BS EN 60556-2006 Gyromagnetic materials intended for application at microwave frequencies - Measuring methods for properties《用于微波频率的旋磁材料 性能的测量方法》.pdf

1、BRITISH STANDARDBS EN60556:2006Gyromagnetic materials intended for application at microwave frequencies Measuring methods for propertiesThe European Standard EN 60556:2006 has the status of a British StandardICS 29.100.10g49g50g3g38g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g4

2、4g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58Licensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSIBS EN 60556:2006This British Standard was published under the authority of the Standards Polic

3、y and Strategy Committee on 31 July 2006 BSI 2006ISBN 0 580 48909 4National forewordThis British Standard is the official English language version of EN 60556:2006. It is identical with IEC 60556:2006.The UK participation in its preparation was entrusted to Technical Committee EPL/51, Transformers,

4、inductors, magnetic components and ferrite materials, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its secretary.Cross-referencesThe British Standards which implement international or European publications referred to in this do

5、cument may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online.This publication does not purport to include all the necessary provisions of a contract

6、. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for c

7、hange, and keep UK interests informed; monitor related international and European developments and promulgate them in the UK.Summary of pagesThis document comprises a front cover, an inside front cover, the EN title page, pages 2 to 57 and a back cover.The BSI copyright notice displayed in this docu

8、ment indicates when the document was last issued.Amendments issued since publicationAmd. No. Date CommentsLicensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSIEUROPEAN STANDARD EN 60556 NORME EUROPENNE EUROPISCHE NORM June 2006 CENELEC European Committee for Electrote

9、chnical Standardization Comit Europen de Normalisation Electrotechnique Europisches Komitee fr Elektrotechnische Normung Central Secretariat: rue de Stassart 35, B - 1050 Brussels 2006 CENELEC - All rights of exploitation in any form and by any means reserved worldwide for CENELEC members. Ref. No.

10、EN 60556:2006 E ICS 29.100.10 English version Gyromagnetic materials intended for application at microwave frequencies - Measuring methods for properties (IEC 60556:2006) Materiaux gyromagntiques destins aux applications hyperfrquences -Mthodes de mesure des caractristiques(CEI 60556:2006) Gyromagne

11、tische Materialien fr Mikrowellenanwendungen - Messverfahren zur Ermittlung der Eigenschaften (IEC 60556:2006) This European Standard was approved by CENELEC on 2006-05-01. CENELEC members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this Eu

12、ropean Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CENELEC member. This European Standard exists in two official versions (Eng

13、lish and German). A version in any other language made by translation under the responsibility of a CENELEC member into its own language and notified to the Central Secretariat has the same status as the official versions. CENELEC members are the national electrotechnical committees of Austria, Belg

14、ium, Cyprus, the Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, the Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Licensed Copy: Wang

15、Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSIForeword The text of document 51/850/FDIS, future edition 2 of IEC 60556, prepared by IEC TC 51, Magnetic components and ferrite materials, was submitted to the IEC-CENELEC parallel vote and was approved by CENELEC as EN 60556 on 2006-

16、05-01. This Standard is to be used in conjunction with IEC 60392. The following dates were fixed: latest date by which the EN has to be implemented at national level by publication of an identical national standard or by endorsement (dop) 2007-02-01 latest date by which the national standards confli

17、cting with the EN have to be withdrawn (dow) 2009-05-01 Annex ZA has been added by CENELEC. _ Endorsement notice The text of the International Standard IEC 60556:2006 was approved by CENELEC as a European Standard without any modification. _ EN 60556:2006 2 Licensed Copy: Wang Bin, na, Mon Sep 18 07

18、:45:20 BST 2006, Uncontrolled Copy, (c) BSI 3 EN 60556:2006 CONTENTS 1 Scope 7 2 Normative references .7 3 Terms and definitions .7 4 Saturation magnetization Ms.7 4.1 General .7 4.2 Object .8 4.3 Theory.8 4.4 Test sample.9 4.5 Measuring apparatus for the vibrating coil method (VCM) .9 4.5.1 Arrange

19、ment of detection coils and sample.9 4.5.2 The electromagnet .10 4.5.3 Elimination of applied field effects 10 4.5.4 Electronic instrumentation 11 4.6 Measuring apparatus for the vibrating sample method (VSM)12 4.6.1 Arrangement of detection coils and sample.12 4.6.2 The electromagnet .13 4.6.3 Elec

20、tronic instrumentation 13 4.7 Calibration.15 4.7.1 Comparison method .15 4.7.2 “Slope” method 15 4.8 Measuring procedure .16 4.8.1 Zero setting Vibrating coil method .16 4.8.2 Zero setting Vibrating sample method17 4.8.3 Measurement.17 4.9 Calculation 17 4.10 Accuracy .17 4.11 Data presentation 18 5

21、 Magnetization (at specified field strength) MH.18 5.1 General .18 5.2 Object .18 5.3 Theory.18 5.4 Test specimen .20 5.5 Measuring apparatus .21 5.6 Calibration.23 5.7 Measuring procedure .24 5.8 Calculation 24 5.9 Accuracy .24 5.10 Data presentation 24 6 Gyromagnetic resonance linewidth H and effe

22、ctive Land factor geff(general).25 6.1 General .25 6.2 Object .25 6.3 Theory.25 6.4 Test specimens and cavities 26 Licensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSIEN 60556:2006 4 6.5 Measuring apparatus .29 6.6 Measuring procedure .29 6.7 Calculation 31 6.8 Accur

23、acy .31 6.9 Data presentation 31 7 Gyromagnetic resonance linewidth H10and effective Land factor g10(at 10 GHz) .31 7.1 General .31 7.2 Object .31 7.3 Theory.31 7.4 Test specimen and cavity.32 7.5 Measuring apparatus .33 7.6 Measuring procedure .33 7.7 Calculation 34 7.8 Accuracy .34 7.9 Data presen

24、tation 35 8 Spin-wave resonance linewidth Hk.35 8.1 General .35 8.2 Object .35 8.3 Theory.35 8.4 Test specimen and cavity.38 8.5 Measuring apparatus .39 8.6 Calibration.39 8.7 Measuring procedure .39 8.8 Calculation 40 8.9 Accuracy .40 8.10 Data presentation 40 9 Effective linewidth Heff.40 9.1 Gene

25、ral .40 9.2 Object .40 9.3 Theory.41 9.3.1 Definitions .41 9.3.2 Measurement.41 9.4 Test specimen and cavity.43 9.5 Measuring apparatus .43 9.6 Calibration.44 9.7 Apparatus adjustment44 9.7.1 Adjustment principle.44 9.7.2 Adjustment procedure 45 9.8 Measuring procedure .45 9.8.1 Measurement of f0.45

26、 9.8.2 Determination of Q0.45 9.8.3 Measurement of f and Q .46 9.9 Calculation 46 9.10 Accuracy .46 9.11 Data presentation 46 10 Complex permittivity r.47 10.1 General .47 Licensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSI 5 EN 60556:2006 10.2 Object .47 10.3 Theor

27、y.47 10.4 Test specimen and cavity.50 10.5 Measuring apparatus .50 10.6 Measurement procedure 51 10.7 Calculation 51 10.8 Accuracy .52 10.9 Data presentation 52 11 Apparent density app52 11.1 General .52 11.2 Apparent density (by mensuration).52 11.2.1 Object52 11.2.2 Test specimen .53 11.2.3 Measur

28、ing apparatus53 11.2.4 Calibration .53 11.2.5 Measuring procedure .53 11.2.6 Calculation.53 11.2.7 Accuracy53 11.2.8 Data presentation 53 11.3 Apparent density (by water densitometry).54 11.3.1 Object54 11.3.2 Theory.54 11.3.3 Test specimen .54 11.3.4 Measuring apparatus54 11.3.5 Calibration .54 11.

29、3.6 Measuring procedure .55 11.3.7 Calculation.55 11.3.8 Accuracy55 11.3.9 Data presentation 55 Annex ZA (normative) Normative references to international publications with their corresponding European publications58 Licensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) B

30、SIEN 60556:2006 6 Figure 1 Vibrating coil method Sample and coils arrangement9 Figure 2 Magnetic field configuration 10 Figure 3 Measuring apparatus (VCM) .12 Figure 4 Vibrating sample method Sample and coil arrangement13 Figure 5 Measuring apparatus (VSM) .14 Figure 6 Hysteresis curves for a magnet

31、ic material: B(H) curve, M(H) curve19 Figure 7 Test sample with compensation unit20 Figure 8 Test specimen21 Figure 9 Measuring circuit for determining magnetization (at specified field strength) MH22 Figure 10 Miller integrator 23 Figure 11 Cavity for measurement of gyromagnetic resonance linewidth

32、 and effective Land factor .27 Figure 12 Stripline resonator for measurement of gyromagnetic resonance linewidth and effective Land factor at low frequency.28 Figure 13 Schematic diagram of the equipment required for measurement of gyromagnetic resonance linewidth and effective Land factor 30 Figure

33、 14 Schematic diagram of the equipment required for measurement of gyromagnetic resonance linewidth and effective Land factor at 10 GHz 34 Figure 15 Subsidiary absorption and saturation of the normal resonance.36 Figure 16 Pulse deterioration at onset of subsidiary resonance .36 Figure 17 Measured c

34、ritical r.f. field strength as a function of pulse duration td37 Figure 18 Typical TE104cavity for the measurement of spin-wave resonance linewidth at about 9,3 GHz .38 Figure 19 Block diagram of spin-wave resonance linewidth test equipment39 Figure 20 Sectional view of the cavity with specimen 42 F

35、igure 21 Dimensions of a cavity designed for resonance at a frequency of 9,1 GHz .42 Figure 22 Schematic diagram of equipment for measuring effective linewidth Heff44 Figure 23 Determination of Q046 Figure 24 Ideal resonant cavity with specimen, used for theoretical calculation (sectional view).48 F

36、igure 25 Dimensions of the resonant cavity with specimen 50 Figure 26 Schematic diagram of equipment required for the measurement of complex dielectric constant .51 Licensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSI 7 EN 60556:2006 GYROMAGNETIC MATERIALS INTENDED F

37、OR APPLICATION AT MICROWAVE FREQUENCIES MEASURING METHODS FOR PROPERTIES 1 Scope This International Standard describes methods of measuring the properties used to specify polycrystalline microwave ferrites in accordance with IEC 60392 and for general use in ferrite technology. These measuring method

38、s are intended for the investigation of materials, generally referred to as ferrites, for application at microwave frequencies. Single crystals and thin films generally fall outside the scope of this standard. NOTE 1 For the purposes of this standard, the words “ferrite” and “microwave” are used in

39、a broad sense: by “ferrites” is meant not only magneto-dielectric chemical components having a spinel crystal structure, but also materials with garnet and hexagonal structures; the “microwave” region is taken to include wavelengths approximately between 1 m and 1 mm, the main interest being concent

40、rated on the region 0,3 m to 10 mm. NOTE 2 Examples of components employing microwave ferrites are non-reciprocal devices such as circulators, isolators and non-reciprocal phase-shifters. These constitute the major field of application, but the materials may be used in reciprocal devices as well, fo

41、r example, modulators and (reciprocal) phase-shifters. Other applications include gyromagnetic filters, limiters and more sophisticated devices, such as parametric amplifiers. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated

42、references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendment) applies. IEC 60050-221, International Electrotechnical Vocabulary (IEV) Part 221: Magnetic materials components IEC 60205:2006, Calculation of the effective par

43、ameters of magnetic piece parts IEC 60392:1972, Guide for the drafting of specifications for microwave ferrites 3 Terms and definitions For the purposes of this document, the terms and definitions given in IEC 60050-221 apply. 4 Saturation magnetization Ms4.1 General Saturation magnetization is a ch

44、aracteristic parameter of ferrite materials. It is widely used in theoretical calculations, for instance in computation of tensor permeability components (see IEC 60050-221). In a variety of microwave applications, saturation magnetization determines the lower frequency limit of the device, mainly d

45、ue to the occurrence of so-called low-field loss when the material is unsaturated. Licensed Copy: Wang Bin, na, Mon Sep 18 07:45:20 BST 2006, Uncontrolled Copy, (c) BSIEN 60556:2006 8 4.2 Object The object is to give two similar techniques for measuring saturation magnetization. These are the vibrat

46、ing coil method (VCM) and vibrating sample method (VSM). The vibrating coil method 112 has the advantages of easier sample mounting and simpler mechanical arrangement when measurements over a range of temperatures are required, particularly at low temperatures. The vibrating sample method is more ac

47、curate, given a similar degree of elaboration in electronic apparatus. The equipment needed in both cases is very similar and the calibration methods are identical. The same test samples can be used for either technique. 4.3 Theory When a sphere of isotropic magnetic material is placed in a uniform

48、magnetic field, the sphere becomes uniformly magnetized in the direction parallel to the applied field. The sphere now produces its own external magnetic field, equivalent to that of a magnetic dipole at the centre of the sphere and orientated parallel to the direction of magnetization. If a small d

49、etection coil (in practice a pair wound in opposition) is now vibrated at small amplitude, close to the sample sphere and in a direction at right angles to the applied field, a voltage es, will be induced in the coil, proportional to the rate of change of flux sdue to the sample at the mean coil position x0whose value is given by dtdxdxdNex=0ss(1) where N is the number of turns on the coil. The motion of the coil, in the x-direction,