DIN EN 13523-13-2014 Coil coated metals - Test methods - Part 13 Resistance to accelerated ageing by the use of heat German version EN 13523-13 2014《覆层金属卷材 试验方法 第13部分 耐热加速老化性能 EN 1.pdf

1、August 2014 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS

2、25.220.60!%:;2“2232415www.din.deDDIN EN 13523-13Coil coated metals Test methods Part 13: Resistance to accelerated ageing by the use of heat;English version EN 13523-13:2014,English translation of DIN EN 13523-13:2014-08Bandbeschichtete Metalle Prfverfahren Teil 13: Bestndigkeit gegen beschleunigte

3、Alterung durch Wrmeeinwirkung;Englische Fassung EN 13523-13:2014,Englische bersetzung von DIN EN 13523-13:2014-08Tles prlaques Mthodes dessai Partie 13: Rsistance au vieillissement acclr par la chaleur;Version anglaise EN 13523-13:2014,Traduction anglaise de DIN EN 13523-13:2014-08SupersedesDIN EN 1

4、3523-13:2001-12www.beuth.deDocument comprises 12 pagesIn case of doubt, the German-language original shall be considered authoritative.07.14DIN EN 13523-13:2014-08 2 A comma is used as the decimal marker. National foreword This document (EN 13523-13:2014) has been prepared by Technical Committee CEN

5、/TC 139 “Paints and varnishes”, (Secretariat: DIN, Germany), Working Group WG 9 “Testing of coil coated metals” (Secretariat: DIN, Germany). The responsible German body involved in its preparation was the Normenausschuss Beschichtungsstoffe und Beschichtungen (DIN Standards Committee Coatings and Co

6、ating Materials), Working Committee NA 002-00-07 AA Allgemeine Prfverfahren fr Beschichtungsstoffe und Beschichtungen. Amendments This standard differs from DIN EN 13523-13:2001-12 as follows: a) in Subclause 8.2.1, the preparation of test specimen has been made optional for the case that no prepare

7、d test specimens are available; b) in Subclauses 8.2.5 and 8.2.6, the measurement of adhesion has been made optional; c) in Subclause 8.3.2, the time for storage after bending has been specified; d) the supplementary information in the former Annex A has been integrated in the test report. Previous

8、editions DIN EN 13523-13: 2001-12 EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 13523-13 June 2014 ICS 25.220.60 Supersedes EN 13523-13:2001English Version Coil coated metals - Test methods - Part 13: Resistance to accelerated ageing by the use of heat Tles prlaques - Mthodes dessai - Partie

9、13: Rsistance au vieillissement acclr par la chaleur Bandbeschichtete Metalle - Prfverfahren - Teil 13: Bestndigkeit gegen beschleunigte Alterung durch Wrmeeinwirkung This European Standard was approved by CEN on 7 May 2014. CEN members are bound to comply with the CEN/CENELEC Internal Regulations w

10、hich stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This

11、European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN member

12、s are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal

13、, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014 CEN All rights of exploitation in any form

14、and by any means reserved worldwide for CEN national Members. Ref. No. EN 13523-13:2014 EEN 13523-13:2014 (E) 2 Contents Page Foreword 3 1 Scope 5 2 Normative references 5 3 Terms and definitions .5 4 Principle 5 5 Apparatus and materials .5 6 Sampling .6 7 Test specimens 6 8 Procedure .6 8.1 Proced

15、ure using flat specimens 6 8.2 Procedure using specimens that are to be aged after bending 6 8.3 Procedure using specimens that are to be bent after ageing .7 9 Expression of results 7 10 Precision .9 11 Test report 9 Bibliography . 10 DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 3 Foreword This doc

16、ument (EN 13523-13:2014) has been prepared by Technical Committee CEN/TC 139 “Paints and varnishes”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by Decemb

17、er 2014, and conflicting national standards shall be withdrawn at the latest by December 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent

18、 rights. This document supersedes EN 13523-13:2001. The main technical changes are: a) in 8.2.1 the preparation of test specimen was made optional for the case that no prepared test specimens are available; b) in 8.2.5 and 8.2.6 the measurement of adhesion was made optional; c) in 8.3.2 the time for

19、 storage after bending was specified; d) the supplementary information in the former Annex A were integrated in the test report. EN 13523, Coil coated metals Test methods, consists of the following parts: Part 0: General introduction Part 1: Film thickness Part 2: Gloss Part 3: Colour difference Ins

20、trumental comparison Part 4: Pencil hardness Part 5: Resistance to rapid deformation (impact test) Part 6: Adhesion after indentation (cupping test) Part 7: Resistance to cracking on bending (T-bend test) Part 8: Resistance to salt spray (fog) Part 9: Resistance to water immersion Part 10: Resistanc

21、e to fluorescent UV radiation and water condensation Part 11: Resistance to solvents (rubbing test) Part 12: Resistance to scratching Part 13: Resistance to accelerated ageing by the use of heat DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 4 Part 14: Chalking (Helmen method) Part 15: Metamerism Part

22、 16: Resistance to abrasion Part 17: Adhesion of strippable films Part 18: Resistance to staining Part 19: Panel design and method of atmospheric exposure testing Part 20: Foam adhesion Part 21: Evaluation of outdoor exposed panels Part 22: Colour difference Visual comparison Part 23: Resistance to

23、humid atmospheres containing sulfur dioxide Part 24: Resistance to blocking and pressure marking Part 25: Resistance to humidity Part 26: Resistance to condensation of water Part 27: Resistance to humid poultice (Cataplasm test) Part 29: Resistance to environmental soiling (Dirt pick-up and striping

24、) According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, G

25、ermany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 5 1 Scope This Part of EN 13523 specifie

26、s the procedure for determining the behaviour of an organic coating on a metallic substrate when submitted to accelerated ageing by heating at a defined temperature for a defined period of time. It is not possible to test heat resistance in such a way as to control all possible conditions of use. Th

27、e aim of this test is therefore to furnish the basic test method for the effect of heat. Special applications might require that properties other than those mentioned in this Part of EN 13523 be checked. The test(s) to be done should then be agreed between the interested parties. 2 Normative referen

28、ces The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN

29、13523-0:2014, Coil coated metals Test methods Part 0: General introduction EN 13523-2, Coil coated metals Test methods Part 2: Specular gloss EN 13523-3, Coil coated metals Test methods Part 3: Colour difference Instrumental comparison EN 13523-7:2014, Coil coated metals Test methods Part 7: Resista

30、nce to cracking on bending (T-bend test) EN 23270, Paints and varnishes and their raw materials Temperatures and humidities for conditioning and testing (ISO 3270) EN 60454-2, Pressure-sensitive adhesive tapes for electrical purposes Part 2: Methods of test (IEC 60454-2) 3 Terms and definitions For

31、the purposes of this document, the terms and definitions given in EN 13523-0:2014 apply. 4 Principle A test specimen is subjected to an elevated temperature during a defined period of time. Certain physical properties of the test specimen are then compared to those of a reference specimen which has

32、been kept during the same period of time in ambient conditions of temperature. 5 Apparatus and materials 5.1 Air circulation oven, capable of being maintained at the chosen test temperature to 5 % (in C). 5.2 Apparatus as described in EN 13523-2, EN 13523-3 and EN 13523-7. 5.3 Transparent pressure-s

33、ensitive adhesive tape, 25 mm wide, with an adhesion strength of (10 1) N per 25 mm width when tested in accordance with EN 60454-2. DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 6 6 Sampling See EN 13523-0. 7 Test specimens See EN 13523-0. Two sets of specimens shall be taken: one set for the ageing

34、 tests and one set as reference specimens. Test and reference specimens shall be taken from the same precoated sheet of coil coated metal in order to ensure a precise assessment of the property being evaluated. The number and size of all specimens shall be such that all required tests can be carried

35、 out. See 8.1.1 and 8.3.1 respectively. 8 Procedure 8.1 Procedure using flat specimens 8.1.1 Select two specimens for each test. 8.1.2 Place one specimen, the reference specimen, in the ambient storage conditions. For more accurate tests, as required for instance in case of dispute, the ambient temp

36、erature shall be (23 2) C and the relative humidity (50 5) %, in accordance with EN 23270. 8.1.3 Subject the other specimen, the test specimen, to accelerated ageing in the air circulation oven (5.1) at the specified or agreed test temperature and for the specified or agreed period of time. 8.1.4 Af

37、ter the specified or agreed period of time remove the test specimen from the oven and condition it for at least 16 h under conditions as specified in 8.1.2. 8.1.5 Measure the gloss and colour of both the reference specimen and the aged test specimen, using the same apparatus and following the proced

38、ures described in EN 13523-2 and EN 13523-3 respectively. Calculate the gloss and colour differences. 8.2 Procedure using specimens that are to be aged after bending 8.2.1 If not otherwise agreed, select and bend specimens as described in EN 13523-7, i.e. by using the minimum bending radius that the

39、 material can tolerate without cracking being visible at 10 magnification. Assuming that Ta= a, where a represents the minimum radius and t the thickness of the substrate, prepare two sets of five specimens and bend them according to the following radii: Ta= a Tb= a + 0,5 t Tc= a + 1,0 t Td= a + 1,5

40、 t Te= a + 2,0 t Alternatively, bend the specimens using the conical wedge mandrel specified in EN 13523-7:2014, 5.1.2. 8.2.2 Place one set of specimens, the reference specimens, in the ambient storage conditions. For more accurate tests, as required for instance in case of dispute, the ambient temp

41、erature shall be (23 2) C and the relative humidity (50 5) %, in accordance with EN 23270. DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 7 8.2.3 Subject the second set of specimens, the test specimens, to accelerated ageing in the air circulation oven (5.1) at the specified or agreed test temperature

42、 and for the specified or agreed period of time. 8.2.4 After the specified or agreed period of time remove the test specimens from the oven and condition them for at least 16 h under conditions as specified in 8.2.2. 8.2.5 Assess the reference specimens for cracking which might have occurred during

43、natural ageing, and if specified measure loss of adhesion using the adhesive tape (5.3). 8.2.6 Assess the test specimens for cracking, and if specified measure loss of adhesion using the adhesive tape (5.3). 8.3 Procedure using specimens that are to be bent after ageing 8.3.1 Select and age five fla

44、t specimens at the specified or agreed test temperature and for the specified or agreed period of time. 8.3.2 Bend the reference specimens using the procedure described in 8.2.1 and place them for at least 16 h in ambient storage conditions as described in 8.2.2. 8.3.3 Bend the aged test specimens t

45、o the same radii as determined in 8.2.1. 8.3.4 Assess both the reference specimens and the test specimens as described in 8.2.5 and 8.2.6 respectively. 9 Expression of results Express the results as indicated in Table 1. DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 8 Table 1 Expression of results Ty

46、pe of specimen Property Obtained values Difference in values Reference specimen(s) Test specimen(s) Flat specimens Gloss Colour Specimens to be aged after bending Resistance to cracking TaTbTcTdTeconical wedge mandrel Loss of adhesion TaTbTcTdTeconical wedge mandrel Specimens to be bent after ageing

47、 Resistance to cracking TaTbTcTdTeconical wedge mandrel Loss of adhesion TaTbTcTdTeconical wedge mandrel DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 9 10 Precision No precision data are currently available. 11 Test report The test report shall contain at least the following information: a) all deta

48、ils necessary to identify the product tested; b) a reference to this Part of EN 13523 (EN 13523-13); c) the test temperature; d) the duration of ageing at the test temperature; e) whether the specimens have been bent and if so, whether the bend was carried out before or after ageing; f) the results

49、of the test, as indicated in Clause 9; g) any deviation from the test method specified; h) any unusual features (anomalies) observed during the test; i) the date of the test. DIN EN 13523-13:2014-08 EN 13523-13:2014 (E) 10 Bibliography 1 EN 1396, Aluminium and aluminium alloys Coil coated sheet and strip for general applications - Specifications 2 EN 10169, Continuously organic coated (coil coated) steel flat products T