1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS ISO 13124:2011Fine ceramics (advancedceramics, advanced technicalceramics) Test method forinterfacial bond strength ofceramic materialsBS ISO 13124:2011 BRITISH STANDARDNation
2、al forewordThis British Standard is the UK implementation of ISO 13124:2011.The UK participation in its preparation was entrusted to TechnicalCommittee RPI/13, Advanced technical ceramics.A list of organizations represented on this committee can beobtained on request to its secretary.This publicatio
3、n does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. BSI 2011ISBN 978 0 580 66975 0ICS 81.060.30Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authorit
4、y of theStandards Policy and Strategy Committee on 30 June 2011.Amendments issued since publicationDate Text affectedBS ISO 13124:2011Reference numberISO 13124:2011(E)ISO 2011INTERNATIONAL STANDARD ISO13124First edition2011-05-15Fine ceramics (advanced ceramics, advanced technical ceramics) Test met
5、hod for interfacial bond strength of ceramic materials Cramiques techniques Mthode dessai pour la rsistance de linterface des matriaux cramiques BS ISO 13124:2011ISO 13124:2011(E) COPYRIGHT PROTECTED DOCUMENT ISO 2011 All rights reserved. Unless otherwise specified, no part of this publication may b
6、e reproduced or utilized in any form or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISOs member body in the country of the requester. ISO copyright office Case postale 56 CH-1211 Geneva 20 Tel. +
7、41 22 749 01 11 Fax + 41 22 749 09 47 E-mail copyrightiso.org Web www.iso.org Published in Switzerland ii ISO 2011 All rights reservedBS ISO 13124:2011ISO 13124:2011(E) ISO 2011 All rights reserved iiiContents Page Foreword iv 1 Scope1 2 Normative references1 3 Terms and definitions .1 4 Symbols and
8、 abbreviated terms 3 5 Principle3 6 Apparatus.5 6.1 Testing machine 5 6.2 Data acquisition.5 6.3 Dimension-measuring device 5 6.4 Testing fixture5 7 Test pieces .7 7.1 Test-piece size .7 7.2 Test-piece preparation7 8 Test procedure.8 8.1 Test mode and rate8 8.2 Preparation of test pieces.8 8.3 Measu
9、rements of the tensile bond strength.8 8.4 Measurements of the shear bond strength.9 8.5 Measurement of the cross-bonded area .10 8.6 Post test10 9 Calculation of results 10 9.1 Interfacial tensile bond strength10 9.2 Interfacial shear bond strength11 10 Test report12 Bibliography13 BS ISO 13124:201
10、1ISO 13124:2011(E) iv ISO 2011 All rights reservedForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each
11、 member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the Internationa
12、l Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International Standards. Draft International Standards
13、 adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this document may be the subject of
14、 patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 13124 was prepared by Technical Committee ISO/TC 206, Fine ceramics. BS ISO 13124:2011INTERNATIONAL STANDARD ISO 13124:2011(E) ISO 2011 All rights reserved 1Fine ceramics (advanced ceramics, advanced
15、 technical ceramics) Test method for interfacial bond strength of ceramic materials 1 Scope This International Standard specifies a test method for determining the interfacial tensile and shear bond strength of ceramic-ceramic, ceramic-metal, and ceramic-glass joining at ambient temperature by compr
16、ession tests on cross-bonded test pieces. Methods for test-piece preparation, test modes and rates (load rate or displacement rate), data collection and reporting procedures are addressed. This International Standard applies primarily to ceramic materials, including monolithic fine ceramics and whis
17、ker-, fibre- or particulate-reinforced ceramic composites. This test method can be used for materials research, quality control, and characterization and design data generation purposes. 2 Normative references The following referenced documents are indispensable for the application of this document.
18、 For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 3611:2010, Geometrical product specifications (GPS) Dimensional measuring equipment: Micrometers for external measurements Design and m
19、etrological characteristics ISO 7500-1:2004, Metallic materials Verification of static uniaxial testing machines Part 1: Tension/compression testing machines Verification and calibration of the force-measuring system ISO 14704:2008, Fine ceramics (advanced ceramics, advanced technical ceramics) Test
20、 method for flexural strength of monolithic ceramics at room temperature 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 fine ceramic (advanced ceramic, advanced technical ceramic) highly engineered, high-performance predominately non-metalli
21、c, inorganic, ceramic material having specific functional attributes BS ISO 13124:2011ISO 13124:2011(E) 2 ISO 2011 All rights reserved3.2 cross-bonded sample test sample in the form of a symmetrical cross, which is prepared by joining two rectangular bars with the same shape and size NOTE 1 See Figu
22、re 1. NOTE 2 The two bars joined to form the cross-bonded sample may be the same or different materials. NOTE 3 The approach used for joining can be any chemical or physical bonding. NOTE 4 The two bars should be joined perpendicularly and symmetrically within 1 ( = 90 1). hbFigure 1 Schematic diagr
23、am of the cross-bonded samples 3.3 tensile failure load maximum tensile load applied to the interface during a tensile bond strength test 3.4 tensile bond strength maximum mean tensile stress applied to the interface during a bond strength test NOTE The tensile bond strength is calculated using the
24、tensile failure load and the bonded area. 3.5 shear failure load maximum shear load applied to the interface during a shear test of the cross-bonded sample 3.6 shear bond strength maximum mean shear stress applied to the interface during a shear bond strength test NOTE The shear bond strength is cal
25、culated using the shear failure load and the shear loaded area. BS ISO 13124:2011ISO 13124:2011(E) ISO 2011 All rights reserved 34 Symbols and abbreviated terms For the purposes of this document, the symbols and designations given in Table 1 apply. Table 1 Symbols and designations Symbol Designation
26、 Unit References l Test-piece length mm Table 2 h Test-piece thickness mm Figure 1, Table 2 b Test-piece width mm Figure 1, Table 2 Right angle of cross-bonded sample Figure 1 D Diameter of the ball in pressure head mm Figure 3 tTensile bond strength MPa Equation 1 Shear bond strength MPa Equation 4
27、 PcCritical load to debond N Equations 1, 4 A1Tensile loaded area mm2Equation 1 A2Shear loaded area mm2Equation 4 n Number of valid tests 1 Equations 2, 3, 5, 6 t Mean tensile bond strength MPa Equation 2 Mean shear bond strength MPa Equation 5 s Standard deviation MPa Equations 3, 6 5 Principle A c
28、ross-bonded sample is loaded in compression which yields tensile or shear stress in the interface until the occurrence of debonding in the interface. Two different forms of mounting the cross-bonded sample in a fixture are designed to measure the interfacial tensile and shear bond strength, respecti
29、vely. In the case of the former, a uniaxial tensile stress is generated when the testing sample is subjected to a compressive load, as shown in Figure 2 a). For the latter, a cross-bonded sample is loaded in compression to induce failure by shear at the interface, as shown in Figure 2 b). The test i
30、s usually performed at a constant cross-head displacement rate. The load at fracture and the bonded area are used to compute the tensile and shear bond strength. BS ISO 13124:2011ISO 13124:2011(E) 4 ISO 2011 All rights reserved1FqqFa) Schematic diagram of loading, supporting and bonded area for cros
31、s-bonded sample in the test of the tensile bond strength 1qqFb) Schematic diagram of loading, supporting and bonded area for cross-bonded sample in the test of the shear bond strength Key 1 loading, supporting and bonded area F applied load q uniform resultant stress on the supporting surfaces Figur
32、e 2 Schematic diagram of measuring the tensile and shear bond strength using the cross-bonded test piece subjected to compressive load BS ISO 13124:2011ISO 13124:2011(E) ISO 2011 All rights reserved 56 Apparatus 6.1 Testing machine A suitable testing machine capable of applying a uniform cross-head
33、speed shall be used. The testing machine shall be in accordance with ISO 7500-1:2004, Class 1, with an accuracy of 1 % of the indicated load during compression or tension tests. 6.2 Data acquisition Obtain the maximum load and at least an autographic record of the applied load versus cross-head disp
34、lacement or versus testing time. Use either analog chart recorders or digital data acquisition systems. Recording devices shall be accurate to within 1 % of the selected range of the testing equipment including the readout unit, and have a minimum data acquisition rate of 10 Hz with a response of 50
35、 Hz deemed more than sufficient. 6.3 Dimension-measuring device Micrometers and other devices used for measuring linear dimensions must be accurate to at least 0,01 mm and shall be in accordance with ISO 3611. Alternative dimension-measuring instruments may be used provided that they have a resoluti
36、on of 0,01 mm or finer. 6.4 Testing fixture The sketch of the testing fixtures is shown in Figure 3. To avoid unsymmetrical stress in the sample, the top of the pressure head is in the centre point of the pressure head, and it is arc shaped at two perpendicular directions, as shown in Figure 3 a). A
37、lternatively, a bearing ball inlayed in the centre of a rectangular pressure head can be used, as shown in Figure 3 b). Thus, a point-contact at the top of the pressure head can be realized in the compressive process. The supporting fixture shall be suitable and moveable, and the width of the groove
38、 such that the cross-bonded sample can be inserted into the fixture freely and with a smooth contact, as shown in Figure 3 c). The fixture shall remain elastic over the load ranges used. The fixture should be made of a hard metal with elastic modulus over 200 GPa and hardness (HV) over 3 GPa. The pr
39、essure head is designed for applying the tensile load in the interface during the tensile bonding strength test, not for the shear bond strength test. The weight of the pressure head should be added into the final load for calculating the strength. To avoid the unsymmetrical tensile stress, it is re
40、commended that the width of the pressure head should be equal to that of the test piece, e.g. b = b3. The parallelism tolerance on opposite longitudinal faces of the supporting fixture shall not exceed 0,01 mm, and both the upper and lower surfaces should be smooth planes. NOTE While the cross-bonde
41、d sample is put into the testing fixture, as shown in Figures 5 and 6, the inside bar would be in smooth contact with two inner surfaces of the fixture, without friction when it moves. The thickness of the pressure head should be a little smaller than the width of the groove, and the depth of the gr
42、oove in the pressure head is larger than the thickness of the bar, e.g. b3h. BS ISO 13124:2011ISO 13124:2011(E) 6 ISO 2011 All rights reservedb3c2c1h3h2a) Pressure head used to apply load during tensile bonding strength tests h4h3h2c2c1b3Db) Alternative pressure head used to apply load during tensil
43、e bond strength tests L1h1L2b2b1c) Supporting fixture for both tensile and shear bond strength tests Figure 3 Schematic illustration of the testing fixtures BS ISO 13124:2011ISO 13124:2011(E) ISO 2011 All rights reserved 77 Test pieces 7.1 Test-piece size A rectangular test bar with a square or rect
44、angular section shall be prepared before bonding, as shown in Figure 4. The angles of the cross-section should be right-angles within 1. Table 2 shows the recommended dimensions of the bars with the section size of 4 mm 4 mm, and the length should be larger than 12 mm. The parallelism tolerance on t
45、he opposite longitudinal face is 0,015 mm. All of the bar samples shall not be chamfered. lhbFigure 4 Schematic illustrations of the rectangular test pieces Table 2 Recommended dimensions for cross-bonded sample and fixture Dimensions in millimetres Dimension Description Value Tolerance l b h Length
46、 of the bar Width of the bar Thickness of the bar 12 4 4 0,5 0,1 0,1 NOTE Preferably, two rectangular bars with the same dimension are joined for preparing the cross-sectional samples. The phase compositions of the two rectangular samples can be the same or different. 7.2 Test-piece preparation 7.2.
47、1 General This International Standard allows several options for test-piece preparation. For chemical diffusion joining, the contact surfaces of the bars are polished up to at least 1200# SiC paper, and then cleaned. For strength evaluation of glues, the surface of the test piece does not need polis
48、hing. Each pair of bars that need to bond (sometimes of the same material) is joined to form a symmetrical cross, as shown in Figure 1. The technique used for joining, depending on the aims of measurement, can be chemical or physical bonding. 7.2.2 Test-piece storage The test pieces shall be handled
49、 with care to avoid the introduction of damage after test-piece preparation. Test pieces shall be stored separately and not allowed to impact or scratch each other. 7.2.3 Number of test pieces A minimum of 10 test pieces is required for the purpose of estimating the mean interfacial tensile bond strength or interfacial shear bond strength. A minimum of 30 test pieces is recommended if a statistical strength analysis (e.g. a Weibull analysis) is demanded. The use of 30 test pie
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