BS EN 590-2013 Automotive fuels Diesel Requirements and test methods《内燃机燃料 柴油 试验方法和要求》.pdf

1、BSI Standards PublicationBS EN 590:2013Automotive fuels Diesel Requirements and testmethodsCopyright European Committee for Standardization Provided by IHS under license with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013 BRITISH STANDARDNational

2、 forewordThis British Standard is the UK implementation of EN 590:2013. Itsupersedes BS EN 590:2009+A1:2010 which is withdrawn.The UK participation in its preparation was entrusted to TechnicalCommittee PTI/2, Liquid Fuels.A list of organizations represented on this committee can beobtained on reque

3、st to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. The British Standards Institution 2013. Published by BSI StandardsLimited 2013ISBN 978 0 580 75962 8ICS 75.160.20Compliance with a British Sta

4、ndard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and Strategy Committee on 30 September 2013.Amendments issued since publicationDate Text affectedCopyright European Committee for Standardization Provided by IHS under li

5、cense with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 590 September 2013 ICS 75.160.20 Supersedes EN 590:2009+A1:2010English Version Automotive fuels - Diesel - Requirements and test methods

6、 Carburants pour automobiles - Carburants pour moteur diesel (gazole) - Exigences et mthodes dessai Kraftstoffe fr Kraftfahrzeuge - Dieselkraftstoff - Anforderungen und Prfverfahren This European Standard was approved by CEN on 26 July 2013. CEN members are bound to comply with the CEN/CENELEC Inter

7、nal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any

8、CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official ver

9、sions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

10、 Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2013 CEN All rights of exploitation in any

11、form and by any means reserved worldwide for CEN national Members. Ref. No. EN 590:2013: ECopyright European Committee for Standardization Provided by IHS under license with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013EN 590:2013 (E) 2 Contents

12、 Page Foreword 3 1 Scope 4 2 Normative references 4 3 Sampling .6 4 Pump marking 6 5 Requirements and test methods 6 5.1 Dyes and markers 6 5.2 Additives .6 5.2.1 General 6 5.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT) 6 5.3 Fatty acid methyl ester (FAME) 6 5.4 Other (bio-) components .7

13、5.5 Generally applicable requirements and related test methods 7 5.6 Climate dependent requirements and related test methods .9 5.7 Precision and dispute 10 Annex A (normative) Details of inter-laboratory test programme . 11 Bibliography . 12 Copyright European Committee for Standardization Provided

14、 by IHS under license with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013EN 590:2013 (E) 3 Foreword This document (EN 590:2013) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petro

15、leum, synthetic and biological origin”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by March 2014, and conflicting national standards shall be withdrawn a

16、t the latest by March 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 590:2009+A1:2010. This documen

17、t has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association 5.The requirements of the European Fuels Directive 98/70/EC 1, including amendments 2003/17/EC 2, 2009/30/EC 3 and 2011/63/EC 4, have been included. Dates are included with all normati

18、ve test method references in order to comply with the requirements of the European Commission; with the accompanying assurance by CEN/TC 19 that any referenced updated versions will always give similar accuracy and the same or better precision (see 4). Significant technical changes between this Euro

19、pean Standard and the previous edition are: Inclusion of the revised EN 14214 FAME specification. Specific requirements concerning the limitation of use of methylcyclopentadienyl manganese tricarbonyl (MMT) as required by the EC have been incorporated. Addition of the Fuel Ignition Tester (EN 16144)

20、 as an alternate test method to the CFR engine test. Addition of Simulated Distillation by gas chromatography (GC), EN ISO 3924, as an alternate test method to distillation by EN ISO 3405. Introduction of the improved EDXRF determination technique for low sulfur contents, EN ISO 13032, in replacemen

21、t of EN ISO 20847. Annex A is normative and contains the precision data generated on the test methods, which are the result of inter-laboratory testing, carried out by working groups of CEN/TC 19. Many of the test methods included in this standard were the subject of inter-laboratory testing to dete

22、rmine the applicability of the method and its precision in relation to blends of automotive diesel fuel containing 10 % (V/V) or higher of different sources of fatty acid methyl esters (FAME). According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following co

23、untries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

24、Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Copyright European Committee for Standardization Provided by IHS under license with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013EN 590:201

25、3 (E) 4 1 Scope This European Standard specifies requirements and test methods for marketed and delivered automotive diesel fuel. It is applicable to automotive diesel fuel for use in diesel engine vehicles designed to run on automotive diesel fuel containing up to 7,0 %(V/V) Fatty Acid Methyl Ester

26、. NOTE For the purposes of this European Standard, the terms “% (m/m)” and “% (V/V)” are used to represent respectively the mass fraction and the volume fraction. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable fo

27、r its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 116:19971), Diesel and domestic heating fuels - Determination of cold filter plugging point prEN 12662:20122), Liquid

28、petroleum products - Determination of total contamination in middle distillates, diesel fuels and fatty acid methyl esters EN 12916:20061), Petroleum products - Determination of aromatic hydrocarbon types in middle distillates - High performance liquid chromatography method with refractive index det

29、ection EN 14078:20091), Liquid petroleum products - Determination of fatty acid methyl ester (FAME) content in middle distillates - Infrared spectrometry method EN 14214:20123), Liquid petroleum products - Fatty acid methyl esters (FAME) for use in diesel engines and heating applications - Requireme

30、nts and test methods EN 15195:20071), Liquid petroleum products - Determination of ignition delay and derived cetane number (DCN) of middle distillate fuels by combustion in a constant volume chamber EN 15751:20091), Automotive fuels - Fatty acid methyl ester (FAME) fuel and blends with diesel fuel

31、- Determination of oxidation stability by accelerated oxidation method EN 16144:2012, Liquid petroleum products - Determination of ignition delay and derived cetane number (DCN) of middle distillate fuels - Fixed range injection period, constant volume combustion chamber method EN 16329:2013, Diesel

32、 and domestic heating fuels - Determination of cold filter plugging point - Linear cooling bath method prEN 16576:20132), Automotive fuels - Determination of manganese and iron content in middle distillate fuels - Inductively coupled plasma optical emission spectrometry (ICP OES) method EN 23015:199

33、4, Petroleum products - Determination of cloud point (ISO 3015:1992) EN ISO 2160:1998, Petroleum products - Corrosiveness to copper - Copper strip test (ISO 2160:1998) EN ISO 2719:2002, Determination of flash point - Pensky-Martens closed cup method (ISO 2719:2002) 1)Under revision. 2) In preparatio

34、n. 3) This document is currently impacted by EN 14214:2012/FprA1:2013. Copyright European Committee for Standardization Provided by IHS under license with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013EN 590:2013 (E) 5 EN ISO 3104:1996, Petroleum

35、 products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity (ISO 3104:1994) EN ISO 3170:2004, Petroleum liquids - Manual sampling (ISO 3170:2004) EN ISO 3171:19991), Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988) EN ISO 3405

36、:2011, Petroleum products - Determination of distillation characteristics at atmospheric pressure (ISO 3405:2011) EN ISO 3675:1998, Crude petroleum and liquid petroleum products - Laboratory determination of density - Hydrometer method (ISO 3675:1998) EN ISO 3924:2010, Petroleum products - Determina

37、tion of boiling range distribution - Gas chromatography method (ISO 3924:2010) EN ISO 4259:2006, Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006) EN ISO 4264:20074), Petroleum products - Calculation of cetane index of middle-distilla

38、te fuels by the four-variable equation (ISO 4264:2007) EN ISO 5165:19981), Petroleum products - Determination of the ignition quality of diesel fuels - Cetane engine method (ISO 5165:1998) EN ISO 6245:2002, Petroleum products - Determination of ash (ISO 6245:2001) EN ISO 10370:1995, Petroleum produc

39、ts - Determination of carbon residue - Micro method (ISO 10370:1993) EN ISO 12156-1:2006, Diesel fuel - Assessment of lubricity using the high-frequency reciprocating rig (HFRR) - Part 1: Test method (ISO 12156-1:2006) EN ISO 12185:1996, Crude petroleum and petroleum products - Determination of dens

40、ity - Oscillating U-tube method (ISO 12185:1996) EN ISO 12205:1996, Petroleum products - Determination of the oxidation stability of middle-distillate fuels (ISO 12205:1995) EN ISO 12937:2000, Petroleum products - Determination of water - Coulometric Karl Fischer titration method (ISO 12937:2000) EN

41、 ISO 13032:2012, Petroleum products - Determination of low concentration of sulfur in automotive fuels - Energy-dispersive X-ray fluorescence spectrometric method (ISO 13032:2012) EN ISO 13759:1996, Petroleum products - Determination of alkyl nitrate in diesel fuels - Spectrometric method (ISO 13759

42、:1996) EN ISO 20846:2011, Petroleum products - Determination of sulfur content of automotive fuels - Ultraviolet fluorescence method (ISO 20846:2011) EN ISO 20884:2011, Petroleum products - Determination of sulfur content of automotive fuels - Wavelength-dispersive X-ray fluorescence spectrometry (I

43、SO 20884:2011) 4) This document is currently impacted by EN ISO 4264:2007/A1:2013. Copyright European Committee for Standardization Provided by IHS under license with CENNot for ResaleNo reproduction or networking permitted without license from IHS-,-,-BS EN 590:2013EN 590:2013 (E) 6 3 Sampling Samp

44、les shall be taken as described in EN ISO 3170 or EN ISO 3171 and/or in accordance with the requirements of national standards or regulations for the sampling of automotive diesel fuel. The national requirements shall be set out in detail or shall be referred to by reference in a National Annex to t

45、his European Standard. In view of the sensitivity of some of the test methods referred to in this European Standard, particular attention shall be paid to compliance with any guidance on sampling containers which is included in the test method standard. 4 Pump marking Information to be marked on dis

46、pensing pumps used for delivering automotive diesel fuel, and the dimensions of the mark shall be in accordance with the requirements of national standards or regulations for the marking of pumps for automotive diesel fuel. Such requirements shall be set out in detail or shall be referred to by refe

47、rence in a National Annex to this European Standard. Labelling shall be clearly visible, easily legible and displayed at any point where diesel with metallic additives is made available to consumers. The label shall contain: “Contains metallic additives” in the national language(s) and shall be laid

48、 down in the National Annex to this document. 5 Requirements and test methods 5.1 Dyes and markers The use of dyes or markers is allowed. 5.2 Additives 5.2.1 General In order to improve the performance quality, the use of additives is allowed. Suitable fuel additives without known harmful side-effec

49、ts are recommended in the appropriate amount, to help to avoid deterioration of driveability and emissions control durability. Other technical means with equivalent effect may also be used. NOTE Deposit forming tendency test methods suitable for routine control purposes have not yet been identified and developed. 5.2.2 Methylcyclopentadienyl manganese tri