BS EN ISO 2815-2003 Paints and varnishes - Buchholz indentation test《涂料和清漆 布赫兹(Buchholz)压痕试验》.pdf

1、BRITISH STANDARD BS EN ISO 2815:2003 BS 3900-E9:2003 Paints and varnishes Buchholz indentation test The European Standard EN ISO 2815:2003 has the status of a British Standard ICS 87.040 BS EN ISO 2815:2003 This British Standard was published under the authority of the Standards Policy and Strategy

2、Committee on 20 August 2003 BSI 20 August 2003 ISBN 0 580 42485 5 National foreword This British Standard is the official English language version of EN ISO 2815:2003. It is identical with ISO 2815:2003. It supersedes BS EN ISO 2815:1998 which is withdrawn. The UK participation in its preparation wa

3、s entrusted to Technical Committee STI/10, Test methods for paints, which has the responsibility to: A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publications referr

4、ed to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI Electronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisi

5、ons of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers to understand the text; present to the responsible international/European committee any enquiries on the interpretation, o

6、r proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document comprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages

7、 ii to iv, pages 1 to 10, the Annex ZA page and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued since publication Amd. No. Date CommentsEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM ENISO2815 April2003 ICS87.040 Supers

8、edesENISO2815:1998 Englishversion PaintsandvarnishesBuchholzindentationtest(ISO 2815:2003) PeinturesetvernisEssaisdindentationBuchholz(ISO 2815:2003) BeschichtungsstoffeEindruckversuchnachBuchholz (ISO2815:2003) ThisEuropeanStandardwasapprovedbyCENon25March2003. CENmembersareboundtocomplywiththeCEN/

9、CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheManagementCentreortoanyCENmember. ThisEuropeanStandardexistsin

10、threeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheManagementCentrehasthesamestatusasthe official versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium,CzechRepublic,Denmark,Finlan

11、d,France,Germany,Greece, Hungary,Iceland,Ireland,Italy,Luxembourg,Malta,Netherlands,Norway,Portugal,Slovakia,Spain,Sweden,SwitzerlandandUn ited Kingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussels 2003CEN

12、Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.ENISO2815:2003EINESO82:5102(30E) 2 CORRECTED20030716 Foreword Thisdocument(ENISO2815:2003)hasbeenpreparedbyTechnicalCommitteeISO/TC35 “Paintsandvarnishes“incollaborationwithTechnicalCommitteeCEN/TC139“Paints

13、and varnishes“,thesecretariatofwhichisheldbyDIN. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationof anidenticaltextorbyendorsement,atthelatestbyOctober2003,andconflictingnational standardsshallbewithdrawnatthelatestbyOctober2003. ThisdocumentsupersedesENISO2815:1998.

14、AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsof thefollowingcountriesareboundtoimplementthisEuropeanStandard:Austria,Belgium,Czech Republic,Denmark,Finland,France,Germany,Greece,Hungary,Iceland,Ireland,Italy, Luxembourg,Malta,Netherlands,Norway,Portugal,Slovakia,Spai

15、n,Sweden,Switzerlandand theUnitedKingdom. Endorsementnotice ThetextofISO2815:2003hasbeenapprovedbyCENasENISO2815:2003withoutany modifications. NOTENormativereferencestoInternationalStandardsarelistedinAnnexZA(normative). ENISO2815:2003 Reference number ISO 2815:2003(E) OSI 3002INTERNATIONAL STANDARD

16、 ISO 2815 Second edition 2003-04-01 Paints and varnishes Buchholz indentation test Peintures et vernis Essais dindentation Buchholz ENISO2815:2003IS:5182 O3002(E) DPlcsid Fremia ihTs PDF file mya ctnoian emdebt dedyfepcaes. In ccacnadrow eitA hebods licnesilop gnic,y tihs file mirp eb yatnde iv rowe

17、b detu slahl ton ide ebtlnu deess teh typfecaes wihce era hml era deddebicsnede ti dna onstlalde t noeh comuptfrep reromign tide ehtin.g In wodlnidaot gnihs fil,e trapise atpecc tiereht nser ehnopsiiblity fo nto ifnriigngn Aebods licnesilop gnic.y ehT ISO tneClar Secrteirata caceptl on siibality in

18、this .aera Ai ebods a tedarmfo kra Aebod SystemI snctaropro.de teDials fo teh sfotwcudorp erats sut deo crtaee tihs PDF file cna f ebi dnuon tlareneG eh Ifnler oatit evt oeh file; tP ehDc-Frtaeino marapterew stpo ereimizde fro irptni.gn Evyre cera neeb sah takne tsne oeru taht teh file is siutlbae f

19、osu re yb ISO memdob rebeis. In tlnu ehikletneve y ttah lborp aem lertait gno it is f,dnuo plsaee ifnrom ttneC ehlar Secterirata ta teh serddaig sleb nevwo. ISO 3002 All irthgs erse.devr lnUeto sswrehise specified, on trap fo this lbupictaion maeb y cudorperro de tuilizi den yna form ro na ybm ynae,

20、s lecetrinoc ro mceinahcla, incliduntohp gcoiypodna gn micrfoilm, wittuoh repmissii now nritign from ietI rehSa Ot tsserdda eh ebolw or ISOs memreb i ydobn the cnuotfo yr ttseuqer ehe.r ISO cirypothg fofice saCe tsopale 65 eneG 1121-HC 02 av leT. 4 + 10 947 22 1 11 xaF0 947 22 14 + 9 74 E-mial coiry

21、pthgis.o gro We bwww.is.o groii ISO 3002 Allr ihgtsser edevrENISO2815:2003IS:5182 O3002(E) I SO 3002 All irhgts seredevr iiiContents Page Foreword iv 1 Scope 1 2 Normative references . 1 3 Principle . 1 4 Apparatus. 1 5 Sampling 4 6 Test panels 4 7 Procedure. 5 8 Calculation and expression of result

22、s 6 9 Precision 6 10 Test report 7 Annex A (informative) Buchholz indentation resistance 8 ENISO2815:2003IS:5182 O3002(E) iv I SO 3002 All irhgts seredevrForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The

23、work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-gover

24、nmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. Th

25、e main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote

26、. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 2815 was prepared by Technical Committee ISO/TC 35, Paints and varnishes, Subcommittee SC 9, Ge

27、neral test methods for paints and varnishes. This second edition cancels and replaces the first edition (ISO 2815:1973), which has been technically revised. The main changes are as follows: only indentation length is now determined; the conversion of indentation length to indentation resistance is d

28、escribed in an informative annex. ENISO2815:2003INTENRATIONAL TSANDADR IS:5182 O3002(E)I SO 3002 All irhgts seredevr 1Paints and varnishes Buchholz indentation test 1 Scope This International Standard describes a method for carrying out an indentation test on a single coating or multicoat system of

29、paint, varnish or related product, using a Buchholz indentor. The length of the indentation produced is indicative of the residual deformation of the coating. This indentation test is not suitable for products which contain a strong plasticizer. NOTE 1 Since the indentation test, like other physical

30、 tests on paints, gives results which can be dependent upon time, temperature and humidity, comparable results will only be obtained if the test is carried out under well-defined conditions. NOTE 2 Since the indentation depth depends upon the film thickness, the result obtained for the indentation l

31、ength is only valid if the coating thickness exceeds a certain minimum value (see Annex A). 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest editi

32、on of the referenced document (including any amendments) applies. ISO 1513, Paints and varnishes Examination and preparation of samples for testing ISO 1514, Paints and varnishes Standard panels for testing ISO 2808, Paints and varnishes Determination of film thickness ISO 15528, Paints, varnishes a

33、nd raw materials for paints and varnishes Sampling 3 Principle An indentor of specified size and shape is applied to the coating under defined conditions. The indentation length is measured in millimetres (see Annex A). 4 Apparatus 4.1 Indentation apparatus This is shown in Figure 1. It consists ess

34、entially of a rectangular block of metal, which forms the body of the instrument, an indentor and two pointed feet. ENISO2815:2003IS:5182 O3002(E) 2 I SO 3002 All irhgts seredevrFigure 1 Indentation apparatus (oblique underside view) The indentor is a sharpened sharp-edged metal wheel of hardened to

35、ol steel. The cross-section through its axis of rotation and its dimensions shall be as shown in Figure 2. Figures 3a) and 3b) show the shape of the indentation produced. Dimensions in millimetres Key 1 sharp edge 2 indentor 3 coating 4 substrate Figure 2 Buchholz indentor ENISO2815:2003IS:5182 O300

36、2(E) I SO 3002 All irhgts seredevr 3a) Shape of indentation b) Indentation length l (mm) and indentation depth h (m) (enlarged) Key 1 coating Figure 3 Shape of indentation The indentor and the two feet are so positioned in the body that, when the instrument is placed on a level surface, it is stable

37、, its upper surface is horizontal and the effective load upon the indentor is (500 5) g. 4.2 Measuring device A suitable device for measuring the length of the indentation consists of a microscope with 20 magnification and an eyepiece fitted with a graduated scale capable of reading to 0,1 mm. The a

38、rea of indentation shall be illuminated by means of a light source located so that the angle of incidence of the light exceeds 60, as shown in Figure 4. The microscope shall be positioned vertically over the illuminated area and focused to bring the shadow produced by the indentation (see Figures 4

39、and 5) and the graduated scale together. NOTE The position of the indentation mark can be located by means of a suitable template prepared from a triangular sheet of transparent plastics film (see Figure 6). Key 1 light source 2 microscope 3 indentation 4 coating 5 substrate Figure 4 Position of the

40、 light source and the microscope ENISO2815:2003IS:5182 O3002(E) 4 I SO 3002 All irhgts seredevrKey 1 indentation visible by its shadow 2 light source Figure 5 Shadow produced by the indentation Key 1 position of the indentation 2 position of the feet of the instrument Figure 6 Template to locate the

41、 position of the indentation 4.3 Timing device Use a stopwatch or other suitable timing device capable of measuring 30 s to the nearest 1 s. 5 Sampling Take a representative sample of the product to be tested (or of each product in the case of a multicoat system), as described in ISO 15528. The samp

42、le shall then be examined and prepared for testing as described in ISO 1513. 6 Test panels 6.1 Materials and dimensions Unless otherwise agreed, the test panels shall be of metal or glass conforming to the requirements of ISO 1514. The test panels shall be flat and free from distortion, and the surf

43、ace shall be free from any visible ridges or cracks. ENISO2815:2003IS:5182 O3002(E) I SO 3002 All irhgts seredevr 5Unless otherwise agreed, the test panels shall have minimum dimensions of 150 mm 100 mm and a thickness of not less than 0,75 mm. NOTE The test panels may be cut to size after coating a

44、nd drying, provided no distortion occurs. 6.2 Preparation and coating of panels The test panels shall be prepared in accordance with ISO 1514, unless otherwise agreed, and shall then be coated by the specified method with the product or system under test to the specified film thickness limits. Any v

45、ariation from the requirements of ISO 1514 shall be noted in the test report (see Clause 10). 6.3 Drying and conditioning of the test panels The coated test panels shall be dried (or stoved) and aged (if applicable) for the specified time and under the specified conditions and, unless otherwise spec

46、ified, shall be conditioned at a temperature of (23 2) C and a relative humidity of (50 5) % for a minimum of 16 h. The test procedure shall then be carried out as soon as possible. 6.4 Thickness of coating The average thickness, in micrometres, of the dry coating in the region to be tested shall be

47、 determined by the method specified, using one of the procedures specified in ISO 2808. 7 Procedure 7.1 Ambient conditions The test shall be carried out at a temperature of (23 2) C and a relative humidity of (50 5) %, unless otherwise agreed. 7.2 Determination of indentation length Place the test p

48、anel, paint film uppermost, on a firm horizontal surface. Take the indentation apparatus (4.1) and place it gently and without any tilting or lateral movement on the test panel, leave the indentor in position for (30 1) s and remove it carefully. When the apparatus is put in place, the feet of the apparatus shall first be allowed to