BS ISO 19983-2017 Rubber Determination of precision of test methods《橡胶 试验方法精度的测定》.pdf

1、Rubber Determination of precision of test methodsBS ISO 19983:2017BSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06 ISO 2017Rubber Determination of precision of test methodsCaoutchouc Dtermination de la fidlit des mthodes dessaiINTERNATIONAL STANDARDISO19983First edit

2、ion2017-07Reference numberISO 19983:2017(E)National forewordThis British Standard is the UK implementation of ISO 19983:2017.The UK participation in its preparation was entrusted to Technical Committee PRI/22, Testing and analysis of rubber.A list of organizations represented on this committee can b

3、e obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2017 Published by BSI Standards Limited 2017ISBN 978 0 580 88039 1ICS 83.060Compliance

4、with a British Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of the Standards Policy and Strategy Committee on 30 September 2017.Amendments/corrigenda issued since publicationDate Text affectedBRITISH STANDARDBS ISO 19983:2017 ISO 2017

5、Rubber Determination of precision of test methodsCaoutchouc Dtermination de la fidlit des mthodes dessaiINTERNATIONAL STANDARDISO19983First edition2017-07Reference numberISO 19983:2017(E)BS ISO 19983:2017ISO 19983:2017(E)ii ISO 2017 All rights reservedCOPYRIGHT PROTECTED DOCUMENT ISO 2017, Published

6、 in SwitzerlandAll rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior written permission. Permission c

7、an be requested from either ISO at the address below or ISOs member body in the country of the requester.ISO copyright officeCh. de Blandonnet 8 CP 401CH-1214 Vernier, Geneva, SwitzerlandTel. +41 22 749 01 11Fax +41 22 749 09 47copyrightiso.orgwww.iso.orgBS ISO 19983:2017ISO 19983:2017(E)ii ISO 2017

8、 All rights reservedCOPYRIGHT PROTECTED DOCUMENT ISO 2017, Published in SwitzerlandAll rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on the int

9、ernet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below or ISOs member body in the country of the requester.ISO copyright officeCh. de Blandonnet 8 CP 401CH-1214 Vernier, Geneva, SwitzerlandTel. +41 22 749 01 11Fax +41 22 749 09 47copy

10、rightiso.orgwww.iso.orgISO 19983:2017(E)Foreword ivIntroduction v1 Scope . 12 Normative references 13 Terms and definitions . 14 Symbols and abbreviated terms . 25 Interlaboratory test programme . 36 Procedures 36.1 Application . 36.2 Repeatability conditions . 36.3 Day-to-day repeatability conditio

11、ns . 46.4 Reproducibility conditions . 46.5 Testing elements 46.6 Planning 46.7 Methodology . 56.7.1 Method A . 56.7.2 Method B . 56.8 Treatment of outliers . 67 Report 6Annex A (normative) Calculations for method A . 7Annex B (normative) Calculations for method B 10Annex C (normative) Calculating t

12、he h and k values (Mandels statistics) 12Annex D (informative) Example of general precision determination .14Annex E (informative) Guidance for using precision results19Bibliography .21 ISO 2017 All rights reserved iiiContents PageBS ISO 19983:2017ISO 19983:2017(E)ForewordISO (the International Orga

13、nization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been establis

14、hed has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization

15、.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with th

16、e editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/ directives).Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any pa

17、tent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www .iso .org/ patents).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.

18、For an explanation on the voluntary nature of standards, the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adherence to the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following URL: ww

19、w .iso .org/ iso/ foreword .html.This document was prepared by Technical Committee ISO/TC 45, Rubber and rubber products, Subcommittee SC 2, Testing and analysis.iv ISO 2017 All rights reservedBS ISO 19983:2017ISO 19983:2017(E)ForewordISO (the International Organization for Standardization) is a wor

20、ldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on

21、 that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this d

22、ocument and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Direc

23、tives, Part 2 (see www .iso .org/ directives).Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the deve

24、lopment of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www .iso .org/ patents).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the voluntary na

25、ture of standards, the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adherence to the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see the following URL: www .iso .org/ iso/ foreword .html.This

26、document was prepared by Technical Committee ISO/TC 45, Rubber and rubber products, Subcommittee SC 2, Testing and analysis.iv ISO 2017 All rights reserved ISO 19983:2017(E)IntroductionThe procedures used for several years by ISO/TC 45/SC 2 for estimating precision of test methods by means of interl

27、aboratory tests (ISO/TR 9272) were closely related to ASTM D4483. ISO/TR 9272 was found to have serious flaws which users were using work-arounds to counteract. It became clear that ISO/TR 9272 needed to be replaced and it was concluded that the best option was to base a new standard on ISO 5725 (al

28、l parts) with specific choices and variations of procedures to suit the particular requirements of rubbers. ISO 2017 All rights reserved vBS ISO 19983:2017Rubber Determination of precision of test methods1 ScopeThis document provides guidelines and specifies requirements for estimating the precision

29、 of rubber test methods by means of interlaboratory test programmes based on the procedures given in ISO 5725 (all parts).2 Normative referencesThe following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated ref

30、erences, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 3534-1, Statistics Vocabulary and symbols Part 1: General statistical terms and terms used in probabilityISO 3534-2, Statistics Vocabulary and symbols

31、 Part 2: Applied statisticsISO 5725-1:1994, Accuracy (trueness and precision) of measurement methods and results Part 1: General principles and definitionsISO 5725-2, Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and

32、reproducibility of a standard measurement methodISO 5725-3, Accuracy (trueness and precision) of measurement methods and results Part 3: Intermediate measures of the precision of a standard measurement methodISO 5725-4, Accuracy (trueness and precision) of measurement methods and results Part 4: Bas

33、ic methods for the determination of the trueness of a standard measurement methodISO 5725-5, Accuracy (trueness and precision) of measurement methods and results Part 5: Alternative methods for the determination of the precision of a standard measurement methodISO 5725-6, Accuracy (trueness and prec

34、ision) of measurement methods and results Part 6: Use in practice of accuracy values3 Terms and definitionsFor the purposes of this document, the terms and definitions given in ISO 3534-1, ISO 3534-2, ISO 5725 (all parts), and the following apply.ISO and IEC maintain terminological databases for use

35、 in standardization at the following addresses: IEC Electropedia: available at h t t p :/ www .electropedia .org/ ISO Online browsing platform: available at h t t p :/ www .iso .org/ obp 3.1day-to-day repeatabilityprecision under the conditions where independent test results are obtained with the sa

36、me method on identical test items in the same laboratory by the same operator using the same equipmentNote 1 to entry: The time interval between repeated tests is normally between one and seven days.INTERNATIONAL STANDARD ISO 19983:2017(E) ISO 2017 All rights reserved 1BS ISO 19983:2017Rubber Determ

37、ination of precision of test methods1 ScopeThis document provides guidelines and specifies requirements for estimating the precision of rubber test methods by means of interlaboratory test programmes based on the procedures given in ISO 5725 (all parts).2 Normative referencesThe following documents

38、are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 3534-1, Statistics

39、 Vocabulary and symbols Part 1: General statistical terms and terms used in probabilityISO 3534-2, Statistics Vocabulary and symbols Part 2: Applied statisticsISO 5725-1:1994, Accuracy (trueness and precision) of measurement methods and results Part 1: General principles and definitionsISO 5725-2, A

40、ccuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement methodISO 5725-3, Accuracy (trueness and precision) of measurement methods and results Part 3: Intermediate measures of the pr

41、ecision of a standard measurement methodISO 5725-4, Accuracy (trueness and precision) of measurement methods and results Part 4: Basic methods for the determination of the trueness of a standard measurement methodISO 5725-5, Accuracy (trueness and precision) of measurement methods and results Part 5

42、: Alternative methods for the determination of the precision of a standard measurement methodISO 5725-6, Accuracy (trueness and precision) of measurement methods and results Part 6: Use in practice of accuracy values3 Terms and definitionsFor the purposes of this document, the terms and definitions

43、given in ISO 3534-1, ISO 3534-2, ISO 5725 (all parts), and the following apply.ISO and IEC maintain terminological databases for use in standardization at the following addresses: IEC Electropedia: available at h t t p :/ www .electropedia .org/ ISO Online browsing platform: available at h t t p :/

44、www .iso .org/ obp 3.1day-to-day repeatabilityprecision under the conditions where independent test results are obtained with the same method on identical test items in the same laboratory by the same operator using the same equipmentNote 1 to entry: The time interval between repeated tests is norma

45、lly between one and seven days.INTERNATIONAL STANDARD ISO 19983:2017(E) ISO 2017 All rights reserved 1 ISO 19983:2017(E)3.2type 1 precisionprecision determined directly on a target materialNote 1 to entry: Prepared test pieces or test portions of the target material (class of elements) drawn from a

46、homogeneous source are tested, with no processing or other operations required prior to testing.3.3type 2 precisionprecision determined indirectly for a target materialNote 1 to entry: The target material is usually combined with a number of homogeneous ancillary materials to form a composite materi

47、al and testing is conducted on samples of this and the property response of the target material is determined.4 Symbols and abbreviated termsDijday-to-day effect, the day-to-day variance component of which is D2h values Mandels between-laboratory consistency test statistick values Mandels within-lab

48、oratory consistency test statisticLibetween-laboratory effect, the between-laboratory variance component of which is L2Mijkrepeatability effect, the repeatability variance component of which is M2n number of measurementsp number of laboratoriesq number of daysr repeatabilityrDday-to-day repeatabilit

49、yR reproducibility(r) relative repeatability(rD) relative day-to-day repeatability(R) relative reproducibilitysM2repeatability variancesrD2day-to-day repeatability variancesR2reproducibility variancesD2day-to-day variancesL2between-laboratory variances standard deviation of datasrrepeatability standard deviationsrDday-to-day repeatability standard deviationsRreproducibility standard deviationSTtotal sum of squaresSLbetween-laboratory sum of squaresSDday-to-day sum of s