BS EN 1482-3-2016 Fertilizers and liming materials Sampling and sample preparation Sampling of static heaps《肥料和石灰质材料 取样和样品制备 静态料堆的取样》.pdf

1、Fertilizers and liming materials Sampling and samplepreparationPart 3: Sampling of static heapsBS EN 1482-3:2016Incorporating corrigendum February 2017BSI Standards PublicationBS EN 1482-3:2016 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN 1482-3:2016.The UK p

2、articipation in its preparation was entrusted to Technical Committee CII/37, Fertilisers and related chemicals.A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Us

3、ers are responsible for its correct application. The British Standards Institution 2017. Published by BSI Standards Limited 2017ISBN 978 0 580 97505 9ICS 65.080Compliance with a British Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of

4、the Standards Policy and Strategy Committee on 31 August 2016.Amendments/corrigenda issued since publicationDate Text affected28 February 2017 Implementation of CEN/CENELEC Correction Notice 17 August 2016: Figure 3 replaced BS EN 1482-3:2016g3g3g3g8g24g21g18g19g8g4g17g3g22g23g4g17g7g4g21g7g3g17g18g

5、21g16g8g3g8g24g21g18g19g50g8g17g17g8g3g8g24g21g18g19g34g12g22g6g11g8g3g17g18g21g16g3EN 1482-3 g3 g3g3 g4g151g137g151g149g150g3g884g882g883g888g3g12g6g22g3g888g887g484g882g890g882g3g8g144g137g142g139g149g138g3g25g135g148g149g139g145g144g3g3g9g135g148g150g139g142g139g156g135g148g149g3g131g144g134g3g14

6、2g139g143g139g144g137g3g143g131g150g135g148g139g131g142g149g3g486g3g22g131g143g146g142g139g144g137g3g131g144g134g3g149g131g143g146g142g135g3g146g148g135g146g131g148g131g150g139g145g144g3g486g3g19g131g148g150g3g885g483g3g22g131g143g146g142g139g144g137g3g145g136g3g149g150g131g150g139g133g3g138g135g131

7、g146g149g3g8g144g137g148g131g139g149g3g135g150g3g131g143g135g144g134g135g143g135g144g150g149g3g143g139g144g177g148g131g151g154g3g132g131g149g139g147g151g135g149g3g486g3g50g133g138g131g144g150g139g142g142g145g144g144g131g137g135g3g135g150g3g146g148g177g146g131g148g131g150g139g145g144g3g134g135g3g142g

8、821g177g133g138g131g144g150g139g142g142g145g144g3g486g3g19g131g148g150g139g135g3g885g3g483g3g50g133g138g131g144g150g139g142g142g145g144g144g131g137g135g3g134g135g149g3g150g131g149g3g149g150g131g150g139g147g151g135g149g3g3 g7g242g144g137g135g143g139g150g150g135g142g3g151g144g134g3g14g131g142g141g134g

9、242g144g137g135g148g3g486g3g19g148g145g132g135g144g131g138g143g135g3g151g144g134g3g19g148g145g132g135g144g152g145g148g132g135g148g135g139g150g151g144g137g3g486g3g23g135g139g142g3g885g483g3g19g148g145g132g135g144g131g138g143g135g3g131g151g149g3g149g150g131g150g139g149g133g138g135g144g3g11g131g151g136

10、g153g135g148g141g135g144g3g23g138g139g149g3g8g151g148g145g146g135g131g144g3g22g150g131g144g134g131g148g134g3g153g131g149g3g131g146g146g148g145g152g135g134g3g132g155g3g6g8g17g3g145g144g3g883g884g3g13g151g144g135g3g884g882g883g888g484g3g3g3g6g8g17g3g143g135g143g132g135g148g149g3g131g148g135g3g132g145g

11、151g144g134g3g150g145g3g133g145g143g146g142g155g3g153g139g150g138g3g150g138g135g3g6g8g17g512g6g8g17g8g15g8g6g3g12g144g150g135g148g144g131g142g3g21g135g137g151g142g131g150g139g145g144g149g3g153g138g139g133g138g3g149g150g139g146g151g142g131g150g135g3g150g138g135g3g133g145g144g134g139g150g139g145g144g1

12、49g3g136g145g148g3g137g139g152g139g144g137g3g150g138g139g149g3g8g151g148g145g146g135g131g144g3g22g150g131g144g134g131g148g134g3g150g138g135g3g149g150g131g150g151g149g3g145g136g3g131g3g144g131g150g139g145g144g131g142g3g149g150g131g144g134g131g148g134g3g153g139g150g138g145g151g150g3g131g144g155g3g131g

13、142g150g135g148g131g150g139g145g144g484g3g24g146g486g150g145g486g134g131g150g135g3g142g139g149g150g149g3g131g144g134g3g132g139g132g142g139g145g137g148g131g146g138g139g133g131g142g3g148g135g136g135g148g135g144g133g135g149g3g133g145g144g133g135g148g144g139g144g137g3g149g151g133g138g3g144g131g150g139g1

14、45g144g131g142g3g149g150g131g144g134g131g148g134g149g3g143g131g155g3g132g135g3g145g132g150g131g139g144g135g134g3g145g144g3g131g146g146g142g139g133g131g150g139g145g144g3g150g145g3g150g138g135g3g6g8g17g486g6g8g17g8g15g8g6g3g16g131g144g131g137g135g143g135g144g150g3g6g135g144g150g148g135g3g145g148g3g150

15、g145g3g131g144g155g3g6g8g17g3g143g135g143g132g135g148g484g3g3g23g138g139g149g3g8g151g148g145g146g135g131g144g3g22g150g131g144g134g131g148g134g3g135g154g139g149g150g149g3g139g144g3g150g138g148g135g135g3g145g136g136g139g133g139g131g142g3g152g135g148g149g139g145g144g149g3g523g8g144g137g142g139g149g138g

16、481g3g9g148g135g144g133g138g481g3g10g135g148g143g131g144g524g484g3g4g3g152g135g148g149g139g145g144g3g139g144g3g131g144g155g3g145g150g138g135g148g3g142g131g144g137g151g131g137g135g3g143g131g134g135g3g132g155g3g150g148g131g144g149g142g131g150g139g145g144g3g151g144g134g135g148g3g150g138g135g3g148g135g1

17、49g146g145g144g149g139g132g139g142g139g150g155g3g145g136g3g131g3g6g8g17g3g143g135g143g132g135g148g3g139g144g150g145g3g139g150g149g3g145g153g144g3g142g131g144g137g151g131g137g135g3g131g144g134g3g144g145g150g139g136g139g135g134g3g150g145g3g150g138g135g3g6g8g17g486g6g8g17g8g15g8g6g3g16g131g144g131g137g

18、135g143g135g144g150g3g6g135g144g150g148g135g3g138g131g149g3g150g138g135g3g149g131g143g135g3g149g150g131g150g151g149g3g131g149g3g150g138g135g3g145g136g136g139g133g139g131g142g3g152g135g148g149g139g145g144g149g484g3g3g6g8g17g3g143g135g143g132g135g148g149g3g131g148g135g3g150g138g135g3g144g131g150g139g1

19、45g144g131g142g3g149g150g131g144g134g131g148g134g149g3g132g145g134g139g135g149g3g145g136g3g4g151g149g150g148g139g131g481g3g5g135g142g137g139g151g143g481g3g5g151g142g137g131g148g139g131g481g3g6g148g145g131g150g139g131g481g3g6g155g146g148g151g149g481g3g6g156g135g133g138g3g21g135g146g151g132g142g139g13

20、3g481g3g7g135g144g143g131g148g141g481g3g8g149g150g145g144g139g131g481g3g9g139g144g142g131g144g134g481g3g9g145g148g143g135g148g3g28g151g137g145g149g142g131g152g3g21g135g146g151g132g142g139g133g3g145g136g3g16g131g133g135g134g145g144g139g131g481g3g9g148g131g144g133g135g481g3g10g135g148g143g131g144g155g

21、481g3g10g148g135g135g133g135g481g3g11g151g144g137g131g148g155g481g3g12g133g135g142g131g144g134g481g3g12g148g135g142g131g144g134g481g3g12g150g131g142g155g481g3g15g131g150g152g139g131g481g3g15g139g150g138g151g131g144g139g131g481g3g15g151g154g135g143g132g145g151g148g137g481g3g16g131g142g150g131g481g3g1

22、7g135g150g138g135g148g142g131g144g134g149g481g3g17g145g148g153g131g155g481g3g19g145g142g131g144g134g481g3g19g145g148g150g151g137g131g142g481g3g21g145g143g131g144g139g131g481g3g22g142g145g152g131g141g139g131g481g3g22g142g145g152g135g144g139g131g481g3g22g146g131g139g144g481g3g22g153g135g134g135g144g48

23、1g3g22g153g139g150g156g135g148g142g131g144g134g481g3g23g151g148g141g135g155g3g131g144g134g3g24g144g139g150g135g134g3g14g139g144g137g134g145g143g484g3g3g3g3g3g8g24g21g18g19g8g4g17g3g6g18g16g16g12g23g23g8g8g3g9g18g21g3g22g23g4g17g7g4g21g7g12g29g4g23g12g18g17g3g6g18g16g12g23g50g3g8g24g21g18g19g50g8g17g

24、3g7g8g3g17g18g21g16g4g15g12g22g4g23g12g18g17g3g8g24g21g18g19g34g12g22g6g11g8g22g3g14g18g16g12g23g8g8g3g9g111g21g3g17g18g21g16g24g17g10g3g3g3g3CEN-CENELECg3Management Centre: Avenue Marnix 17, B-1000 Brussels g825g3g884g882g883g888g3g6g8g17g3 g4g142g142g3g148g139g137g138g150g149g3g145g136g3g135g154g1

25、46g142g145g139g150g131g150g139g145g144g3g139g144g3g131g144g155g3g136g145g148g143g3g131g144g134g3g132g155g3g131g144g155g3g143g135g131g144g149g3g148g135g149g135g148g152g135g134g3g153g145g148g142g134g153g139g134g135g3g136g145g148g3g6g8g17g3g144g131g150g139g145g144g131g142g3g16g135g143g132g135g148g149g4

26、84g3g21g135g136g484g3g17g145g484g3g8g17g3g883g886g890g884g486g885g483g884g882g883g888g3g8BS EN 1482-3:2016EN 1482-3:2016 (E) 2 Contents Page European foreword . 3 Introduction 4 1 Scope 5 2 Normative references 5 3 Terms and definitions . 5 4 Sampling plans and quantitative data . 5 4.1 General 5 4.

27、2 Characterization of the lot to be sampled 6 4.3 Sampling plan . 6 4.3.1 General 6 4.3.2 Elements of the sampling plan . 6 4.4 Determination of the volume/mass of the lot. 8 4.5 Determination of sampling units and sampling points . 8 4.5.1 Determination of the number and location of the sampling un

28、its 8 4.5.2 Minimum total number of sampling units . 8 4.5.3 Determination of sampling units from which incremental samples shall be taken . 8 4.5.4 Determination of the minimum number of sampling points from which sub-samples are to be taken 8 4.6 Quantitative data . 8 4.6.1 Determination of the mi

29、nimum mass of increments . 8 4.6.2 Mass of increments . 9 4.6.3 Aggregate/reduced and final samples . 9 5 Incremental sampling methods . 9 5.1 General 9 5.2 Sampling apparatus 9 5.3 Procedure 11 5.4 Aggregate and reduced samples . 12 6 Final samples . 12 6.1 Division into final samples . 12 6.2 Prac

30、tical arrangements for final (laboratory) samples . 12 6.2.1 Final sample packaging materials . 12 6.2.2 Dealing with final samples 12 7 Sampling report 12 Annex A (informative) Determination of mass/volume of a static heap 13 A.1 Volume of a conical heap without edgewise limitation 13 A.2 Volume of

31、 a storage box, partly filled (rectangular base, three flanks closed) . 13 A.3 Determination of the mass . 14 Annex B (informative) Alternative method according to GOST . 15 Bibliography . 16 BS EN 1482-3:2016EN 1482-3:2016 (E) 3 European foreword This document (EN 1482-3:2016) has been prepared by

32、Technical Committee CEN/TC 260 “Fertilizers and liming materials”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2017, and conflicting national

33、standards shall be withdrawn at the latest by February 2017. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights This document has been prepared under a m

34、andate given to CEN by the European Commission and the European Free Trade Association. EN 1482 “Fertilizers and liming materials Sampling and sample preparation” consists of three parts: Part 1: Sampling; Part 2: Sample preparation; Part 3: Sampling of static heaps. According to the CEN-CENELEC Int

35、ernal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland,

36、Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. BS EN 1482-3:2016EN 1482-3:2016 (E) 4 Introduction The establishment of European Standards for methods of sampling and

37、analysis is of utmost importance to guarantee a uniform application and control of the European legislation in all Member States. Standardized methods of sampling and analysis are essential elements in guaranteeing a high level of quality and safety of EC fertilizers for the benefit of purchasers. I

38、n order to avoid any improper use of the term “EC fertilizer” Member States are required to check the nutrient content of such fertilizers. To achieve this, representative sampling is essential for reliable analytical results. Competent authorities have limited resources for conformity assessment an

39、d these are most efficiently deployed at the downstream end of the supply chain. The purpose of Regulation (EC) No 2003/2003 1 is to ensure that the fertilizer meets European requirements and complies with the declaration of the required characteristics applied to it when delivered to a purchaser. E

40、N 1482-1:2007 might not fully satisfy the needs of Member States when a large quantity of fertilizer is stored in a static heap that cannot be realistically put into motion. An evaluation was requested to be carried out by CEN to see what, if any, static heaps of fertilizer could be representatively

41、 sampled at affordable costs see (see 3). The fundamental principle of representative sampling is that every particle has an equal chance of being sampled. This principle cannot easily be complied with in the case of bulk static heaps of solid fertilizers as a large proportion of the material cannot

42、 practically be reached by any sampling device. Wherever possible, this fertilizer should be sampled during transfer, during the building up of the heap, during dispatch or where it can practically be moved solely for sampling purposes. However, in some cases, sampling in the way described is not pr

43、acticable. The European Commission asked CEN/TC 260/WG 1 to draft a European Standard in response to mandate M/454, which requires the development of a method of sampling static heaps that could not be sampled according to EN 1482-1:2007. This states that the sampling of static heaps should only be

44、carried out when the product is in motion. In response to the mandate, sampling methods to sample static heaps have been developed and standardized as specified in this document. BS EN 1482-3:2016EN 1482-3:2016 (E) 5 1 Scope This European Standard is applicable to the sampling of mineral fertilizers

45、 and liming materials supplied or ready for supply to third parties, as a lot or in smaller lots, where such supply or readiness for supply is subject to legal requirements. This European Standard specifies plans and methods of sampling of a lot of solid fertilizer or liming material, if sampling in

46、 motion is not possible, to obtain samples from static bulk heaps in order to ascertain compliance with legal requirements, in particular in relation to the accuracy of compulsory or permitted statutory declarations. The methods specified in this document are not applicable to obtain samples for phy

47、sical analysis or for the chemical analysis which may be altered by particle granulometric segregation. This European Standard is applicable to single nutrient fertilizers, to uniform complex fertilizers and to milled or granulated liming materials. The methods described in this document are not sui

48、table for sampling other types of fertilizer, for example blended fertilizers. NOTE The term fertilizer is used throughout the body of this European Standard and includes liming materials unless otherwise indicated. 2 Normative references The following documents, in whole or in part, are normatively

49、 referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1482-1:2007, Fertilizers and liming materials - Sampling and sample preparation - Part 1: Sampling 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 1482-1:2007 and the following apply. 3.1 fertilizer solid inorganic material designated for use as a fertilizer including liming materials 3.2 sampling p