DIN 52123-2014 Testing of bitumen and polymer bitumen sheets《沥青和聚合沥青薄板试验》.pdf

1、June 2014 English price group 6No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 91.100.50!%ivC“2708332www.din.deDIN

2、52123Testing of bitumen and polymer bitumen sheets,English translation of DIN 52123:2014-06Prfung von Bitumen- und Polymerbitumenbahnen,Englische bersetzung von DIN 52123:2014-06Essai de feuilles de toiture bitumineuses et en bitume polymre,Traduction anglaise de DIN 52123:2014-06Together with DIN E

3、N 1107-1:1999-10, DIN EN 1108:1999-10, DIN EN 1109:2013-07, DIN EN 1110:2011-03, DIN EN 1297:2004-12, DIN EN 1849-1:2000-01, DIN EN 1850-1:1999-12, DIN EN 1928:2000-07 and DIN EN 13416:2001-09 supersedes DIN 52123:1985-08Supersedes: see belowwww.beuth.deDocument comprises 8 pagesDTranslation by DIN-

4、Sprachendienst.In case of doubt, the German-language original shall be considered authoritative.08.17 DIN 52123:2014-06 2 A comma is used as the decimal marker. Contents Page Foreword . 3 1 Scope 4 2 Normative references 4 3 Designation 4 4 Determination of the content of soluble matter. 4 5 Testing

5、 of the base . 5 6 Determination of the granulometric composition of the mineral surfacing . 5 7 Determination of mineral fillers in the covering . 6 8 Test report . 6 Annex A (normative) Alternative method of determining the content of soluble matter 7 DIN 52123:2014-06 3 Foreword This standard (DI

6、N 52123:2014-06) has been prepared by DIN-Normenausschuss Bauwesen (DIN Standards Committee Building and Civil Engineering), Working Committee NA 005-02-10 AA “Bitumen sheeting for roofs and for waterproofing (national mirror committee for CEN/TC 254/SC 1)”. Attention is drawn to the possibility tha

7、t some of the elements of this document may be the subject of patent rights. DIN and/or DKE shall not be held responsible for identifying any or all such patent rights. Amendments This standard differs from DIN 52123:1985-08 as follows: a) the designation of the products tested in accordance with th

8、is standard has been changed; b) the following tests standardized at European level have been deleted: 1) testing of the external condition and of impregnation; 2) testing of thickness; 3) testing of imperviousness to water; 4) testing of maximum tensile force and of elongation at maximum tensile fo

9、rce; 5) testing of cold bend behaviour; 6) testing of stability under exposure to heat; c) the standard has been editorially revised. Previous editions DIN DVM = DIN 52123: 1928-04, 1939-03 DIN 52123: 1960-11, 1985-08 DIN 52123-1: 1977-03 DIN 52123-2: 1971-06, 1977-03 DIN 52123:2014-06 4 1 Scope Thi

10、s standard applies to the testing of the content of soluble matter, testing of the base, determination of the granulometric composition of the mineral surfacing, determination of mineral fillers in the covering of bitumen felt and polymer bitumen sheeting and felt, that is not covered by European te

11、st methods. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (includi

12、ng any amendments) applies. DIN 12331, Laboratory glassware Beakers DIN 12449, Paper laboratory ware Extraction thimbles DIN 52129, Uncoated bitumen saturated sheeting Definition, designation, requirements DIN EN 1049-2, Textiles Woven fabrics Construction Methods of analysis Part 2: Determination o

13、f number of threads per unit length DIN ISO 3310-1, Test sieves Technical requirements and testing Part 1: Test sieves of metal wire cloth 3 Designation Designation of a comprehensive test as required by this standard (AZ): Test DIN 52123 AZ 4 Determination of the content of soluble matter 4.1 Prepa

14、ration of specimens A strip at least 100 mm long and extending over the whole width of the sheet shall be taken from each test piece. Three specimens, each 100 mm 100 mm, shall be taken from each strip, two of them from points 100 mm from each end of the strip and one from the centre (individual spe

15、cimens). These three specimens shall be tested together (collective specimen). 4.2 Procedure 4.2.1 The content of soluble matter shall be determined by extraction. Additionally, 4.2.2 shall apply for the examination of uncoated bituminous sheeting. The specimens shall be lightly brushed prior to ext

16、raction, in order to remove loosely adhering aggregates. Extraction thimbles as specified in DIN 12449 shall be used for the extraction process. Together with a wad of cotton wool as a stopper, they shall be dried at about 105 C to constant mass, cooled to ambient temperature (18 C to 28 C) in a des

17、iccator over a suitable desiccant and, after removal from the desiccator, weighed to the nearest 0,01 g. The three specimens taken as described in 4.1 shall be inserted into the extraction thimble; the thimble shall be sealed with the wad of cotton wool and immediately weighed to the nearest 0,01 g.

18、 DIN 52123:2014-06 5 Exhaustive extraction shall then take place in an extraction device, that is to say, until the solvent running off is colourless. For this purpose, the following solvents shall be used: for bituminous sheeting: trichlormethane, trichlorethylene, toluene (methylbenzene) or xylene

19、, for sheeting of polymer bitumen: toluene or xylene. When the solvent has dripped off, the thimble is to be dried at about 105 C to constant mass and, after being cooled in the desiccator, is to be reweighed at ambient temperature to the nearest 0,01 g. The loss of mass in grams (g) shall be multip

20、lied by 100/3, giving the content of soluble matter per unit area, in g/m2. 4.2.2 In the case of uncoated bitumen sheeting as specified in DIN 52129, the extraction procedure shall be carried out in accordance with 4.2.1. The quantity of impregnating material determined shall be expressed as a mass

21、fraction (%) of the mass of fibre felt extracted. 5 Testing of the base 5.1 Mass per unit area A soft paintbrush shall be used to remove any particles adhering to the three specimens of base material remaining after the determination of the content of soluble matter as described in Clause 4 or in An

22、nex A. The specimens shall then be dried in an open weighing glass of 60 mm diameter and 120 mm height, at about 105 C until constant mass is reached and, after cooling in a desiccator, weighed in a closed weighing glass to the nearest 0,01 g. After the weighing glass has been opened with a pair of

23、tweezers and the three specimens taken out with tweezers, the weighing glass and lid shall be reweighed. The difference between the two weighings is the weighing result in g, which shall be multiplied by 100/3 to give the mean mass per unit area of the base, in g/m2. In the case of fibre felt, 9 % i

24、s to be added to the mass per unit area ascertained, to allow for the normal moisture content of fibre felt. The result is the mean mass per unit area of the processed fibre felt. In the case of hessian, 16 % is to be added to the mass per unit area ascertained, to allow for the normal moisture cont

25、ent of hessian. The result is the mean mass per unit area of the processed hessian. In the case of textile glass fabric obtained by extraction, the mass determined after drying and subsequent calcination (for 30 min at about 600 C) shall be deemed to be the mean mass per unit area of the processed r

26、aw unfinished glass fabric. 5.2 Sett of hessian The sett shall be determined in the direction of the warp and weft over a length of 100 mm, as specified in DIN EN 1049-2. 6 Determination of the granulometric composition of the mineral surfacing The aggregates obtained in the course of determining th

27、e content of soluble matter in accordance with Clause 4 and Annex A shall be placed on a set of sieves consisting of metal wire cloth test sieves of sizes 1 mm, 0,71 mm, 0,25 mm and 0,09 mm as specified in DIN ISO 3310-1. After sieving for at least 10 min in a vibrating machine, the proportions of p

28、article sizes in the mineral surfacing of over 1,0 mm, 1,0 mm to 0,71 mm, 0,71 mm to 0,25 mm and 0,25 mm to 0,09 mm shall be ascertained by weighing to the nearest 0,1 g. The percentage of the individual particle sizes in the mineral surfacing shall be calculated and stated to the nearest 0,5 %. Par

29、ticle size 0 to less than 0,09 mm is to be regarded as a filler. DIN 52123:2014-06 6 7 Determination of mineral fillers in the covering This test shall be carried out only if the quantity of filler determined in accordance with Clause 6 is greater than 10 % of the content of soluble matter as descri

30、bed in 6.2. About 5 g of the filler that has been separated as specified in Clause 6 by sieving with the 0,09 mm wire cloth test sieve to DIN ISO 3310-1, and that has been dried at (105 2) C to constant mass, are weighed to the nearest 0,001 g, placed in a DIN 12331 H 600 beaker and mixed with 200 m

31、l of hydrochloric acid having a 5 % mass fraction of w(HCl) and a density 20= 1,023 g/cm3. The beaker shall be allowed to stand for about 24 hours, while being swirled frequently. The undissolved fraction shall then be collected on a weighed filter. Following rinsing out with distilled water, the re

32、sidue, together with the filter, shall be dried at (105 2) C to constant mass, weighed and the mass of the filter deducted. The content of soluble matter shall be calculated from the residue on the filter and expressed as a mass fraction of the initial mass. 8 Test report The test report shall conta

33、in the following information corresponding to the requirements placed on the sheeting or felt in question: a) reference to this standard; b) designation of the sheeting or felt tested and location of sampling; c) test method to determine the content of soluble matter; d) content of soluble matter in

34、 g/m2, rounded to the nearest 10 g/m2; e) granulometric composition of the mineral surfacing, mass fraction of each particle size, expressed as a percentage of the total mineral surfacing, rounded to the nearest 0,5 %; f) fillers in the covering, mass fraction of soluble fillers, expressed as a perc

35、entage of total fillers, mean value, rounded to the nearest 1 %; g) mass per unit area of the base in g/m2, rounded to the nearest 10 g/m2; h) sett of hessian base, in units per 100 mm, separately for the direction of the warp and weft, to the nearest unit; i) date of test, testing laboratory. DIN 5

36、2123:2014-06 7 Annex A (normative) Alternative method of determining the content of soluble matter A.1 General The alternative test procedure described below for determining the content of soluble matter is especially suitable for use with sheeting having thicker covering layers. A.2 Preparation of

37、specimens A strip at least 200 mm long, and extending over the whole width of the sheet, shall be cut out of each of the test pieces taken as described in Clause 3. Three specimens, each measuring 200 mm 100 mm, shall be taken from each of the strips, one specimen from points 100 mm from each end of

38、 the strip and one specimen from the centre of the strip. These three specimens shall be tested together. A.3 Procedure The content of soluble matter is determined by extraction. Prior to extraction, the specimens shall be lightly brushed in order to remove loosely adhering aggregates. Thereafter, t

39、hey are weighed to the nearest 0,01 g and exhaustively extracted. For this purpose, the following solvents shall be used: for bituminous sheeting: trichlormethane, trichlorethylene, toluene (methylbenzene) or xylene, for sheeting of polymer bitumen: toluene or xylene. A beaker of 5 000 ml nominal ca

40、pacity, tall type, without a spout and with a fitted flat cooling lid and a silumin base dish for distributing the warmth from heating1), is to be used as the extraction apparatus. The three specimens to be extracted shall be placed in a test frame made, for example, from wire grating and providing

41、a base clearance of about 80 mm, and inserted into the extraction apparatus. The test frame consists of 3 parallel grids, inclined at an angle of about 70 and secured to a base grating. About 500 ml to 700 ml of the solvent shall be used for extraction. Extraction is concluded when the solvent dripp

42、ing off is virtually colourless. Any surfacing material still adhering to the specimens of base material shall then be washed off with a washing bottle, after which they shall be carefully taken out of the extraction apparatus with crucible tongs. The remaining solution, together with the aggregates

43、, shall be poured through a test sieve of metal wire cloth having a 0,09 mm wire sieving medium complying with DIN ISO 3310-1, followed by separation in a concurrent centrifuge. The centrifuge used shall be sufficiently effective to ensure that the residue on ignition of the recovered binder does no

44、t exceed a mass fraction of 1 %. After the extracted base material, the surfacing material and the fillers which have been centrifuged have been dried, the loss of mass in g shall be multiplied by 50/3, giving the content of soluble matter per unit area, in g/m2. When uncoated bitumen sheeting compl

45、ying with DIN 52129 is tested, the quantity of impregnating compound ascertained shall be stated as a mass fraction of the extracted fibre felt. 1)Obtainable through retailers specialized in equipping laboratories for earthworks and asphalt road construction.DIN 52123:2014-06 8 Bibliography DIN EN 1

46、109, Flexible sheets for waterproofing Bitumen sheets for roof waterproofing Determination of flexibility at low temperature DIN EN 1110, Flexible sheets for waterproofing Bitumen sheets for roof waterproofing Determination of flow resistance at elevated temperature DIN EN 1848-1, Flexible sheets fo

47、r waterproofing Determination of length, width and straightness Part 1: Bitumen sheets for roof waterproofing DIN EN 1849-1, Flexible sheets for waterproofing Determination of thickness and mass per unit area Part 1: Bitumen sheets for roof waterproofing DIN EN 1931, Flexible sheets for waterproofing Bitumen, plastic and rubber sheets for roof waterproofing Determination of water vapour transmission properties DIN EN 12311-1, Flexible sheets for waterproofing Part 1: Bitumen sheets for roof waterproofing Determination of tensile properties