1、BSI Standards PublicationBS EN 13924-2:2014Bitumen and bituminousbinders Specificationframework for special pavinggrade bitumenPart 2: Multigrade paving grade bitumensBS EN 13924-2:2014 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN 13924-2:2014.The UK particip
2、ation in its preparation was entrusted to TechnicalCommittee B/510/19, Bitumen and related products.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are respo
3、nsible for its correctapplication. The British Standards Institution 2014. Published by BSI StandardsLimited 2014ISBN 978 0 580 75655 9ICS 75.140; 91.100.50Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theSt
4、andards Policy and Strategy Committee on 30 April 2014.Amendments issued since publicationDate Text affectedBS EN 13924-2:2014EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13924-2 March 2014 ICS 75.140; 91.100.50 English Version Bitumen and bituminous binders - Specification framework for spe
5、cial paving grade bitumen - Part 2: Multigrade paving grade bitumens Bitumes et liants bitumineux - Cadre de spcifications pour les bitumes routiers spciaux - Partie 2: Bitumes routiers multigrades Bitumen und bitumenhaltige Bindemittel - Anforderungsrahmenwerk fr spezielle Straenbaubitumen - Teil 2
6、: Multigrade Straenbaubitumen This European Standard was approved by CEN on 4 February 2014. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date
7、 lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation u
8、nder the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Forme
9、r Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT E
10、UROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 13924-2:2014 EBS EN 13924-2:2014EN 13924-2:2014 (E) 2 Cont
11、ents Page Foreword 3 Introduction .4 1 Scope 5 2 Normative references 5 3 Terms and definitions .5 4 Sampling .6 5 Requirements and test methods 6 5.1 General 6 5.2 Properties and related test methods .6 5.2.1 General 6 5.2.2 Consistency at intermediate service temperature .6 5.2.3 Consistency at el
12、evated service temperature 6 5.2.4 Temperature dependence of consistency .6 5.2.5 Brittleness at low service temperature 6 5.2.6 Durability Resistance to hardening 7 5.2.7 Temperature dependency of mixing 7 5.2.8 Other properties .7 5.2.9 Informative properties .7 5.3 Release of regulated dangerous
13、substances .7 5.4 Precision .7 6 Assessment and verification of constancy of performance - AVCP 9 6.1 General 9 6.2 Type testing 9 6.2.1 General 9 6.2.2 Test samples, testing and compliance criteria 10 6.2.3 Test reports . 10 6.2.4 Shared other party results . 10 6.3 Factory production control (FPC)
14、 . 11 6.3.1 General . 11 6.3.2 Requirements 11 6.3.3 Initial inspection of factory and of FPC 14 6.3.4 Continuous surveillance of FPC . 14 6.3.5 Procedure for modifications 15 6.3.6 One-off products, pre-production products (e.g. prototypes) and products produced in very low quantity. 15 Annex A (no
15、rmative) Calculation of the penetration index, Ip. 17 Annex B (normative) Informative properties . 19 Annex ZA (informative) Clauses of this European Standard addressing the provisions of the EC Construction Products Regulation . 20 ZA.1 Scope and relevant characteristics 20 ZA.2 Procedure for AVCP
16、of multigrade paving grade bitumens . 21 ZA.2.1 System of attestation of conformity . 21 ZA.2.2 Declaration of performance (DoP) 22 ZA.2.2.1 General . 22 ZA.2.2.2 Content . 23 ZA.2.2.3 Example of DoP . 24 ZA.3 CE marking and labelling . 25 Bibliography . 29 BS EN 13924-2:2014EN 13924-2:2014 (E) 3 Fo
17、reword This document (EN 13924-2:2014) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the la
18、test by September 2014 and conflicting national standards shall be withdrawn at the latest by December 2015. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or a
19、ll such patent rights. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association, and supports essential requirements of EU Directive(s). For relationship with EU Directive(s), see informative Annex ZA which is an integral part of
20、 this document. This European Standard is part of a family of European Standards for bitumen as follows: NOTE Industrial applications are not covered by mandate M/124. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to impl
21、ement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania
22、, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. BS EN 13924-2:2014EN 13924-2:2014 (E) 4 Introduction This document is closely related to EN 12591. This introduction gives information on the basis for selection of the grades defined in this document, the status of cer
23、tain of the properties and test methods, and proposed development of this document. The general principle adopted in the development of EN 12591 was to provide a range of grades suitable for the manufacture of the materials for road construction and maintenance used, and the climatic and traffic con
24、ditions encountered, in all the Member States. This document extends the range of grades specified in EN 12591, following the wider use of materials for road construction and maintenance. This document has been based on the regional requirements identified when the process started. It is a first ste
25、p in harmonising the so-called “empirical“ specifications and it is intended to evaluate alternative properties and test methods to develop new specifications that are more directly performance-related. To this end, work programmes are being undertaken and the results will be considered for a future
26、 revision of this document. The progress of those work programmes are reported in CEN/TR 15352 1, and the results will be considered for future revisions of this European Standard. For multigrade paving grade bitumens (MG), the testing of the five essential characteristics, according to the mandate
27、M/124, also gives an indication that its intrinsic cohesive properties are adequate for its normal use. The properties of “adhesion“ and “setting ability“ are indicated by tests used on the finished asphalt mixtures, EN 12697-1, EN 12697-11, EN 12697-12, EN 12697-26 (respectively 2 to 5), rather tha
28、n tests on the bitumen itself. In certain acid modified binders the structure may change when mixed with aggregate. Table B.1 lists informative properties which suppliers of multigrade bitumens are encouraged to produce as “Supplier Declared Values”. It is hoped that the data so provided will form t
29、he basis for developing performance-related specifications in the future. BS EN 13924-2:2014EN 13924-2:2014 (E) 5 1 Scope This document provides a framework for specifying the properties and relevant test methods for multigrade paving grade bitumens which are suitable for use in the construction and
30、 maintenance of roads, airfields and other paved areas, together with information for attestation and verification of constancy of performance. Multigrade paving grade bitumens are designated in EN 12597:2000 as special bitumens for road applications having a positive penetration index (Ip). This do
31、cument does not directly address cohesion, adhesion and settling ability, (see Clause Introduction). 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cite
32、d applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders - Sampling bituminous binders EN 1426, Bitumen and bituminous binders - Determination of needle penetration EN 1427, Bitumen and bituminous binde
33、rs - Determination of the softening point - Ring and Ball method EN 12592, Bitumen and bituminous binders - Determination of solubility EN 12593, Bitumen and bituminous binders - Determination of the Fraass breaking point EN 12594, Bitumen and bituminous binders - Preparation of test samples EN 1259
34、5, Bitumen and bituminous binders - Determination of kinematic viscosity EN 12596, Bitumen and bituminous binders - Determination of dynamic viscosity by vacuum capillary EN 12597:2000, Bitumen and bituminous binders - Terminology EN 12607-1, Bitumen and bituminous binders - Determination of the res
35、istance to hardening under the influence of heat and air - Part 1: RTFOT method EN 15326 Bitumen and bituminous binders Measurement of density and specific gravity Capillary-stoppered pyknometer method EN ISO 2592, Determination of flash and fire points - Cleveland open cup method (ISO 2592:2000) EN
36、 ISO 4259, Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259) 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 12597:2000 apply. 3.1 multigrade paving grade bitumens multigrade paving grade bi
37、tumens are designated by stating MG and the nominal penetration range at 25 C, followed by the softening point range (see Table 1), e.g. “MG 20/30-64/74“ BS EN 13924-2:2014EN 13924-2:2014 (E) 6 4 Sampling Samples of bulk products shall be taken as described in EN 58. Test samples shall be taken from
38、 the laboratory samples, and prepared for testing, as described in EN 12594. 5 Requirements and test methods 5.1 General The requirements for the properties for a specific grade shall be selected from the classes given in Tables 1 and 2. The properties in Table 1 shall be specified for all multigrad
39、e paving grade bitumens. They are associated with regulatory or Health Safety and Environmental requirements. The properties in Table 2 are required to meet specific regional conditions. They are associated with regulatory or other regional requirements. When tested by the methods given in the table
40、s, the various multigrade paving grade bitumens shall conform to the limits specified by classes in these tables. NOTE The TBR class has been included to facilitate selection in countries which merely wish to record a suppliers range for a particular requirement. It should not be considered as a “Cl
41、ass“ for the purpose of regulatory marking. These values can be used as a basis for the development of future technical specifications. The selection of classes should be made from past experience to avoid unworkable combinations. 5.2 Properties and related test methods 5.2.1 General For specifying
42、multigrade paving grade bitumens the appropriate class for each technical requirement is selected in turn. Different classes may be selected for different properties. 5.2.2 Consistency at intermediate service temperature Consistency at intermediate service temperature for these multigrade paving gra
43、de bitumens shall comply with the requirements for penetration at 25 C in Table 1. 5.2.3 Consistency at elevated service temperature Consistency at elevated service temperature for these multigrade paving grade bitumens shall comply with the requirements for softening point Ring and Ball in Table 1.
44、 5.2.4 Temperature dependence of consistency Temperature dependence of consistency shall comply with the requirements for penetration index (Ip) in Table 1. Where required, multigrade paving grade bitumens shall comply also with the requirement for dynamic viscosity in Table 2. The penetration index
45、 shall be calculated in accordance with Annex A. 5.2.5 Brittleness at low service temperature Brittleness at low service temperature may be required to meet specific regional conditions. Where required, multigrade paving grade bitumens shall conform to the requirements for Fraass breaking point in T
46、able 2. BS EN 13924-2:2014EN 13924-2:2014 (E) 7 5.2.6 Durability Resistance to hardening Durability shall be demonstrated by compliance with the required surrogate characteristics “Resistance to hardening“ of Table 1. Resistance to hardening shall be tested after running the Rolling Thin Film Oven T
47、est (RTFOT), EN 12607-1. NOTE Appropriate tests and classes, for measurements on material after the hardening procedure, are given in Table 1. The choice of class may depend upon the intended use of the product. 5.2.7 Temperature dependency of mixing Where required, multigrade paving grade bitumens
48、shall comply also with the requirement for kinematic viscosity in Table 2. 5.2.8 Other properties 5.2.8.1 Flash point Flash point shall be determined by the Cleveland open cup method in EN ISO 2592. NOTE The Pensky-Martens closed cup method (see EN ISO 2719 8) can be used to investigate possible con
49、tamination, but is likely to give lower values. 5.2.8.2 Density If the supplier wishes to declare the density of multigrade paving grade bitumens, it shall be determined in accordance with EN 15326. 5.2.8.3 Solubility Solubility shall be determined on the fresh multigrade paving grade bitumens in accordance with EN 12592. 5.2.9 Informative properties The specifications include a table of informative properties (Annex B) based on new test methods. Suppliers of multigrade paving grade bitumens are invited to supply data from these measurements to the client o
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