reference lines approximately 0.1mm wide shall be provided on the upper face of the gage atright angles to the vertical axis. Two lines shall be 180 6 0.5apart, and

33、the other two lines shall be 90 6 0.5 and 120 6 0.5from one of the first two lines.7. Requirements for Taper-Ground Flask Stoppers7.1 The designations and dimensions for taper-ground flaskstoppers shall be as shown in Fig. 10 and Table 10.7.2 TaperAll taper-ground flask stoppers shall have ataper of

34、 1 6 0.006 mm of diameter per 10 mm of length (1 to10).7.3 Master GagesDimensions and tolerances for mastergages shall be as shown in Fig. 11 and Fig. 12 and Table 11 andTable 12. The overall diameter of the ring gage shall beapproximately twice the diameter of the small end of the bore,but not less

35、 than 25 mm.7.3.1 Fit of Product in Working Gages The large end ofstopper shall come flush with large end of ring gage within60.5 mm along the axis for stopper Nos. 8 to 19, inclusive; andwithin6 1.0 mm along the axis for stopper Nos. 22 and 38,inclusive.7.3.2 The plug gage shall enter the flask so

36、that gaging pointon plug shall be at least 0.5 mm and not over 1.5 mm above theextreme top surface of the flask for stopper Nos. 8 to 19,inclusive; and at least 1.0 mm and not over 3.0 mm for stopperNos. 22 to 38, inclusive.8. Requirements for Taper-Ground Bottle Stoppers8.1 The designations and dim

37、ensions of taper-ground re-agent bottle stoppers shall be as shown in Fig. 13 and Table 13.TABLE 2 Master Plug Gages for Single Straight-Bore StopcocksStopcockDesignationLength of TaperedPortion +2.0 mm,0 mmEEDiameter atGaging Point60.003 mmDDDistance fromLarge End ofTapered Portionto GagingPoint, m

38、mNN1-MA32 7 20142 12 5112 42 12 2524 2352 17 3045556 20 265 3864 5 610 68 35 38AMicro size.TABLE 3 Master Ring Gages for Single Straight-Bore StopcocksStopcockDesignationLength ofRing, +0.2mm, 0 mmEEInside Diameterat Gaging Point,60.003 mmDDDistance fromTop to GagingPoint, mmNN1-MA20 7 101301215112

39、30 12 15340172045 4202264852252610 56 35 28AMicro size.E 675 02 (2007)38.2 TaperAll taper-ground reagent bottle stoppers shallhave a taper of 1 6 0.006 mm of diameter per 10 mm of length.8.3 Master GagesDimensions and tolerances for mastergages shall be as shown in Fig. 14 and Fig. 15 and Table 14 a

40、ndTable 15. The overall diameter of the ring gage shall beapproximately twice the diameter of the small end of the bore,but not less than 25 mm.8.3.1 Fit of Product in Working Gages The large end ofthe stopper shall come flush with large end of ring gage withinFIG. 4 Single Oblique-Bore StopcockTABL

41、E 4 Single Oblique-Bore StopcockStopcockDesignationDiameter of Plug atGaging Point, mmDLength of Shell,60.5 mmEDiameter of Borein Plug, mmFDistance from Large Endof Shell to GagingPoint, 60.5 mmNDistance betweenBore Holes,PA1 12.60 40 1 14.0 12112 12.60 40 112 14.0 122 12.60 40 2 14.0 123 17.35 50 3

42、 16.5 174 17.35 50 4 16.5 17ASee 3.3.3.FIG. 5 Master Plug Gage for Single Oblique-Bore StopcocksFIG. 6 Master Ring Gage for Single Oblique-Bore StopcocksE 675 02 (2007)4TABLE 5 Master Plug Gages for Single Oblique-Bore StopcocksStopcock DesignationLength ofTapered Portion,+2.0 mm, 0 mmEEDiameter at

43、GagingPoint, 60.003 mmDDDistance from Large End ofTapered Portion to GagingPoint +1.5 mm, 0 mmNNDistance from Gaging Pointto Lower ReferenceLine 60.03 mmPP1 52 12.60 24.5 12112 52 12.60 24.5 122 52 12.60 24.5 123 62 17.35 27.0 174 62 17.35 27.0 17TABLE 6 Master Ring Gages for Single Oblique-Bore Sto

44、pcocksStopcock DesignationLength of Ring, +0.2mm, 0 mmEEInside Diameter at GagingPoint, 60.003 mmDDDistance from Top to GagingPoint (Approximate)NNDistance from GagingPointto Lower Reference Point,60.03 mmPP1 40 12.60 14.0 12112 40 12.60 14.0 122 40 12.60 14.0 123 50 17.35 16.5 174 50 17.35 16.5 17F

45、IG. 7 Double Oblique-Bore StopcockTABLE 7 Double Oblique-Bore StopcockStopcockDesignationDiameter ofPlug atGaging Point, mmDLength ofShell, 60.5 mmEDiameter ofBore in Plug, mmFDistance fromLarge End ofShell to Gaging point,60.5 mmNDistance fromGaging Point toCenterline of Bore NearLarge End, mmRADis

46、tance fromGaging Point toCenterline ofBore Near Small EndSA1 14.5 50 1 25 12.5 11.5112 14.5 50 112 25 12.5 11.52 14.5 50 2 25 12.5 11.53 16.2 56 3 28 14.0 12.94 16.2 56 4 28 14.0 12.9ASee 3.3.3.E 675 02 (2007)56 0.5 mm along the axis for stopper Nos. 14 and 19, andwithin6 1.0 mm along the axis for s

47、topper Nos. 24 to 45,inclusive.8.3.2 The plug gage shall enter bottle so that gaging point onplug shall be at least 0.5 mm and not over 1.5 mm above theextreme top surface of the bottle for stopper Nos. 14 and 19;and at least 1.0 mm and not over 3.0 mm for stopper Nos. 24to 45, inclusive.9. Sampling

48、 and Testing9.1 For sampling and testing refer to Specification E 1157.10. Product Marking10.1 Interchangeable taper-ground stopcocks, and stoppersconforming to this specification may be marked on bothmembers with (), indicating standard taper, the size designa-tion, and the trade-mark of the manufa

49、cturer or distributor. Thissymbol is the manufacturers assurance to purchasers that theitem identified by the symbol is a standard interchangeable sizeand type, and is manufactured within the tolerances permittedby this specification. It shall not be used on stopcocks, orstoppers, nor in advertising descriptions of stopcocks, orstoppers of any size or type other than those described in thisspecification.11. Packaging11.1 For packaging select from Specifications E 920, E 921,or Practices E 1133.12. Keywords12.1 ground;