DIN EN 12849-2009 Bitumen and bituminous binders - Determination of penetration power of bituminous emulsions English version of DIN EN 12849 2009-07《沥青和沥青粘合剂 测定沥青乳液的渗透性 DIN EN 128.pdf

1、July 2009DEUTSCHE NORM English price group 10No part of this standard may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 75.140; 91.100.50!$Xls“15

2、37380www.din.deDDIN EN 12849Bitumen and bituminous binders Determination of penetration power of bituminous emulsionsEnglish version of DIN EN 12849:2009-07Bitumen und bitumenhaltige Bindemittel Bestimmung der Eindringfhigkeit von BitumenemulsionenEnglische Fassung DIN EN 12849:2009-07SupersedesDIN

3、EN 12849:2002-08www.beuth.deDocument comprises 12 pagesDIN EN 12849:2009-07 2 National foreword This standard has been prepared by Technical Committee CEN/TC 336 “Bituminous binders” (Secretariat: AFNOR, France). The responsible German bodies involved in its preparation were the Normenausschuss Mate

4、rialprfung (Materials Testing Standards Committee) and the Normenausschuss Bauwesen (Building and Civil Engineering Standards Committee), Joint Technical Committee NA 062-03-32 GA Bitumen; Prfverfahren und Anforderungen fr die Bindemittel. Amendments This standard differs from DIN EN 12849:2002-08 a

5、s follows: a) The reference filler has been modified. b) The standard has been editorially revised. Previous editions DIN 52046: 1980-12 DIN EN 12849: 2002-08 EUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 12849March 2009ICS 75.140; 91.100.50 Supersedes EN 12849:2002 English VersionBitumen and bi

6、tuminous binders - Determination of penetrationpower of bituminous emulsionsBitumes et liants bitumineux - Dtermination du pouvoir depercolation des mulsions de bitumeBitumen und bitumenhaltige Bindemittel - Bestimmung derEindringfhigkeit von BitumenemulsionenThis European Standard was approved by C

7、EN on 17 February 2009.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards

8、 may be obtained on application to the CEN Management Centre or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any other language made by translationunder the responsibility of a CEN member into its own language and notified to the

9、CEN Management Centre has the same status as theofficial versions.CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland,France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherland

10、s, Norway, Poland, Portugal,Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR NORMUNGManagement Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All rights of exploitation in any for

11、m and by any means reservedworldwide for CEN national Members.Ref. No. EN 12849:2009: EEN 12849:2009 (E) 2 Contents Page Foreword 3 1 Scope 4 2 Normative references 4 3 Terms and definitions .4 4 Principle 4 5 Reagents and materials 4 6 Apparatus .5 7 Sampling .6 8 Procedure .6 9 Expression of resul

12、ts 6 10 Precision .7 11 Test report 7 Annex A (normative) Characteristics of the Silica Sand Type F 34 8 Annex B (normative) Characteristics of the Testing Silica Filler 315-001 .9 Bibliography . 10 DIN EN 12849:2009-07 EN 12849:2009 (E) 3 Foreword This document (EN 12849:2009) has been prepared by

13、Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2009, and conflicting national standards s

14、hall be withdrawn at the latest by September 2009. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 12849:2

15、002. From the previous edition, new reference filler is now specified; a mixture of silica sand and silica filler is used as reference filler. Characteristics of both silica sand and silica filler are given respectively in normative Annex A and Annex B. According to the CEN/CENELEC Internal Regulati

16、ons, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherla

17、nds, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. DIN EN 12849:2009-07 EN 12849:2009 (E) 4 1 Scope This European Standard specifies a method for the determination of the penetration power of bituminous emulsions, through reference filler.

18、This test method is applicable to low-viscosity bituminous emulsions. WARNING The use of this standard can involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this

19、 standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applie

20、s. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders - Sampling bituminous binders EN 12594, Bitumen and bituminous binders - Preparation of test samples 3 Terms and definitions For the purposes of this doc

21、ument, the following terms and definitions apply. 3.1 penetration power ability of a bitumen emulsion to penetrate into a reference filler 3.2 penetration time time, in minutes, required for a specified quantity of bituminous emulsion to penetrate into a defined quantity of a reference filler 4 Prin

22、ciple A specified quantity of the emulsion to be tested is poured onto the reference filler. The time required for the emulsion to penetrate into the filler is measured. 5 Reagents and materials A mixture of specified silica sand and silica filler is used as the reference filler. In the event of a d

23、ispute, the reference filler specified shall be used. 5.1 Sand The silica sand type F 341shall be used as one of the two components of the reference filler. Characteristics are given in Annex A. 1The silica sand type F 34 is the trade name of a product supplied by Quarzwerke GmbH. This information i

24、s given for the convenience of users of this European Standard and does not constitute an endorsement by CEN of the product name. Equivalent products may be used if they can be shown to lead to the same results, or if a correlation between the products has been established. DIN EN 12849:2009-07 EN 1

25、2849:2009 (E) 5 5.2 Filler The testing silica filler 315-0012)shall be used as one of the two components of the reference filler. Characteristics are given in Annex B. 6 Apparatus Usual laboratory apparatus and glassware, together with the following: 6.1 Test apparatus, as shown in Figure 1, consist

26、ing of a glass tube with fused-on glass filter disc with pore size between 160 m and 250 m. A vent, below the glass filter disc, provides pressure compensation when the test apparatus is charged. The vent shall be cut perpendicular to the vertical axis, with its edges slightly fused. NOTE The vent c

27、an be dispensed with if, during the test procedure, the test apparatus is supported. Dimensions in millimetres Key 1. Glass filter disc 2. Vent Figure 1 Test apparatus 2) The testing silica filler 315-001 is the trade name of a product supplied by Quarzwerke GmbH. This information is given for the c

28、onvenience of users of this European Standard and does not constitute an endorsement by CEN of the product name. Equivalent products may be used if they can be shown to lead to the same results, or if a correlation between the products has been established. DIN EN 12849:2009-07 EN 12849:2009 (E) 6 6

29、.2 Balance, capable of weighing 100 g, with an accuracy of 0,1 g. 6.3 Oven, capable of being maintained at (110 5) C. 6.4 Wooden board, 200 mm x 200 mm x 10 mm in size. 6.5 Stopwatch, graduated in divisions of 1 s or less. 7 Sampling The material under test shall be sampled in accordance with EN 58

30、and prepared in accordance with EN 12594. The test shall be carried out on two test portions of the sample, each weighing (10,0 0,1) g (see Clause 8). 8 Procedure 8.1 General Carry out the procedure under normal laboratory conditions, between 18 C and 28 C. 8.2 Test Dry the quantities of silica sand

31、 and testing silica filler, required for the test, in the oven (6.3) at a temperature of (110 5) C until constant mass is reached and cool to ambient temperature in a desiccator. For each test portion, mix intimately (50,0 0,1) g of silica sand and (50,0 0,1) g of testing silica filler and transfer

32、via a funnel to the upper part of the test apparatus (6.1), lifting the funnel with increasing filling height. Level the surface of the filler mixture in the apparatus by knocking the lower edge of the test apparatus three times on the wooden board (6.4). Place the apparatus on the balance (6.2). Po

33、ur (10,0 0,1) g of the emulsion to be tested along a glass rod onto the centre of the filler mixture. Pour the entire quantity of emulsion within (10 1) s. Start measuring the time immediately after pouring the emulsion. Cover the test apparatus using a watch glass. Determine the time for the emulsi

34、on to completely penetrate into the filler mixture, i.e. when the structure of the filler at its upper surface can be clearly recognised. If penetration of the filler mixture is not completed within 20 min, discontinue the test. Repeat the test procedure using new quantities of filler and emulsion.

35、If the results for both sample portions differ by more than 3 min, repeat the procedure for a third sample portion. The two values nearest to each other are used to calculate the mean penetration time. 9 Expression of results Express the individual penetration times and the average penetration time,

36、 in minutes, to the nearest integer. Express the result as the arithmetic mean of the two individual results of penetration time, to the nearest integer. DIN EN 12849:2009-07 EN 12849:2009 (E) 7 10 Precision NOTE The precision of the method was evaluated in accordance with EN ISO 4259 2. 10.1 Repeat

37、ability The difference between two successive test results, obtained by the same operator with the same apparatus under constant operating conditions on identical test material would, in the long run, in the normal and correct operation of the test method, exceed 3 min in only one case in twenty. 10

38、.2 Reproducibility The difference between two single and independent results obtained by different operators working in different laboratories on identical test material would, in the long run, in the normal and correct operation of the test method, exceed 6 min in only one case in twenty (provided

39、that both results have been determined within two weeks). NOTE The source of precision data is DIN 52046 1. 11 Test report The test report shall contain at least the following information: a) type and complete identification of the sample under test; b) reference to this European Standard; c) refere

40、nce to the type of apparatus used; d) reference to the used sand and filler; e) result of the test (see Clause 9); f) any deviation, by agreement or otherwise, from the procedure specified; g) date of sampling, date of sample preparation and date of the test. DIN EN 12849:2009-07 EN 12849:2009 (E) 8

41、 Annex A (normative) Characteristics of the Silica Sand Type F 34 The Silica Sand Type F 34 shall have at least the following properties: Natural fine silica, uncrushed; SiO2content greater than 99 %; Density of (2 650 20) kg/m3; Particle size distribution, as % passing: 0,355 mm from 0 % to 4 %; 0,

42、25 to 0,355 mm from 2 % to 22 %; 0,18 to 0,25 mm from 32 % to 67 %; 0,125 to 0,18 mm from 19 % to 51 %; 315 m 0,1%; 250 m 2 %; 200 m 9 %; 160 m 25 %; 125 m 54 %; 100 m 69 %; 80 m 74 %; 63 m 78 %; 50 m 82 %; 40 m 84 %. The Testing Silica Filler Type 315-001 is available from Quarzwerke GmbH, Kaskaden

43、weg 40, D-50226 Frechen, Tel.: +49-(0)2234-101-0, Fax: +49-(0)2234-101-400, e-mail: , . Key X Particle size, mm Y residue, % Figure B.1 Typical gradation of Testing Silica Filler 315-001 DIN EN 12849:2009-07 EN 12849:2009 (E) 10 Bibliography 1 DIN 52046, Testing of bituminous binders Determination of the wettability of bonding emulsion 2 EN ISO 4259, Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006) DIN EN 12849:2009-07