1、 One or more corrigenda exist with corrections to this document. These can be searched online and ordered free of charge at www.beuth.de October 2009DEUTSCHE NORM English price group 8No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berli
2、n. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83.180; 91.100.10!$Z7“1552096www.din.deDDIN EN 12808-4Grouts for tiles Part 4: Determination of shrinkageEnglish version of DIN EN 12808-4:2009-10Klebstoffe und Fugenmrtel fr Fliesen und
3、 Platten Teil 4: Bestimmung der SchwindungEnglische Fassung DIN EN 12808-4:2009-10SupersedesDIN EN 12808-4:2002-04www.beuth.deDocument comprises pages13DIN EN 12808-4:2009-10 National foreword This standard has been prepared by Technical Committee CEN/TC 67 “Ceramic tiles” (Secretariat: UNI, Italy).
4、 The responsible German body involved in its preparation was the Normenausschuss Bauwesen (Building and Civil Engineering Standards Committee), Technical Committee NA 005-09-82 AA Keramische Fliesen und Platten (Sp CEN/TC 67, ISO/TC 189). DIN EN 12808 consists of the following parts, under the gener
5、al title Grouts for tiles: Part 1: Determination of chemical resistance of reaction resin mortars Part 2: Determination of resistance to abrasion Part 3: Determination of flexural and compressive strength Part 4: Determination of shrinkage Part 5: Determination of water absorption Amendments This st
6、andard differs from DIN EN 12808-4:2002-04 as follows: a) The reference to EN 196-1 in subclause 6.3 is now undated. b) In subclause 6.1, the specifications for moulds have been rendered more precise. c) In subclause 7.1, the last paragraph has been deleted. d) In subclause 7.2, the application of a
7、 release agent has been included. e) Figures 1 to 4 have been replaced by new linguistically neutral figures with corresponding keys. f) The bibliography has been updated. g) The standard has been editorially revised. Previous editions DIN EN 12808-4: 2002-04 2 EUROPEAN STANDARDNORME EUROPENNEEUROPI
8、SCHE NORMEN 12808-4July 2009ICS 83.180; 91.100.10 Supersedes EN 12808-4:2001 English VersionGrouts for tiles - Part 4: Determination of shrinkageMortiers de joints pour carrelages - Partie 4: Dterminationdu retraitKlebstoffe und Fugenmrtel fr Fliesen und Platten - Teil 4:Bestimmung der SchwindungThi
9、s European Standard was approved by CEN on 21 May 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references c
10、oncerning such nationalstandards may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its o
11、wn language and notified to the CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuani
12、a, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All r
13、ights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 12808-4:2009: EEN 12808-4:2009 (E) 2 Contents Page Foreword 31 Scope 42 Normative references 43 Sampling .44 Test conditions 45 Test materials .46 Apparatus .47 Procedure .57.1 Mixing of grouts
14、.57.2 Preparation of test specimens .57.3 Test procedure .68 Evaluation of results .69 Test report 6Bibliography . 11DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 3 Foreword This document (EN 12808-4:2009) has been prepared by Technical Committee CEN/TC 67 “Ceramic tiles”, the secretariat of which is h
15、eld by UNI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2010, and conflicting national standards shall be withdrawn at the latest by January 2010. Attention is drawn to the possibility
16、 that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 12808-4:2001. This document is one of a series of European Standards for ceramic tile adhesives
17、 including: EN 1308, Adhesives for tiles Determination of slip EN 1323, Adhesives for tiles Concrete slabs for tests EN 1324, Adhesives for tiles Determination of shear adhesion strength of dispersion adhesives EN 1346, Adhesives for tiles Determination of open time EN 1347, Adhesives for tiles Dete
18、rmination of wetting capability EN 1348, Adhesives for tiles Determination of tensile adhesion strength for cementitious adhesives EN 12002, Adhesives for tiles Determination of transverse deformation for cementitious adhesives and grouts EN 12003, Adhesive for tiles Determination of shear adhesion
19、strength of reaction resin adhesives EN 12004, Adhesives for tiles Requirements, evaluation of conformity, classification and designation EN 12808-1, Grouts for tiles Part 1: Determination of chemical resistance of reaction resin mortars EN 12808-2, Grouts for tiles Part 2: Determination of resistan
20、ce to abrasion EN 12808-3, Grouts for tiles Part 3: Determination of flexural and compressive strength EN 12808-4, Grouts for tiles Part 4: Determination of shrinkage EN 12808-5, Grouts for tiles Part 5: Determination of water absorption According to the CEN/CENELEC Internal Regulations, the nationa
21、l standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Pol
22、and, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 4 1 Scope This European Standard applies to all ceramic tile grouts for internal and external tile installations on walls and floors. This European Standard speci
23、fies the test method to be used to determine the shrinkage of ceramic tile grouts. This European Standard does not contain performance requirements or recommendations for the design and installation of ceramic tiles. NOTE Ceramic tile grouts can also be used for other types of tiles (natural and agg
24、lomerated stones, etc.), where these do not adversely affect the stones. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the reference
25、d document (including any amendments) applies. EN 196-1, Methods of testing cement Part 1: Determination of strength EN 1067, Adhesives Examination and preparation of samples for testing EN ISO 15605, Adhesives Sampling (ISO 15605:2000) 3 Sampling Take a sample of at least 2 kg of the product to be
26、tested in accordance with EN ISO 15605 and EN 1067. 4 Test conditions Standard conditions shall be (23 2) C and (50 5) % R.H. and a speed of air in the working area less than 0,2 m/s. 5 Test materials Condition all test materials for at least 24 h under standard conditions. 6 Apparatus 6.1 Moulds, u
27、sed to prepare prismatic specimens 40 mm x 40 mm x 160 mm (three-gang mould), with ground surfaces, made of steel, in accordance with EN 196-1. Holes for fitting suitable pins shall be drilled into the ends of the sides of the moulds corresponding to the ends of test specimen (see Figure 1). Moulds
28、provided with internal dimensions (10 0,5) mm width, (40 0,5) mm depth and (160 1) mm length, to enable three specimens to be prepared simultaneously; either: a) moulds with horizontal compartments 10 mm x 40 mm x 160 mm (see EN 196-1 in principle) or b) moulds in accordance with EN 196-1 with horiz
29、ontal compartments 10 mm x 40 mm x 160 mm and width reducing plastic or metal inserts, DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 5 two for each mould. 6.2 Six smooth, rigid, non-absorbent frames (e.g. in polyethylene or PTFE) to be inserted, with dimensions of 40 mm x 160 mm and thickness of 15 mm.
30、 6.3 Jolting apparatus or jolting table used for the compaction of 10 mm x 40 mm x 160 mm grout specimen; in accordance with EN 196-1. 6.4 Measuring apparatus that shall consist of a measurement attachment and a base with adjustment screws. The measurement attachment shall be formed either by an ana
31、logue or digital gauge, which reads accurately to 0,01 mm, rigidly mounted in a measuring frame (see Figures 2, 3 and 4). 6.5 Calibration rod or reference rod that shall be used as a standard length against which gauge readings can be tested. The rod shall be made of material having a negligible coe
32、fficient of expansion (e.g. Invar). 7 Procedure 7.1 Mixing of grouts The amount of water and/or liquid admix required for preparing the cementitious grout shall be as stated by the manufacturer in parts by mass, i.e. liquid to dry powder. Prepare at least 2 kg of the grout in a mixer of the type des
33、cribed in EN 196-1, using the slow speed settings, (140 5) r/min rotation and (62 5) r/min planetary movement. Carry out the following procedure: pour the liquid into the pan; scatter the dry powder over the liquid; mix for 30 s; take out the mixing paddle; scrape down the paddle and pan within 1 mi
34、n; replace the paddle and mix for 1 min. Let the grout mature if and as specified in the manufacturers instructions, and then mix for a further 15 s. In the case of reaction resin grouts follow the manufacturers instructions. 7.2 Preparation of test specimens Insert two non-absorbent frames at the s
35、ides of each compartment of the mould, to reduce the width to 10 mm. Apply a thin layer of release agent to the internal faces of the mould. Mould the specimens immediately after the preparation of the grout, with the mould firmly clamped to the jolting table. Introduce, using a suitable scoop, the
36、first of two layers of grout into each of the compartments, directly from the mixing bowl. Spread the layer uniformly, then compact using 60 jolts. Introduce the second layer of grout, level and compact with a further 60 jolts. DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 6 Lift the mould gently from
37、the jolting table, strike off excess of material and smooth the surface with a flat trowel. Wipe off the grout left on the perimeter of the mould. Cover with a glass plate according to EN 196-1. Place the mould, suitably identified, on a horizontal base in standard conditions, (23 2) C and (50 5) %
38、R.H. After 24 h remove carefully the specimen from the mould and determine with the measuring apparatus (6.4) the length of the test sample (initial reading). Keep the demoulded prism in standard conditions leaving a clearance of at least 25 mm on all sides. Prepare three specimens for each grout. 7
39、.3 Test procedure Take the reading of each specimen 27 days 12 h after the initial reading. 8 Evaluation of results The linear shrinkage is evaluated in mm/m as the mean of three values based on the initial measurement. 9 Test report The test report shall provide the following information: c) number
40、, title and issue of this European Standard; d) place and date of sampling; e) type of grout, commercial designation and manufacturer name; f) identification of the test sample; g) handling and storage of samples before testing; h) test conditions; i) date of testing; j) amount of water or liquid us
41、ed for preparing the grout; k) test results (individual and means values) in mm/m; l) any other factor that could have influenced the result. DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 7 Dimensions in millimetres Key 1 Cover strip 2 Top frame internal width (39,6 0,2) mm 3 With top frame 4 Without t
42、op frame Figure 1 Three gang mould used to prepare prismatic specimens 40 mm x 40 mm x 160 mm DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 8 Key 1 Adjustment screw 2 Frame 3 Measurement stud 4 Side rod 5 Specimen 6 Holder Figure 2 Measuring apparatus (type A) DIN EN 12808-4:2009-10 EN 12808-4:2009 (E)
43、 9 Key 1 Stop device 2 Holder Figure 3 Measuring apparatus (type B) DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 10 Key 1 Horizontal 2 Measuring axis 3 Stand 1 4 Measuring area (164 to 170) mm 5 Stand 2 Figure 4 Measuring apparatus (type C) DIN EN 12808-4:2009-10 EN 12808-4:2009 (E) 11 Bibliography 1 EN 13888, Grout for tiles Requirements, evaluation of conformity, classification and designation DIN EN 12808-4:2009-10
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