ASTM F660-1983(2013) Standard Practice for Comparing Particle Size in the Use of Alternative Types of Particle Counters《替换型粒子计数器使用过程中粒度比较的标准实施规范》.pdf

1、Designation: F660 83 (Reapproved 2013)Standard Practice forComparing Particle Size in the Use of Alternative Types ofParticle Counters1This standard is issued under the fixed designation F660; the number immediately following the designation indicates the year of originaladoption or, in the case of

2、revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A superscriptepsilon () indicates an editorial change since the last revision or reapproval.1. Scope1.1 This practice provides a procedure for comparing thesizes of nonspherical particles in a test sa

3、mple determined withdifferent types of automatic particle counters, which operate ondifferent measuring principles.1.2 A scale factor is obtained by which, in the examinationof a given powder, the size scale of one instrument may bemultiplied to agree with the size scale of another.1.3 The practice

4、considers rigid particles, free of fibers, ofthe kind used in studies of filtration, such as: commerciallyavailable test standards of quartz or alumina, or fly ash, orsome powdered chemical reagent, such as iron oxide orcalcium sulfate.1.4 Three kinds of automatic particle counters are consid-ered:1

5、.4.1 Image analyzers, which view stationary particles un-der the microscope and, in this practice, measure the longestend-to-end distance of an individual particle.1.4.2 Optical counters, which measure the area of a shadowcast by a particle as it passes by a window; and1.4.3 Electrical resistance co

6、unters, which measure the vol-ume of a particle as it passes through an orifice in anelectrically conductive liquid.1.5 This practice also considers the use of instruments thatprovide sedimentation analyses, which is to say providemeasures of the particle mass distribution as a function ofStokes dia

7、meter. The practice provides a way to convert massdistribution into number distribution so that the meaning ofStokes diameter can be related to the diameter measured by theinstruments in 1.4.1.6 This standard does not purport to address all of thesafety concerns, if any, associated with its use. It

8、is theresponsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulatory limitations prior to use.2. Referenced Documents2.1 ASTM Standards:2F661 Practice for Particle Count and Size Distribution Mea-surement in Batch Samp

9、les for Filter Evaluation Using anOptical Particle Counter (Discontinued 2000) (Withdrawn2000)3F662 Test Method for Measurement of Particle Count andSize Distribution in Batch Samples for Filter EvaluationUsing an Electrical Resistance Particle Counter (Discon-tinued 2002) (Withdrawn 2002)3F796 Prac

10、tice for Determining The Performance of a FilterMedium Employing a Single-Pass, Constant-Pressure,Liquid Test (Withdrawn 2002)33. Summary of Practice3.1 After calibrating an automatic particle counter withstandard spherical particles, such as latex beads, the instrumentis presented with a known weig

11、ht of filtration-test particlesfrom which is obtained the data: cumulative number ofparticles, N, as a function of particle diameter, d; and a plotof these data is made on log-log paper.3.2 The plot from the results of one kind of instrument isplaced over the plot from another and one plot is moved

12、alongthe particle-diameter axis until the two separate curves coin-cide. (If the two separate curves cannot be made to coincide,then this practice cannot be used.)3.3 The magnitude of the shift from one diameter scale tothe other provides the scale-conversion factor.3.4 Any of the three particle cou

13、nters in 1.4 can provide theframe-of-reference measurement of particle diameter.3.5 An alternative reference is the Stokes diameter, asmentioned in 1.5.4. Significance and Use4.1 This practice supports test methods designed to evaluatethe performance of fluid-filter media, for example, Practice1This

14、 practice is under the jurisdiction of ASTM Committee D19 on Water andis the direct responsibility of Subcommittee D19.07 on Sediments, Geomorphology,and Open-Channel Flow.Current edition approved Jan. 1, 2013. Published January 2013. Originallyapproved in 1983. Last previous edition approved in 200

15、7 as F660 83 (2007).DOI: 10.1520/F0660-83R13.2For referenced ASTM standards, visit the ASTM website, www.astm.org, orcontact ASTM Customer Service at serviceastm.org. For Annual Book of ASTMStandards volume information, refer to the standards Document Summary page onthe ASTM website.3The last approv

16、ed version of this historical standard is referenced onwww.astm.org.Copyright ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States1F796 wherein particle size distributions are addressed and atthe same time this practice provides a means to compare s

17、izemeasurements obtained from several different types of instru-ments.4.2 The factor for converting one kind of diameter scale toanother is only valid for the specific test particles studied.5. Apparatus5.1 Automatic Particle Counters :5.1.1 Any, or all, of the three types are employed:5.1.1.1 The I

18、mage AnalyzerThis instrument counts par-ticles by size as those particles lie on a microscope slide. In thispractice, size means the longest end-to-end distance. Thisdiameter, in the examples to follow, is designated de.5.1.1.2 The Optical CounterThis instrument measures thearea of a shadow cast by

19、a particle as it passes a window. Fromthat area the instrument reports the diameter of a circle of equalarea. This diameter is designated do. See Practice F661.5.1.1.3 The Electrical Resistance Counter This instru-ment measures the volume of an individual particle. From thatvolume the instrument rep

20、orts the diameter of a sphere of equalvolume. This diameter is designated dv. See Method F662.5.2 Sedimentation InstrumentsThese instruments providea measure of the mass distribution of particles (as opposed tothe number distributions determined in 5.1). This diameter, theStokes diameter, is designa

21、ted ds.6. Procedure6.1 Calibrate each particle counter with standard, sphericalparticles, following the instructions of the manufacturer of thecounter.6.2 Present a known mass of particles to the counter. That is,with the image analyzer present a known mass of particles toa field of view; and, with

22、the other counters present a liquidsuspension with a known mass concentration of particles.6.3 In counting particles at the small-diameter end of thespectrum, present at least three different, relatively small,masses of particles. In counting particles at the large-diameterend, present at least thre

23、e different, relatively large, masses.6.4 After obtaining the counts (6.3) correct them all toreflect the count of a common mass. For example, correct allcounts to show particle distribution for each milligram ofsolids. Plot the counts in the manner of Fig. 1.6.5 From these plots select the true num

24、ber distribution;show it as a solid line as shown in Fig. 1.NOTE 1It is important to deduce the optimum raw count to look forduring the examination of a liquid where the mass concentration ofparticles is not known. The manufacturers of each counter specify themaximum count per unit volume of liquid

25、that is meaningful. If the countexceeds this maximum limit, dilute the sample with clean liquid. (Cleanliquid means that where the particle count is less than 10 %, or preferablyless than 1 %, of the sample count.) Alternatively, if the sample shows acount so low that a meaningful count of large par

26、ticles is not obtained,examine a larger sample.6.6 Compare the Fig. 1 type plot obtained with one particlecounter to the plot(s) made from another counter (or othercounters). Follow the example of Fig. 2.6.7 Now, choose one counter to provide the frame-of-reference measure of diameter. Relate other

27、diameter scales toN = cumulative number of particles per unit mass of powderd = particle diameter (see 5.1)The solid line represents the “real” count. The broken lines represent failuresto obtain correct counts because of either presenting too many particles to thecounter, a, or of presenting too fe

28、w, b.FIG. 1 Example of Particle CountsN = cumulative number of particles per unit mass of powderd = particle diameter, m (see 5.1)FIG. 2 Example of a Blend of Particle Counts Obtained with Dif-ferent CountersF660 83 (2013)2that “standard.” For example, if from the present example ofFig. 2, the desca

29、le is the standard, then,de5 1.30 do(1)andde5 1.72 dv(2)ordo5 0.769 de(3)anddv5 0.581 de(4)6.8 In those cases where measurements of particle-sizedistribution are based on mass (rather than number), in Fig. 3,convert the Fig. 3 type data to Fig. 1 type data by the followingtechnique:6.8.1 Divide the

30、diameter scale of Fig. 3 into portions sothat there are ten equally wide portions per decade. That is, oneportion will be in the diameter scale of 1.00 to 1.26 m, thenext will be in the range 1.26 to 1.59 m, etc. That is to say,follow the example in Method F662, where the factor of 1.26is, in fact,

31、the cube root of 2, that is, 1.25992.6.8.2 Replot the Fig. 3 data to obtain the W curve and theW bar chart of Fig. 4.6.8.3 Now, since the diameter scale has been divided intoportions where for an equal weight of particles in two adjacentdiameter ranges the smaller range will contain twice as manypar

32、ticles, employ this 2.0 factor to convert the W bar chartinto the N bar chart; then subsequently draw the N curve.6.9 Superimpose the N curve of Fig. 4 over the curves ofFig. 2, to obtain, in the present example, Fig. 5. See, from Fig.5, thatde5 1.60 ds(5)ords5 0.625 de(6)7. Precision7.1 The example

33、s presented here to explain this practice areresults of actual work where different investigators, usingdifferent instruments, examined a common lot of quartz testdust.47.2 Fig. 6 shows the agreement achieved among threeinvestigators, each of whom employed an electrical resistancecounter; Fig. 7 sho

34、ws the agreement among three investigatorswho employed optical counters.7.3 While the factors reported in 6.7 and 6.9 (for convertingone diameter scale to another) are shown as three significantfigures, such implied precision is not justified by the presentdata.7.4 From the blend of data in Fig. 5 i

35、t is obvious that suchconversion factors are valid only over a finite range of particlediameters, depending on which instruments are involved.8. Keywords8.1 particle counters; Strokes diameter4Johnston, P. R., and Swanson, R. R., “A Correlation Between the Results ofDifferent Instruments Used to Det

36、ermine the Particle-Size Distribution in AC FineTest Dust,” Powder Technology, Vol 32, No. 1, pp. 119124.W = cumulative mass of particles per unit mass of powderds= Stokes diameter of a particle, mFIG. 3 Example of a Particle-Size Distribution Obtained by Sedi-mentation AnalysisW = cumulative mass o

37、f particles per unit mass of powder, from Fig. 3W = mass fraction of particles in each diameter range (deduced from W)N = relative number of particles in each diameter range (deduced from W)N = cumulative number of particlesds= Stokes diameter of particles, mFIG. 4 Example of Converting a Weight Dis

38、tribution into a Num-ber DistributionF660 83 (2013)3N = cumulative number of particles per unit mass of test powderds= Stokes diameter, mdv= diameter of sphere of equal volumede= longest end-to-end distancedo= diameter of circle of equal areaFIG. 5 Blend of Fig. 2 and the N Curve of Fig. 4N = cumula

39、tive number of particles per millilitre in a slurry containing 5 mg/Ldv= particle diameter, m, when instrument is calibrated with standard latex beadsFIG. 6 Particle-Size Distribution in Lot 121 of AC Fine Test Dustas Determined by Three Separate Investigators, in DifferentLaboratories, Each Employi

40、ng an Electrical Resistance CounterF660 83 (2013)4ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentionedin this standard. Users of this standard are expressly advised that determination of the validity of any such patent right

41、s, and the riskof infringement of such rights, are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised, either reapproved or withdrawn. Your comments are invited either for r

42、evision of this standard or for additional standardsand should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of theresponsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing y

43、ou shouldmake your views known to the ASTM Committee on Standards, at the address shown below.This standard is copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959,United States. Individual reprints (single or multiple copies) of this standard may b

44、e obtained by contacting ASTM at the aboveaddress or at 610-832-9585 (phone), 610-832-9555 (fax), or serviceastm.org (e-mail); or through the ASTM website(www.astm.org). Permission rights to photocopy the standard may also be secured from the ASTM website (www.astm.org/COPYRIGHT/).N = cumulative num

45、ber of particles per millilitre in a slurry containing 5 mg/Ldo= particle diameter, m, when instrument is calibrated with standard latex beadsFIG. 7 Particle-Size Distribution in Lot 121 of AC Fine Test Dustas Determined by Three Separate Investigators, in DifferentLaboratories, Each Employing an Optical Particle CounterF660 83 (2013)5