BS EN ISO 105-X02-1996 Textiles Tests for colour fastness Colour fastness to carbonizing Sulfuric acid《纺织品 色牢度试验 第X02部分 耐碳化色牢度 硫酸法》.pdf

1、BRITISH STANDARD BS EN ISO 105-X02:1996 Textiles Tests for colour fastness Part X02: Colour fastness to carbonizing: Sulfuric acid The European Standard ENISO105-X02:1995 has the status of a British Standard ICS 59.080.10BSENISO105-X02:1996 This British Standard, having been prepared under the direc

2、tionof the Sector Board forMaterials and Chemicals, waspublished under the authorityof the Standards Boardand comes into effect on 15March1996 BSI 10-1999 The following BSI references relate to the work on this standard: Committee reference TCI/25 Draft announced in BSI News February 1995 ISBN 0 580

3、 23984 5 Committees responsible for this British Standard The preparation of this British Standard was entrusted to Technical Committee TCI/25, Chemical properties, upon which the following bodies were represented: Association of Consulting Scientists Association of Suppliers to the British Clothing

4、 Industry British Apparel and Textile Confederation British Clothing Industry Association British Measurement and Testing Association British Retail Consortium Chemical Industries Association Consumer Policy Committee of BSI Fabric Care Research Association Ltd. Home Laundering Consultative Council

5、International Wool Secretariat Mail Order Traders Association Ministry of Defence National Wool Textile Export Corporation SATRA Footwear Technology Centre Soap and Detergent Industry Association Society of Dyers and Colourists Textile Finishers Association Participation in the detailed technical wo

6、rk was undertaken by the Society of Dyers and Colourists. Amendments issued since publication Amd. No. Date CommentsBSENISO105-X02:1996 BSI 10-1999 i Contents Page Committees responsible Inside front cover National foreword ii Foreword 2 1 Scope 3 2 Normative references 3 3 Principle 3 4 Apparatus a

7、nd materials 3 5 Test specimen 3 6 Procedure 3 7 Test report 4 Annex ZA (normative) Normative references to international publications with their relevant European publications 5 List of references Inside back coverBSENISO105-X02:1996 ii BSI 10-1999 National foreword This British Standard has been p

8、repared by Technical Committee TCI/25 and is the English language version of ENISO105-X02:1995 Textiles Tests for colour fastness Part X02 Colour fastness to carbonizing: Sulfuric acid, published by the European Committee for Standardization (CEN). It is identical with ISO105-X02:1993, published by

9、the International Organization for Standardization (ISO). This British Standard supersedes the corresponding method in BS1006:1990, which is withdrawn by amendment. A British Standard does not purport to include all the necessary provisions of a contract. Users of British Standards are responsible f

10、or their correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. Cross-references Publication referred to Corresponding British Standard ISO 105-A01:1989 BS EN ISO 105 Textiles Tests for colour fastness Part A01:1996 General principles of te

11、sting ISO 105-A02:1993 BS EN 20105 Textiles Tests for colour fastness Part A02:1995 Grey scale for assessing change in colour Summary of pages This document comprises a front cover, an inside front cover, pages i and ii, theEN ISO title page, pages 2 to 6, an inside back cover and a back cover. This

12、 standard has been updated (see copyright date) and may have had amendments incorporated. This will be indicated in the amendment table on the inside front cover.EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 105-X02 November 1995 ICS 59.080.10 Descriptors: Textiles, dyes, tests, carbonizi

13、ng tests, determination, colour fastness English version Textiles Tests for colour fastness Part X02: Colour fastness to carbonizing: Sulfuric acid (ISO105-X02:1993) Textiles Essais de solidit des teintures Partie X02: Solidit au carbonisage: Acide sulfurique (ISO 105-X02:1993) Textilien Farbechthei

14、tsprfungen Teil X02: Farbechtheit gegen das Karbonisieren: Schwefelsure (ISO 105-X02:1993) This European Standard was approved by CEN on1995-07-28. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of

15、 a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the Central Secretariat or to any CEN member. This European Standard exists in three official versions (English, French, German). A versio

16、n in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Denmark, Finland, France, Germany, Greec

17、e, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. CEN European Committee for Standardization Comit Europen de Normalisation Europisches Komitee fr Normung Central Secretariat: rue de Stassart 36, B-1050 Brussels 1995 All rights of r

18、eproduction and communication in any form and by any means reserved in all countries to CEN and its members. Ref. No. EN ISO 105-X02:1995 EENISO105-X02:1995 BSI 10-1999 2 Foreword The text of the International Standard from ISO/TC38, Textiles, of the International Organization for Standardization (I

19、SO) has been taken over as a European Standard by the Technical Committee CEN/TC248, Textiles and textile products. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May1996, and conflicting nationa

20、l standards shall be withdrawn at the latest by May1996. According to CEN/CENELEC Internal Regulations, the following countries are bound to implement this European Standard: Austria, Belgium, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portug

21、al, Spain, Sweden, Switzerland and the United Kingdom. NOTENormative references to International Standards are listed inAnnex ZA (normative).ENISO105-X02:1995 BSI 10-1999 3 1 Scope This part of ISO105 specifies a method for determining the resistance of the colour of textiles in all forms to the man

22、ufacturing operation designed to remove vegetable impurities by treatment with sulfuric acid at high temperatures. The method is mainly applicable to wool and textiles containing wool. 2 Normative references The following standards contain provisions which, through reference in this text, constitute

23、 provisions of this part of ISO105. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of ISO105 are encouraged to investigate the possibility of applying the most recent editions of the standards indicat

24、ed below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 105-A01:1989, Textiles Tests for colour fastness Part A01: General principles of testing. ISO 105-A02:1993, Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour. 3 Pr

25、inciple A specimen impregnated with sulfuric acid solution is dried, baked, rinsed and neutralized. The changes in colour after rinsing, neutralizing and drying are assessed with the grey scale. 4 Apparatus and materials 4.1 Oven, for drying specimens in air at60 C 2 C and baking in air at105 C 2 C.

26、 4.2 Sulfuric acid solution, containing50g of concentrated sulfuric acid ( 1,84g/ml) per litre. 4.3 Sodium carbonate solution, containing2g of anhydrous sodium carbonate per litre. 4.4 Test control: A dyeing of Cl Mordant Red3 (Colour Index, 3rd Edition) treated with potassium dichromate. The test c

27、ontrol is prepared by entering a well wetted-out pattern of wool cloth at40 C into a dye-bath containing1%Cl Mordant Red3 (Colour Index, 3rd Edition), 10% sodium sulfate decahydrate (Na 2 SO 4 .10H 2 O) and3% acetic acid(300g/l), all percentages being calculated on the mass of the pattern, at a liqu

28、or ratio of40:1. The dye-bath is raised to the boil in30min and boiled for a further30min. If necessary, the dye-bath is exhausted by careful addition of1% to3% acetic acid (300g/l) or1% sulfuric acid ( 1,84g/ml), well diluted with water. The bath is boiled for a further15min after addition of the a

29、cid. The dye-bath is cooled down by addition of cold water, and0,5% potassium dichromate dissolved in water is added. The dye-bath is raised to the boil again and boiled for30min. The pattern is then removed, rinsed in cold, running tap-water and dried. 4.5 Grey scale for assessing change in colour,

30、 complying with ISO105-A02. 5 Test specimen 5.1 If the textile to be tested is fabric, use a specimen measuring40mm 100mm. 5.2 If the textile to be tested is yarn, knit it into fabric and use a specimen measuring40mm 100mm, or make a wick of parallel lengths100mm long and about5mm in diameter, tied

31、near both ends. 5.3 If the textile to be tested is loose fibre, comb and compress enough of it to form a sheet measuring40mm 100mm. 6 Procedure 6.1 Carry out the operations described below in6.2 to6.5 with the test specimen and the test-control specimen in parallel, in separate baths. 6.2 Immerse th

32、e specimen in the sulfuric acid solution (4.2) for15min at room temperature (liquor ratio20:1). Squeeze it to leave in80% of its own mass of solution. 6.3 Dry the specimen by hanging it in an oven for30min, or longer if necessary, at60 C 2 C. Then bake it by heating for15min at105 C 2 C. 6.4 Rinse t

33、he specimen for5min in cold, running tap-water and then divide it into two equal parts. Dry one half by hanging it in air at a temperature not exceeding60 C. 6.5 Agitate the other half for30min at room temperature in the sodium carbonate solution (4.3) (liquor ratio40:1). Then rinse it for5min in co

34、ld, running tap-water and dry it by hanging it in air at a temperature not exceeding60 C. 6.6 Assess the effect on the unneutralized test-control specimen with the grey scale. Ifthechange in colour is not equal to the rating“2yellower” on the appropriate scale, the test has not been carried out corr

35、ectly, and the operations described in6.1 to6.5 inclusive shall berepeated with a fresh test specimen and a fresh test-control specimen.ENISO105-X02:1995 4 BSI 10-1999 6.7 Assess the change in colour of each half of the test specimen with the grey scale. 7 Test report The test report shall include t

36、he following particulars: a) the number and date of publication of this part of ISO 105 (i.e.ISO105-X02:1993); b) all details necessary for the identification of the sample tested; c) the numerical ratings for change in colour for both the rinsed and the neutralized portions of the test specimen.ENI

37、SO105-X02:1995 BSI 10-1999 5 Annex ZA (normative) Normative references to international publications with their relevant European publications This European Standard incorporates by dated or undated reference, provisions from other publications. These normative references are cited at the appropriat

38、e places in the text and the publications are listed hereafter. For dated references, subsequent amendments to or revisions of any of these publications apply to this European Standard only when incorporated in it by amendment or revision. For undated references the latest edition of the publication

39、 referred to applies. Publication Year Title EN Year ISO 105-A01 1994 Textiles Tests for colour fastness Part A01: General principles of testing EN ISO 105-A01 1994 ISO 105-A02 1993 Textiles Tests for colour fastness Part A02: Grey scale for assessing change in colour EN 20105-A02 19946 blankBSENISO

40、105-X02:1996 BSI 10-1999 List of references See national foreword.BS EN ISO 105-X02:1996 BSI 389 Chiswick High Road London W4 4AL BSIBritishStandardsInstitution BSI is the independent national body responsible for preparing BritishStandards. It presents the UK view on standards in Europe and at the

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