BS EN ISO 17227-2003 Leather - Physical and mechanical tests - Determination of dry heat resistance of leather《皮革 物理和机械试验 皮革耐干热的测定》.pdf

1、BRITISH STANDARD BS EN ISO 17227:2002 Incorporating Corrigendum No. 1 Leather Physical and mechanical tests Determination of dry heat resistance of leather The European Standard EN ISO 17227:2002 has the status of a British Standard ICS 59.140.30 BS EN ISO 17227:2002 This British Standard, having be

2、en prepared under the direction of the Materials and Chemicals Sector Policy and Strategy Committee, was published under the authority of the Standards Policy and Strategy Committee on 15 January 2003 BSI 15 September 2003 ISBN 0 580 41096 X National foreword This British Standard is the official En

3、glish language version of EN ISO 17227:2002. It is identical with ISO 17227:2002. The UK participation in its preparation was entrusted to Technical Committee TCI/69, Footwear and leather, which has the responsibility to: A list of organizations represented on this committee can be obtained on reque

4、st to its secretary. Cross-references The British Standards which implement international or European publications referred to in this document may be found in the BSI Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Search” facility of the BSI El

5、ectronic Catalogue or of British Standards Online. This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. Compliance with a British Standard does not of itself confer immunity from legal obligations. aid enquirers t

6、o understand the text; present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; monitor related international and European developments and promulgate them in the UK. Summary of pages This document c

7、omprises a front cover, an inside front cover, the EN ISO title page, the EN ISO foreword page, the ISO title page, pages ii to iv, pages 1 to 4, the Annex ZA page and a back cover. The BSI copyright notice displayed in this document indicates when the document was last issued. Amendments issued sin

8、ce publication Amd. No. Date Comments 14708 Corrigendum No. 1 15 September 2003 Correction to the EN ISO Foreword page and incorporating the Annex ZA pageEUROPEANSTANDARD NORMEEUROPENNE EUROPISCHENORM ENISO17227 December2002 ICS59.140.30 Englishversion LeatherPhysicalandmechanicaltestsDeterminationo

9、fdry heatresistanceofleather(ISO17227:2002) CuirEssaisphysiquesetmcaniquesDterminationde larsistanceducuirlachaleursche(ISO17227:2002) LederPhysikalischeundmechanischePrfungen BestimmungdesTrockenhitzewiderstandesvonLeder (ISO17221:2002) ThisEuropeanStandardwasapprovedbyCENon9September2002. CENmembe

10、rsareboundtocomplywiththeCEN/CENELECInternalRegulationswhichstipulatetheconditionsforgivingthisEurope an Standardthestatusofanationalstandardwithoutanyalteration.Uptodatelistsandbibliographicalreferencesconcernings uchnational standardsmaybeobtainedonapplicationtotheManagementCentreortoanyCENmember.

11、 ThisEuropeanStandardexistsinthreeofficialversions(English,French,German).Aversioninanyotherlanguagemadebytra nslation undertheresponsibilityofaCENmemberintoitsownlanguageandnotifiedtotheManagementCentrehasthesamestatusasthe official versions. CENmembersarethenationalstandardsbodiesofAustria,Belgium

12、,CzechRepublic,Denmark,Finland,France,Germany,Greece, Iceland,Ireland,Italy,Luxembourg,Malta,Netherlands,Norway,Portugal,Spain,Sweden,SwitzerlandandUnitedKingdom. EUROPEANCOMMITTEEFORSTANDARDIZATION COMITEUROPENDENORMALISATION EUROPISCHESKOMITEEFRNORMUNG ManagementCentre:ruedeStassart,36B1050Brussel

13、s 2002CEN Allrightsofexploitationinanyformandbyanymeansreserved worldwideforCENnationalMembers. Ref.No.ENISO17227:2002EINESO71:722200(2E) 2 CORRECTED20030827 Foreword Thisdocument(ENISO17227:2002)hasbeenpreparedbyTechnicalCommitteeCEN/TC289 “Leather“,thesecretariatofwhichisheldbyUNI,incollaborationw

14、iththeInternationalUnionof LeatherTechnologistsandChemistsSocieties(IULTCS). ItisbasedonMethodIUP35oftheInternationalUnionofLeatherTechnologistsandChemists Societies. ThisEuropeanStandardshallbegiventhestatusofanationalstandard,eitherbypublicationof anidenticaltextorbyendorsement,atthelatestbyJune20

15、03,andconflictingnational standardsshallbewithdrawnatthelatestbyJune2003. AccordingtotheCEN/CENELECInternalRegulations,thenationalstandardsorganizationsof thefollowingcountriesareboundtoimplementthisEuropeanStandard:Austria,Belgium,Czech Republic,Denmark,Finland,France,Germany,Greece,Iceland,Ireland

16、,Italy,Luxembourg, Malta,Netherlands,Norway,Portugal,Spain,Sweden,SwitzerlandandtheUnitedKingdom. Endorsementnotice ThetextofISO17227:2002hasbeenapprovedbyCENasENISO17227:2002withoutany modifications. NOTENormativereferencestoInternationalStandardsarelistedinAnnexZA(normative). ENISO17227:2002 Refer

17、ence number ISO 17227:2002(E) IULTCS/IUP 35INTERNATIONAL STANDARD ISO 17227 IULTCS/IUP 35 First edition 2002-12-15 Leather Physical and mechanical tests Determination of dry heat resistance of leather Cuir Essais physiques et mcaniques Dtermination de la rsistance du cuir la chaleur sche ENISO17227:

18、2002ENISO17227:2002iiISO 17227:0022(E) I SO 2002 All irthgs ersedevr iiiContents Page Foreword iv 1Scope1 2Normative references1 3Principle1 4Apparatus.1 5Sampling andsamp lep reparation.1 6Testcondition s2 7Procedure.2 8Expressiono f results3 9Testrepor t4 ENISO17227:2002iiiIS:72271 O2002(E) vi I S

19、O 2002 All irthgs ersedevrForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested

20、in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commi

21、ssion (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards adopted by the technica

22、l committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shal

23、l not be held responsible for identifying any or all such patent rights. ISO 17227 was prepared by the Physical Test Commission of the International Union of Leather Technologists and Chemists Societies (IUP Commission, IULTCS) in collaboration with the European Committee for Standardization (CEN) T

24、echnical Committee CEN/TC 289, Leather, the secretariat of which is held by UNI, in accordance with the Agreement on technical cooperation between ISO and CEN (Vienna Agreement). It is based on IUP 35 originally titled “Heat resistance of industrial glove leather” and published in J. Soc. Leather Te

25、ch. Chem. 73, p. 62, (1989) and declared an official method of the IULTCS in 1989. This updated version was published in J. Soc. Leather Tech. Chem. 84, p. 373, (2000) and reconfirmed as an official method in March 2001. The same principle is used but the text has been updated and includes the numbe

26、r of test pieces to be taken. ENISO17227:2002ivINTERNATIONAL STANDADR ISO 12727:0022(E)I SO 2002 All irthgs ersedevr 11Scope ThisInternationalStandardspecifiesa methodofdeterminingthedryheatresistanceofconditionedleathers.Itis applicable to all leathers. ISO2 418LeatherChemical,physicalandmechanical

27、andfastnesstests Samplinglocation ISO2 419LeatherPhysicalandmechanicaltestsSamplepreparationandconditioning 3Principle Aconditionedtestpieceisheatedinanovenandtheshrinkagedeterminedandchangesinflexibilityareassessed manually. 4Apparatus 4.1 Oven,fittedwithacentralrackcapableofmaintainingtemperatures

28、of150 C 5 C,200 C 5 Cand 250 C 5 C. 4.2 Verniercallipers ,readingto0,1mm. 4.3 Support,forthetestpiecewhileitisbeingheatedintheoven,tominimisecontactwiththeovenrack,for exampleawiregridorpipeclaytriangle. 4.4 Stopclock ,readableto1s. 4.5Pressk nife, the inner wallw hich isa square of side 100 mm 1 mm

29、a s specifiedi n ISO2 419. 5 Samplingandsamplepreparation 5.1SampleinaccordancewithISO2418.From the sample, cutthreetestpiecesforeachoftheconditions required by applyingth ep ress knife (4.5)tot heg rain surface, ifdi stinguishable. NOTEIf there is a requirement form oret hant wohi des or skins tob

30、ete sted in one batch,t hen onlyo ne test piecenee d be takenfromeachhideorskin,providedthattheoveralltotalisnotlessthanthreetestpieces. 5.2Usinganindeliblemarker,markmeasurementreferencepointsA,B,CandDonthetestpieceinthe positionsshowninFigure1. 2 Normative references Leather Physical and mechanica

31、l tests Determination of dry heat resistance of leather The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) ap

32、plies. ENISO17227:20021ISO 17227:0022(E) 2 I SO 2002 All irthgs ersedevrFigure1Locationofmeasurementreferencepointsonatestpiece(alldimensionsinmillimetres1mm) 5.3Condition the test pieces ina ccordance with ISO 2419. 6Test conditions 6.1 Oventemperature Theoventemperatureshouldbeselectedfromoneofthe

33、following: 150 C 5 C 200 C 5 C 250 C 5 C 6.2 Testperiod Thetestperiodshouldbeselectedfromoneofthefollowing: 15min 0,5min 30min 0,5min 60min 0,5min 7Procedure 7.1 Usingtheverniercallipers(4.2),measurethedistancesABandCDoneachtestpiecetothenearest0,1mm andcalculatethemean.SimilarlymeasurethedistancesA

34、CandBDandcalculatethemean. 7.2 Preheattheoven(4.1)tooneofthetemperaturesgivenin6.1.Placethetestpieceonthesupport(4.3)in thecentreoftheoven. 7.3 Afteroneofthetestperiodsgivenin6.2, removethetestpiecefromtheovenandallowthetestpieceto cool. 7.4 Repeat7.2and7.3 ,usingothertesttemperaturesandperiodsasreq

35、uired,usingafreshtestpieceforeach additionaltest. ENISO17227:20022ISO 17227:0022(E) I SO 2002 All irthgs ersedevr 37.5Recondition the test pieces for48 hi na ccordance with ISO2 419. 7.6 Usingtheverniercallipers(4.2),remeasurethedistanceAB,CD,ACandBDandcalculatethemeanasin 7.1. NOTE1 Adryheatstabili

36、tytestat250 Cisanextremelystringenttestonanorganicmaterialsuchasleather.Greatcare shouldbeexercisedinperformingthistestat250 Casitcancausetheleathertosmoulder.Thisriskishigherforleatherswith ahighcontentofoilsandfats. NOTE2 Leathercangiveofffumeswhenheatedundertheconditionsin6.1and6.2. Thetestshould

37、onlybecarriedoutina wellventilatedareatoprotectoperatorsfromtheeffectofthefumes. 7.7 Noteanyvisualchangesinthetestpiece,suchasdistortionorcharringandassessanychangesinflexibility manually. 8 Expressionofresults 8.1 Calculatetheoriginalarea, A 1 ,boundedbythepointsABCDonthetestpiece,asfollows: 2 2 1

38、1 1 1 1 d b c a A (1) where a 1 ,b 1 , c 1 ,d 1 arerespectivelythevaluesofthedimensionsAB,BD,CD,AC(seeFigure1),measuredbeforethe test. Calculatetheareaaftertest, A 2 ,boundedbythepointsABCDonthetestpiece,asfollows: 2 2 2 2 2 2 2 d b c a A (2) where a 2 , b 2 , c 2 , d 2 arerespectivelythevaluesofthe

39、dimensionsAB,BD,CD,AC(seeFigure1),measuredafterthetest. Calculatethepercentagelossofarea(shrinkage) S,usingtheequation: 100 1 2 1 A A A S (3) where A 1 istheoriginalarea,calculatedfrom(1); A 2 istheareaaftertest,calculatedfrom(2). 8.2 Recordanyvisualchangesinthetestpiece,suchasdistortionorcharring.

40、8.3 Recordanychangesintheflexibilityofthetestpiece,assessedmanually. ENISO17227:20023ISO 17227:0022(E) 4 I SO 2002 All irthgs ersedevr9 Testreport Thetestreportshallincludethefollowing: a) referencetot his International Standard, i.e. ISO 17227:2002; b) thetestconditions; c) the percentage lossi na

41、rea ofea ch testp iece, as calculated in 8.1; d) detailso fa ny visual changeso r changes in flexibility; e)thestandardatmosphereusedforconditioningandtestingasgiveninISO2419(i.e.,20C/65% relative humidityo r 23C/5 0 % relative humidity); f) any deviations fromthe method specified in this Internatio

42、nal Standard; g) fulld etails forid entificationo fthe sample and any deviation fromIS O 2418 with respectto sampling. ENISO17227:20024INESO71:722200(2E) 3 AnnexZA (normative) Normativereferencestointernationalpublications withtheirrelevantEuropeanpublications ThisEuropeanStandardincorporatesbydated

43、orundatedreference,provisionsfromother publications.Thesenormativereferencesarecitedattheappropriateplacesinthetextandthe publicationsarelistedhereafter.Fordatedreferences,subsequentamendmentstoorrevisionsof anyofthesepublicationsapplytothisEuropeanStandardonlywhenincorporatedinitby amendmentorrevis

44、ion.Forundatedreferencesthelatesteditionofthepublicationreferredto applies(includingamendments). NOTEWhereanInternationalPublicationhasbeenmodifiedbycommonmodifications,indicated by(mod.),therelevantEN/HDapplies. Publication Year Title EN Year ISO2418 2002 LeatherChemical,physical andmechanicalandfa

45、stness testsSamplinglocation ENISO2418 2002 ISO2419 2002 LeatherPhysicaland mechanicaltestsSample preparationandconditioning ENISO2419 2002 ENISO17227:2002BS EN ISO 17227:2002 BSI 389 Chiswick High Road London W4 4AL BSI British Standards Institution BSI is the independent national body responsible for p