DIN EN 1094-1-2008 Insulating refractory products - Part 1 Terminology classification and methods of test for high temperature insulation wool products English version of DIN EN 10.pdf

1、September 2008DEUTSCHE NORM English price group 12No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 01.040.81; 81.080!$R

2、%“1470295www.din.deDDIN EN 1094-1Insulating refractory products Part 1: Terminology, classification and methods of test for hightemperature insulation wool productsEnglish version of DIN EN 1094-1:2008-09Feuerfeste Erzeugnisse fr Wrmedmmzwecke Teil 1: Terminologie, Klassifizierung und Prfverfahren f

3、r Erzeugnisse ausHochtemperaturwolle zur WrmedmmungEnglische Fassung DIN EN 1094-1:2008-09SupersedesDIN EN 1094-1:1997-07,DIN EN 1094-3:2003-10 andDIN V ENV 1094-7:1994-05www.beuth.deDocument comprises 23 pagesDIN EN 1094-1:2008-09 2 National foreword This standard has been prepared by Technical Com

4、mittee CEN/TC 187 “Refractory products and materials” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Technical Committee NA 062-02-57 AA Ungeformte, dichte geformte und wrmedm

5、mende feuerfeste Erzeugnisse und Werkstoffe. The DIN Standard corresponding to the International Standard referred to in this document is as follows: ISO 565 DIN ISO 565 Amendments This standard differs from DIN EN 1094-1:1997-07, DIN EN 1094-3:2003-10 and DIN V ENV 1094-7:1994-05 as follows: a) Com

6、pared with DIN EN 1094-1:1997-07, terms and definitions have been modified and supplemented and a classification has been established regarding the chemical composition, material and product groups. b) Compared with DIN EN 1094-3:2003-10, the classification by groups (i.e. Table 1) has been deleted

7、and is now replaced by the specification of the classification temperature and Figure 1 showing typical application temperatures. c) Compared with DIN V ENV 1094-7:1994-05, the thermal conductivity and shot content measurement have been deleted. The specifications relating to heating have been modif

8、ied with regard to distances between test pieces in the furnace and heating rates (specifications for test temperatures over 1 500 C deleted, see Table 6). A new Figure 2 showing the position of the markers and method of measurement has been added. d) The standard has been editorially revised. Previ

9、ous editions DIN EN 1094-1: 1997-07 DIN V ENV 1094-3: 1998-02 DIN EN 1094-3: 2003-10 DIN V ENV 1094-7: 1994-05 National Annex NA (informative) Bibliography DIN ISO 565, Test sieves Metal wire cloth, perforated metal plate and electroformed sheet Nominal sizes of openings EUROPEAN STANDARDNORME EUROP

10、ENNEEUROPISCHE NORMEN 1094-1July 2008ICS 81.0801094-7:1993 English VersionInsulating refractory products - Part 1: Terminology,classification and methods of test for high temperature insulationwool productsclassification et mthodes dessai pour produits base delaine isolante haute tempratureFeuerfest

11、e Erzeugnisse fr Wrmedmmzwecke - Teil 1:Terminologie, Klassifizierung und Prfverfahren frErzeugnisse aus Hochtemperaturwolle zurWrmedmmungThis European Standard was approved by CEN on 25 May 2008.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions

12、 for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three offici

13、al versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Bel

14、gium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR S

15、TANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2008 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 1094-1:2008: EProduits rfractaires isolants - Parti

16、e 1: Terminologie,Supersedes EN 1094-1:1997, EN 1094-3:2003, ENVEN 1094-1:2008 (E) 2 Contents Page Foreword3 1 Scope 4 2 Normative references 4 3 Terms and definitions .4 4 Classification temperature7 5 Number of test pieces .9 6 Preparation of test pieces.9 7 Test methods9 8 Test report 20 Bibliogr

17、aphy 21 DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 3 Foreword This document (EN 1094-1:2008) has been prepared by Technical Committee CEN/TC 187 “Refractory products and materials”, the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either

18、 by publication of an identical text or by endorsement, at the latest by January 2009, and conflicting national standards shall be withdrawn at the latest by January 2009. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or

19、 CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 1094-1:1997, EN 1094-3:2003 and ENV 1094-7:1993. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement

20、 this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and

21、the United Kingdom. DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 4 1 Scope This European Standard defines terms for those refractory products and materials which are classed as high temperature insulation wools (HTIW). It also establishes the classification of insulating refractory products made from HT

22、IW and specifies methods for determining the thickness, bulk density, resilience, permanent linear change, tensile strength and moisture and organic matter content of HTIW products. It applies to HTIW bulk wool, blankets, felts, mats, boards, pre-formed shapes and papers, with the exception of produ

23、cts delivered in a wet state. Further test procedures are in development and will be included once they have been ratified. These include a 3 point bend test for boards, a length weighted fibre diameter measurement technique by Scanning Electron Microscope, shot content measurement (dry and wet meth

24、ods) and thermal conductivity measurement. There is a shot content method described in ISO 10635 and there is a thermal conductivity technique described in ASTM C201. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated reference

25、s, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1094 (all parts), Insulating refractory products EN ISO 7500-1, Metallic materials Verification of static uniaxial testing machines Part 1: Tension/compress

26、ion testing machines Verification and calibration of the force-measuring system (ISO 7500-1:2004) 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 General terms and definitions 3.1.1 high temperature insulation wool HTIW man-made mineral wool

27、suitable for use as heat-insulating materials above a temperature of 600C and divided into amorphous alkaline earth silicate wools (AES), aluminosilicate wools (ASW) and the polycrystalline wools (PCW) with a classification temperature greater than 1 000 C 3.1.2 wool non-directional agglomeration of

28、 fibres with varying diameter and length distributions 3.1.3 fibre particles with a length to diameter proportion of L/D 3:1 3.1.4 AES-wool amorphous wools with a typical composition range as given in Table 1 DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 5 Table 1 Typical Composition range of AES-wool Co

29、mponent Percentage by mass CaO + MgO 18 to 43 SiO250 to 82 Al2O3+ TiO2+ ZrO248ZrO220Other oxides 1250 C from ambient temperature up to 1200 C between 5 and 10 C/min from 1200 C to 50 C below the test temperature between 2 and 5 C/min for the last 50 C between 1 and 2 C/ min 7.4.4.3 Measurement of th

30、e test pieces after the test Allow test pieces to cool in the furnace until it is practical to remove them without damage and then allow them to cool further to room temperature, then measure the distances between markers as previously. DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 17 7.4.5 Calculation a

31、nd expression of the results For each test piece, calculate the permanent linear change as the mean of two values measured in two different directions, expressed as a percentage of the initial length measured between the platinum wire markers. Express the test result as the mean of the values record

32、ed for each direction on each of the three test pieces. 7.4.6 Test report Prepare a test report in accordance with clause 8, including the bulk density, the measuring device, the heating rate, with the test result in each direction and the mean for each test piece. 7.5 Determination of the tensile s

33、trength 7.5.1 Principle A test piece of prescribed dimensions is cut from the product or the item, and the tensile strength determined by causing rupture of the test piece at room temperature. 7.5.2 Apparatus 7.5.2.1 Tensile testing machine, provided with two pairs of jaws allowing the clamping of t

34、he test piece over a 75 mm x 40 mm area. This device shall be capable of straining the test piece in tension at a constant cross head speed and shall be Class 2 as defined by EN ISO 7500-1. 7.5.3 Test pieces Cut at least five test pieces (230 5) mm x (75 2) mm x (measured thickness). As far as possi

35、ble, take test pieces at random along the longitudinal axis of the product. It is preferable that the longest dimension of the test piece (230 mm) is parallel with the manufacturing direction of the product. NOTE By agreement between parties, and for supplementary tests, test pieces can be taken per

36、pendicular to the manufacturing direction. Dry test pieces at (110 5) C, then cool them to room temperature in a desiccator and carry out testing immediately on removal. 7.5.4 Procedure Measure the thickness of the test piece in the area to be strained in accordance with subclause 7.1, using the dia

37、l gauge comparator method and the width using a ruler accurate to 1 mm. Clamp the test piece at both ends so that a surface area of approximately (75 x 40) mm is held in the jaws of the testing machine. The rate of the tensile stress shall be variable so that the piece deformation occurs at a consta

38、nt speed of 100 mm/min during the whole test. Apply the stress parallel with the manufacturing direction of the product. In the calculation, reject values from tests where parting occurred closer to the jaws than to the centre. In this case, cut new test pieces For the calculation of the results, us

39、e the maximum load recorded in the course of a test resulting in the parting of the test piece. DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 18 7.5.5 Calculation and expression of the results Calculate the tensile strength, R(m), in Pa, using the equation ()tWFmR= where F is the maximum parting force, i

40、n N; W is the width of the active part of the test piece, in m; t is the measured thickness of the test piece, in m, as measured in subclause 7.1. Express the test result as the mean of those determinations together with the bulk density of the product determined in accordance with subclause 7.2. 7.

41、5.6 Test report Prepare a test report in accordance with Clause 8, including the direction of taking out test pieces, the type of tensile testing machine, the bulk density of the product, and the mean of five determinations carried out on five test pieces. 7.6 Determination of moisture and organic m

42、atter content 7.6.1 General Because of its relatively high surface area, HTIWs are susceptible to moisture pick-up after manufacture and especially during storage. Often it is necessary to know if the product has adsorbed water. Additionally organic binders are used in many of the articles manufactu

43、red with HTIWs and it is often necessary to measure the content of these binders. 7.6.2 Principle Moisture and organic contents are measured by weight loss of the sample at temperatures suitable to remove the water or organic material. 7.6.3 Apparatus 7.6.3.1 Balance, capable of weighing to the near

44、est 0,001 g. 7.6.3.2 Silica dish, or other suitable container. 7.6.3.3 Ventilated oven, capable of maintaining (110 5) C. 7.6.3.4 Desiccator. 7.6.3.5 Muffle furnace, capable of heating test pieces to (650 10) C. DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 19 7.6.4 Procedure 7.6.4.1 Moisture content Use

45、 three test pieces. Weigh not less than 10 g of the sample to 0,001 g, (M1) and place in a tared dry dish. Dry in the ventilated oven for not less than 1 hour, cool in the desiccator and reweigh (M2). 7.6.4.2 Organic content Dry sample as described above to obtain dried weight (M2). Heat the sample

46、in a muffle furnace at (650 10) C for not less than 1 hour. Furnace should be at temperature and sample should be removed from furnace whilst still at 650C. Initially cool, for example on a heat-resisting mat, and when sufficiently cool, transfer to a desiccator. When cool, reweigh (M3). 7.6.5 Calcu

47、lation and expression of result Calculate the moisture content (Mm), expressed as a percentage of the original sample mass, using the equation: 100xMMMM121m= where M1is the initial mass of the sample, in g; M2is the mass of the sample after drying, in g. Calculate the total organic matter content (M

48、o), expressed as a percentage of the dry sample mass, using the following equation: 100xMMMM232o= where M2is the mass of the sample after drying, in g; M3is the mass of the sample after heating, in g. 7.6.6 Test report Prepare a test report in accordance with Clause 8, including the individual resul

49、ts and their mean. DIN EN 1094-1:2008-09 EN 1094-1:2008 (E) 20 8 Test report The test reports shall contain the following: a) all information necessary for identification of the sample tested; b) reference to this European Standard (EN 1094:2008); c) designation of the product tested, in accordance with EN 1094; d) specific information given for each of the methods used; e) results of the test(s), including results of the individual determinations and their mean(s), calculated as specified in Clause 6; f)