DIN EN 1482-3-2016 en 4848 Fertilizers and liming materials - Sampling and sample preparation - Part 3 Sampling of static heaps German version EN 1482-3 2016《肥料和石灰质材料 取样和样品制备 第3部分 .pdf

1、October 2016 English price group 11No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 65.080!%n6“2577519www.din.deDIN

2、EN 1482-3Fertilizers and liming materials Sampling and sample preparation Part 3: Sampling of static heaps;English version EN 14823:2016,English translation of DIN EN 1482-3:2016-10Dngemittel und Kalkdnger Probenahme und Probenvorbereitung Teil 3: Probenahme aus statischen Haufwerken;Englische Fassu

3、ng EN 14823:2016,Englische bersetzung von DIN EN 1482-3:2016-10Engrais et amendements minraux basiques chantillonnage et prparation de lchantillon Partie 3: chantillonnage des tas statiques;Version anglaise EN 14823:2016,Traduction anglaise de DIN EN 1482-3:2016-10www.beuth.deDTranslation by DIN-Spr

4、achendienst.In case of doubt, the German-language original shall be considered authoritative.Document comprises 18 pages 09.16 2 A comma is used as the decimal marker. National foreword This document has been prepared by Technical Committee CEN/TC 260 “Fertilizers and liming materials” (Secretariat:

5、 DIN, Germany) under the mandate M/454. The responsible German body involved in its preparation was DIN-Normenausschuss Lebensmittel und landwirtschaftliche Produkte (DIN Standards Committee Food and Agricultural Products), Working Committee NA 057-03-02 AA Dngemittel. DIN EN 1482-3:2016-10EUROPEAN

6、STANDARD NORME EUROPENNE EUROPISCHE NORM EN 1482-3 August 2016 ICS 65.080 English Version Fertilizers and liming materials - Sampling and sample preparation - Part 3: Sampling of static heaps Engrais et amendements minraux basiques - chantillonnage et prparation de lchantillon - Partie 3 : chantillo

7、nnage des tas statiques Dngemittel und Kalkdnger - Probenahme und Probenvorbereitung - Teil 3: Probenahme aus statischen Haufwerken This European Standard was approved by CEN on 12 June 2016. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for

8、 giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three

9、 official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodi

10、es of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Sp

11、ain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2016 CEN All rights of exploitation in any form and by any means reserved worldwi

12、de for CEN national Members. Ref. No. EN 1482-3:2016 EEN 1482-3:2016 (E) 2 Contents Page European foreword . 3 Introduction 4 1 Scope 5 2 Normative references 5 3 Terms and definitions . 5 4 Sampling plans and quantitative data . 5 4.1 General 5 4.2 Characterization of the lot to be sampled 6 4.3 Sa

13、mpling plan . 6 4.3.1 General 6 4.3.2 Elements of the sampling plan . 6 4.4 Determination of the volume/mass of the lot. 8 4.5 Determination of sampling units and sampling points . 8 4.5.1 Determination of the number and location of the sampling units 8 4.5.2 Minimum total number of sampling units .

14、 8 4.5.3 Determination of sampling units from which incremental samples shall be taken . 8 4.5.4 Determination of the minimum number of sampling points from which sub-samples are to be taken 8 4.6 Quantitative data . 8 4.6.1 Determination of the minimum mass of increments . 8 4.6.2 Mass of increment

15、s . 9 4.6.3 Aggregate/reduced and final samples . 9 5 Incremental sampling methods . 9 5.1 General 9 5.2 Sampling apparatus 9 5.3 Procedure 11 5.4 Aggregate and reduced samples . 12 6 Final samples . 12 6.1 Division into final samples . 12 6.2 Practical arrangements for final (laboratory) samples .

16、12 6.2.1 Final sample packaging materials . 12 6.2.2 Dealing with final samples 12 7 Sampling report 12 Annex A (informative) Determination of mass/volume of a static heap 13 A.1 Volume of a conical heap without edgewise limitation 13 A.2 Volume of a storage box, partly filled (rectangular base, thr

17、ee flanks closed) . 13 A.3 Determination of the mass . 14 Annex B (informative) Alternative method according to GOST . 15 Bibliography . 16 DIN EN 1482-3:2016-10EN 1482-3:2016 (E) 3 European foreword This document (EN 1482-3:2016) has been prepared by Technical Committee CEN/TC 260 “Fertilizers and

18、liming materials”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2017, and conflicting national standards shall be withdrawn at the latest by Fe

19、bruary 2017. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights This document has been prepared under a mandate given to CEN by the European Commission a

20、nd the European Free Trade Association. EN 1482 “Fertilizers and liming materials Sampling and sample preparation” consists of three parts: Part 1: Sampling; Part 2: Sample preparation; Part 3: Sampling of static heaps. According to the CEN-CENELEC Internal Regulations, the national standards organi

21、sations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, M

22、alta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 1482-3:2016-10EN 1482-3:2016 (E) 4 Introduction The establishment of European Standards for methods of sampling and analysis is of utmost importance to guarante

23、e a uniform application and control of the European legislation in all Member States. Standardized methods of sampling and analysis are essential elements in guaranteeing a high level of quality and safety of EC fertilizers for the benefit of purchasers. In order to avoid any improper use of the ter

24、m “EC fertilizer” Member States are required to check the nutrient content of such fertilizers. To achieve this, representative sampling is essential for reliable analytical results. Competent authorities have limited resources for conformity assessment and these are most efficiently deployed at the

25、 downstream end of the supply chain. The purpose of Regulation (EC) No 2003/2003 1 is to ensure that the fertilizer meets European requirements and complies with the declaration of the required characteristics applied to it when delivered to a purchaser. EN 1482-1:2007 might not fully satisfy the ne

26、eds of Member States when a large quantity of fertilizer is stored in a static heap that cannot be realistically put into motion. An evaluation was requested to be carried out by CEN to see what, if any, static heaps of fertilizer could be representatively sampled at affordable costs see (see 3). Th

27、e fundamental principle of representative sampling is that every particle has an equal chance of being sampled. This principle cannot easily be complied with in the case of bulk static heaps of solid fertilizers as a large proportion of the material cannot practically be reached by any sampling devi

28、ce. Wherever possible, this fertilizer should be sampled during transfer, during the building up of the heap, during dispatch or where it can practically be moved solely for sampling purposes. However, in some cases, sampling in the way described is not practicable. The European Commission asked CEN

29、/TC 260/WG 1 to draft a European Standard in response to mandate M/454, which requires the development of a method of sampling static heaps that could not be sampled according to EN 1482-1:2007. This states that the sampling of static heaps should only be carried out when the product is in motion. I

30、n response to the mandate, sampling methods to sample static heaps have been developed and standardized as specified in this document. DIN EN 1482-3:2016-10EN 1482-3:2016 (E) 5 1 Scope This European Standard is applicable to the sampling of mineral fertilizers and liming materials supplied or ready

31、for supply to third parties, as a lot or in smaller lots, where such supply or readiness for supply is subject to legal requirements. This European Standard specifies plans and methods of sampling of a lot of solid fertilizer or liming material, if sampling in motion is not possible, to obtain sampl

32、es from static bulk heaps in order to ascertain compliance with legal requirements, in particular in relation to the accuracy of compulsory or permitted statutory declarations. The methods specified in this document are not applicable to obtain samples for physical analysis or for the chemical analy

33、sis which may be altered by particle granulometric segregation. This European Standard is applicable to single nutrient fertilizers, to uniform complex fertilizers and to milled or granulated liming materials. The methods described in this document are not suitable for sampling other types of fertil

34、izer, for example blended fertilizers. NOTE The term fertilizer is used throughout the body of this European Standard and includes liming materials unless otherwise indicated. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are ind

35、ispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1482-1:2007, Fertilizers and liming materials - Sampling and sample preparation - Part 1: Sampling 3 Term

36、s and definitions For the purposes of this document, the terms and definitions given in EN 1482-1:2007 and the following apply. 3.1 fertilizer solid inorganic material designated for use as a fertilizer including liming materials 3.2 sampling point point in the sampling unit from which a sub-sample

37、is taken Note 1 to entry: For the definition of sub-sample, see EN 14821:2007, Note in 3.5. 3.3 static heap quantity of fertilizer stored in bulk in a single mass 4 Sampling plans and quantitative data 4.1 General The objective of sampling is to acquire a sample of the lot to establish its compositi

38、on and properties. The methods to be used for sampling static heaps are specified in the following clauses. DIN EN 1482-3:2016-10EN 1482-3:2016 (E) 6 4.2 Characterization of the lot to be sampled Before a sampling plan is determined, a description of the characteristics of the lot that is intended t

39、o be sampled shall be undertaken. In particular, the following physical characteristics shall be noted: kind/type, texture, colour, storage conditions, e.g. uncovered/covered, foreign matters. If the owner of the material is applying the same description and statutory information to the whole lot, s

40、ampling should proceed in accordance with this document. Only if there is evidence of deterioration or contamination should consideration be given to the dividing of the lot into parts from which separate samples should be taken. 4.3 Sampling plan 4.3.1 General The sampling plan shall be determined

41、after the characteristics according to 4.2 have been considered. Any variations from the stated sampling plan shall be documented in written form. The sampling plan shall define the course of the sampling process, and associated provisions, in reproducible manner. Sampling only around the base of th

42、e heap or from a single part of the heap does not supply a representative sample. 4.3.2 Elements of the sampling plan Within the sampling plan, the following elements shall be stated: boundary of the lot, determination of the volume/mass of the lot, determination of the number and location of sampli

43、ng units, determination of sampling units from which the increments shall be taken, if necessary, preparation of a sketch-map of the sampling areas (see Figure 1), determination of the minimum number of sampling points from which sub-samples are to be taken to form the incremental sample, determinat

44、ion of minimum volume/mass of increments. DIN EN 1482-3:2016-10EN 1482-3:2016 (E) 7 Key 1 conveyor belt 1 to 32 number of sampling units of equivalent surface 10 random selected sampling units for sampling + sampling points (random distribution in the sampling unit) top ring 2 sampling units (180 ea

45、ch) second ring 6 sampling units (60 each) third ring 8 sampling units (45 each) fourth ring 16 sampling units (22,5 each) Characteristics of the heap: angle of repose: 36 base diameter: 12 m height: 5,3 m circumference: 37,70 m ridge: 8 m volume: 200 m3Figure 1 Example of sampling plan for a conica

46、l heap (developed) DIN EN 1482-3:2016-10EN 1482-3:2016 (E)8 4.4 Determination of the volume/mass of the lot The volume/mass of the lot should either be determined by reference to production/purchase/sales records of the owner or, if this is not possible, shall be estimated by the methods described i

47、n Annex A. 4.5 Determination of sampling units and sampling points 4.5.1 Determination of the number and location of the sampling units The total minimum number of sampling units depends on the size of the lot. Each sampling unit will be represented by approximately the same surface area. 4.5.2 Mini

48、mum total number of sampling units The total number of sampling units into which the lot has to be divided shall be determined in accordance with Table 1. Table 1 Number of sampling units that the lot needs be divided into Lot size t Minimum number of sampling units 25 or less 10 More than 25 and up

49、 to 400 The nearest whole even number above the square root of 4 times the quantity, in tonnes, present More than 400 40 4.5.3 Determination of sampling units from which incremental samples shall be taken Select randomly a minimum of 10 sampling units from the total number of sampling units determined in accordance with 4.5.2 using random number tables or a random number generator. Incremental samples shall be taken from the sele