BS EN 843-1-2006 Advanced technical ceramics - Mechanical properties of nmonolithic ceramics at room temperature - Part 1 Determination of flexural strength《高级工业陶瓷 室温下单片陶瓷的机械特性 第1部.pdf

1、BRITISH STANDARDBS EN 843-1:2006Advanced technical ceramics Mechanical properties of monolithic ceramics at room temperature Part 1: Determination of flexural strengthThe European Standard EN 843-1:2006 has the status of a British StandardICS 81.060.30g49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g5

2、6g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58Licensed Copy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007, Uncontrolled Copy, (c) BSIBS EN 843-1:2006This British Standard was published under

3、 the authority of the Standards Policy and Strategy Committee on 31 January 2007 BSI 2007ISBN 978 0 580 49980 7National forewordThis British Standard was published by BSI. It is the UK implementation of EN 843-1:2006. It supersedes BS EN 843-1:1995 which is withdrawn.The UK participation in its prep

4、aration was entrusted to Technical Committee RPI/13, Advanced technical ceramics.A list of organizations represented on RPI/13 can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct ap

5、plication.Compliance with a British Standard cannot confer immunity from legal obligations. Amendments issued since publicationAmd. No. Date CommentsLicensed Copy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 843-1Decem

6、ber 2006ICS 81.060.30 Supersedes EN 843-1:1995 English VersionAdvanced technical ceramics - Mechanical properties ofmonolithic ceramics at room temperature - Part 1: Determinationof flexural strengthCramiques techniques avances - Proprits mcaniquesdes cramiques monolithiques temprature ambiante -Par

7、tie 1: Dtermination de la rsistance en flexionHochleistungskeramik - Mechanische Eigenschaftenmonolithischer Keramik bei Raumtemperatur - Teil 1:Bestimmung der BiegefestigkeitThis European Standard was approved by CEN on 11 November 2006.CEN members are bound to comply with the CEN/CENELEC Internal

8、Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This

9、European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the nat

10、ional standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United King

11、dom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2006 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 843-1:2006: ELicensed C

12、opy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 843-1:2006 (E) 2 Contents Page Foreword3 1 Scope 4 2 Normative references 4 3 Terms and definitions .5 4 Significance and use .5 5 Apparatus .6 5.1 Test jig 6 5.2 Test machine8 5.3 Micrometer or alternative calibrate

13、d device .8 5.4 Travelling microscope.8 5.5 Humidity measuring device 9 6 Test pieces .9 6.1 General9 6.2 Dimensions and tolerances 9 6.3 Surface finish .10 6.4 Number of test pieces .13 6.5 Precautions 13 7 Procedure .13 8 Calculations14 9 Test report 15 Annex A (informative) Typical fracture patte

14、rns in ceramic test pieces .17 Bibliography 20 Licensed Copy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 843-1:2006 (E) 3 Foreword This document (EN 843-1:2006) has been prepared by Technical Committee CEN/TC 184 “Advanced technical ceramics”, the secretariat of w

15、hich is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2007, and conflicting national standards shall be withdrawn at the latest by June 2007. This document supersedes EN 843-1:

16、1995. EN 843 Advanced technical ceramics Mechanical properties of monolithic ceramics at room temperature comprises six parts: Part 1: Determination of flexural strength Part 2: Determination of Youngs modulus, shear modulus and Poissons ratio Part 3: Determination of subcritical crack growth parame

17、ters from constant stressing rate flexural strength tests Part 4: Vickers, Knoop and Rockwell superficial hardness Part 5: Statistical analysis Part 6: Guidance for fractographic investigation At the time of publication of this Revision of Part 1, Part 6 was available as a Technical Specification. A

18、ccording to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lit

19、huania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. Licensed Copy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 843-1:2006 (E) 4 1 Scope This part of EN 843 specifies methods f

20、or determining the nominal flexural strength of advanced monolithic technical ceramic materials at ambient temperature. The available loading geometries are three- and four-point flexure, using rectangular section test pieces of two prescribed geometries: 20 mm support span (A) and 40 mm support spa

21、n (B). NOTE This part of EN 843 differs from ISO 14704 (see Bibliography) in respect of span A (not included in the ISO version), the absence of the 30 mm span option, and the required use of a fully articulating test jig. The test applies to materials with grain size less than 200 m. The test presc

22、ribes four categories of surface finish applied to the test pieces: I: as-fired or annealed after machining; II: standard finishing by grinding; III: standard finishing by lapping/polishing; IV: machined using agreed grinding procedures and material removal rates. 2 Normative references The followin

23、g referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 623-4, Advanced technical ceramics Monolithic ceramics Gen

24、eral and textural properties Part 4: Determination of surface roughness EN 843-5, Advanced technical ceramics Mechanical properties of monolithic ceramics at room temperature Part 5: Statistical analysis EN ISO 7500-1, Metallic materials Verification of static uniaxial testing machines Part 1: Tensi

25、on/compression testing machines Verification and calibration of the force-measuring system (ISO 7500-1:2004) EN ISO/IEC 17025, General requirements for the competence of testing and calibration laboratories (ISO/IEC 17025:2005) ISO 3611, Micrometer callipers for external measurement ISO 4677-1, Atmo

26、spheres for conditioning and testing Determination of relative humidity Part 1: Aspirated psychrometer method ISO 4677-2, Atmospheres for conditioning and testing Determination of relative humidity Part 2: Whirling psychrometer method Licensed Copy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007,

27、Uncontrolled Copy, (c) BSIEN 843-1:2006 (E) 5 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 nominal flexural strength maximum nominal stress supported by the material at the instant of failure when loaded in linear elastic bending 3.2 three

28、-point flexure means of bending a beam test piece whereby the test piece is supported on bearings near its ends and a central force is applied 3.3 four-point flexure means of bending a beam test piece whereby the test piece is supported on bearings near its ends and is loaded equally at two position

29、s symmetrically disposed about the centre of the supported span 3.4 quarter-point flexure four-point flexure (3.3) wherein the loading bearings are each one-quarter of the support span from the support bearings 4 Significance and use This test is intended to be used for material development, quality

30、 control, characterization and design data acquisition purposes. The strength level determined by the test is calculated on the basis of linear elastic bending of a thin beam on the assumption that the material being tested is elastically homogeneous and isotropic, and shows linear (Hookean) stress-

31、strain behaviour. The result obtained from a strength test is determined by a large number of factors associated with the microstructure of the material, the surface finishing procedure applied in preparation of the test pieces, the size and shape of the test piece, the mechanical function of the te

32、sting apparatus, the rate of load application and the relative humidity of the ambient atmosphere. As a consequence of the brittle nature of ceramics, there is usually a considerable range of results obtained from a number of nominally identical test pieces. These factors combined mean that caution

33、in the interpretation of test results is required. For many purposes, and as described in this European Standard, the results of strength tests may be described in terms of a mean value and a standard deviation. Further statistical evaluation of results is required for design data acquisition, and m

34、ay be desirable for other purposes (see EN 843-5). This method places closely defined restrictions on the size and shape of the test piece and on the function of the test apparatus in order to minimize the errors that can arise as a consequence of the test method. NOTE The basis for the choice of di

35、mensions and tolerances of test pieces and of the requirements of the test-jig may be found in reference 4. All other test factors are required to be stated in the test report (see Clause 9) in order to allow inter-comparison of material behaviours. It is not possible to rigorously standardize parti

36、cular surface finishes, since these are not absolutely controllable in mechanical terms. The inclusion of a standard grinding procedure (see 6.3) as one of the surface finish options in this method is intended to provide a means of obtaining a minimum amount of residual grinding damage in the test m

37、aterial. The extrapolation of flexural strength data to other geometries of stressing, to multiaxial stressing, to other rates of stressing or to other environments should be viewed with caution. Licensed Copy: Wang Bin, na, Wed Apr 04 07:29:24 GMT+00:00 2007, Uncontrolled Copy, (c) BSIEN 843-1:2006

38、 (E) 6 The origin of fracture in a flexural test can be a valuable guide to the nature and position of strength-limiting defects. Fractography of test pieces is highly recommended. In particular, the test may identify fracture origins as being edge defects (caused by edge preparation), surface defec

39、ts (caused by surface preparation), or internal defects (caused by manufacturing inhomogeneities such as pores, large grains, impurity concentrations etc.). Not all advanced monolithic technical ceramics are amenable to clear fractography. 5 Apparatus 5.1 Test jig The test jig shall be capable of ei

40、ther three-point or four-point flexure and functioning as specified below in order to minimize misalignments, twist and frictional forces applied to the test piece. NOTE 1 The precise test jig design is not specified, only the function. Schematic arrangements of the test jig function are shown in Fi

41、gure 1 a) for three-point flexure, and Figure 1 b) for four-point flexure. The test piece shall be supported on two bearing edges perpendicular to its length. The outer support bearing edges shall be parallel rollers of diameter approximately 1,5 times the test piece thickness. Diameters of between

42、2,2 mm and 2,5 mm (for span A - see 6.2) or between 4,5 mm and 5,0 mm (for span B - see 6.2) are recommended. The rollers shall be capable of rolling outward on flat support surfaces. One of the rollers shall additionally be capable of rotating about an axis parallel to the length of the test piece

43、such that torsional loading is minimized. The two rollers shall be positioned initially with their centres 20 mm 0,5 mm apart (span A) or 40 mm 0,5 mm apart (span B) with their axes parallel to 0,2 mm over their lengths ( 12 mm). See Figure 2. For three-point flexure, a third roller shall be located

44、 at the mid-point between and parallel to the two support rollers (Figures 2 a) and 2 c). This roller shall have the same diameter as the support rollers and shall be similarly free to rotate about an axis parallel to the length of the test piece. Its position relative to the midpoint between the su

45、pport rollers shall be better than 0,2 mm, measured to the nearest 0,1 mm in a direction parallel to the length of the test piece using the travelling microscope or other suitable device (see 5.4). For four-point flexure, two loading rollers shall be located at the quarter points (see 3.4), i.e. wit

46、h inner spans 10 mm 0,2 mm (outer span A) or 20 mm 0,2 mm (outer span B), and shall be free to roll inwards (Figures 2 b) and 2 d). As with the three-point apparatus, the two rollers shall also be free to rotate separately about an axis parallel to the length of the test piece to allow alignment. Th

47、e loading rollers shall be symmetrically positioned to within 0,1 mm. The distances between the centres of the support rollers and adjacent loading rollers shall be measured to the nearest 0,1 mm along the length of the test piece perpendicular to the direction of loading, using the travelling micro

48、scope or other suitable device (see 5.4). The arrangement for loading shall ensure that equal forces are applied to the two loading rollers. The separation of the centres of the rollers in their starting positions shall be measured to the nearest 0,1 mm with the travelling microscope (see 5.3.2) or

49、other suitable device. The rollers shall be made from hardened steel or other hard material with a hardness greater than 40 HRC (Rockwell C-scale) for strengths less than 1,4 GPa and not less than 46 HRC for strengths greater than 1,4 GPa. The rollers shall have a smooth burr-free surface finish with roughness less than 0,5 m Raand shall have diameter uniform to 0,015 mm. NOTE 2 The accurate and repeatable lateral positioning of the rollers can best be achieved by ensuring that in the unloaded position, the support roller