DIN EN 1903-2015 Adhesives - Test method for adhesives for plastic or rubber floor coverings or wall coverings - Determination of dimensional changes after accelerated ageing Germa.pdf

1、July 2015 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 83

2、180!%Co“2327661www.din.deDDIN EN 1903Adhesives Test method for adhesives for plastic or rubber floor coverings or wallcoverings Determination of dimensional changes after accelerated ageing;English version EN 1903:2015,English translation of DIN EN 1903:2015-07Klebstoffe Prfverfahren fr Klebstoffe

3、fr Boden- und Wandbelge aus Kunststoff oder Gummi Bestimmung der Manderungen nach beschleunigter Alterung;Englische Fassung EN 1903:2015,Englische bersetzung von DIN EN 1903:2015-07Adhsifs Mthodes dessai des adhsifs pour revtements de sol ou muraux en plastique ou encaoutchouc Dtermination des varia

4、tions dimensionnelles aprs un vieillissement acclr;Version anglaise EN 1903:2015,Traduction anglaise de DIN EN 1903:2015-07SupersedesDIN EN 1903:2008-06www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.Document comprises 11 pages 06.15 DIN EN 1903:2015-07 2

5、 A comma is used as the decimal marker. National foreword This document (EN 1903:2015) has been prepared by Technical Committee CEN/TC 193 “Adhesives” (Secretariat: AENOR, Spain). The responsible German body involved in its preparation was the DIN-Normenausschuss Materialprfung (DIN Standards Commit

6、tee Materials Testing), Working Committee NA 062-10-01 AA Prfung von Klebstoffen fr Bodenbelge, Wand- und Deckenbekleidung. Amendments This standard differs from DIN EN 1903:2008-06 as follows: a) roller dimensions have been changed. Previous editions DIN EN 1903: 1999-10, 2008-06 EUROPEAN STANDARD

7、NORME EUROPENNE EUROPISCHE NORM EN 1903 April 2015 ICS 83.180 Supersedes EN 1903:2008English Version Adhesives - Test method for adhesives for plastic or rubber floor coverings or wall coverings - Determination of dimensional changes after accelerated ageing Adhsifs - Mthodes dessai des adhsifs revt

8、ements de sol ou mura en plastique ou en caoutchouc - D termination des variations dimensionnelles aprs un vieillissement acclr Klebstoffe - Prfverfahren fr Klebstoffe fr Boden- und Wandbelge aus Kunststoff oder Gummi - Bestimmung der Manderungen nach beschleunigter Alterung This European Standard w

9、as approved by CEN on 16 February 2015. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such

10、 national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own

11、language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Gr

12、eece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUN

13、G CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2015 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 1903:2015 EpouruxEN 1903:2015 (E) 2 Contents Page Foreword 3 1 Scope 4 2 Normative references 4 3 Terms and def

14、initions .4 4 Principle 4 5 Apparatus and materials .4 6 Preparation of test specimens .7 6.1 Conditioning of fibre cement substrate.7 6.2 Conditioning of test covering .7 6.2.1 Room temperature storage .7 6.2.2 Elevated temperature pre-treatment 7 6.3 Sampling and conditioning of adhesive 7 6.4 Dat

15、um points 7 6.4.1 Fixing of gauge positions .7 6.4.2 Edge to edge measurements 7 6.5 Initial measurements of dimensions prior to bonding.7 6.6 Preparation of bonded test specimens .8 6.6.1 Cleaning 8 6.6.2 Application of adhesive 8 6.6.3 Bonding 8 7 Procedure .8 7.1 Preconditioning 8 7.2 Conditionin

16、g cycle (accelerated ageing) .8 7.3 Subsequent cycles 8 8 Evaluation and expression of results 9 9 Test report 9 DINEN 1903:2015-07EN 1903:2015 (E) 3 Foreword This document (EN 1903:2015) has been prepared by Technical Committee CEN/TC 193 “Adhesives”, the secretariat of which is held by AENOR. This

17、 European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by October 2015 and conflicting national standards shall be withdrawn at the latest by October 2015. Attention is drawn to the possibility that some of the

18、 elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 1903:2008. The main change in respect to EN 1903:2008 is the change of the roller dimensions. SAFETY PRECAUTIONS

19、 Persons using this document should be familiar with the normal laboratory practice, if applicable. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to

20、ensure compliance with any regulatory conditions. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland,

21、Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 1903:2015-07 EN 1903:2015 (E)

22、4 1 Scope This European Standard specifies a test method that measures the dimensional changes of a plastic or rubber floor or wall covering bonded to a given substrate after accelerated ageing. The term “wall covering” does not include any type of wallpaper. 2 Normative references The following doc

23、uments, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 923:2005+A1:2008, Adh

24、esives - Terms and definitions EN 1067, Adhesives - Examination and preparation of samples for testing EN ISO 9142, Adhesives - Guide to the selection of standard laboratory ageing conditions for testing bonded joints (ISO 9142) EN ISO 15605, Adhesives - Sampling (ISO 15605) ISO 554, Standard atmosp

25、heres for conditioning and/or testing - Specifications 3 Terms and definitions For the purposes of this document, the terms and definitions given in EN 923:2005+A1:2008 and the following apply. 3.1 covering flexible resilient or textile floor covering or wall covering 3.2 adhesive for coverings adhe

26、sive which is intended to produce firm and durable bonds between coverings and various substrates 4 Principle This test method gives a measure of the suitability of a plastic or rubber floor or wall covering/adhesive combination by monitoring dimensional changes during defined conditioning sequences

27、 when bonded to a specific substrate. 5 Apparatus and materials 5.1 Notched trowel (for the shape of the notch, see Figure 1) with dimensions a, b and c specified by the adhesive manufacturer. DINEN 1903:2015-07EN 1903:2015 (E) 5 Key a notch depth b notch width c notch distance Figure 1 Shape of not

28、ches of notched trowels 5.2 Roller, of width (60 5) mm, diameter (90 5) mm and total mass (3,50 0,05) kg with a handle at 90 to the axis (as an example, see Figure 2). Dimensions in millimetres Figure 2 Roller NOTE The length of the handle is not critical and can be used for setting the total mass.

29、5.3 Heating chamber, ventilated and adjustable to a temperature between 20 C and 200 C according to EN ISO 9142. 5.4 Primer, if applicable. DIN EN 1903:2015-07 EN 1903:2015 (E) 6 5.5 Test covering, three test pieces for each combination with adhesive dimensions of (250 5) mm (250 5) mm or (300 5) mm

30、 (300 5) mm. 5.6 Substrate, one uncoated fibre cement panel, fully compressed and autoclaved, of a minimum thickness of approximately 8,0 mm for each test piece. Dimensions shall not be greater than 50 mm longer than the distance between the datum points, i.e. each datum point shall not be greater t

31、han (25 1) mm from the outer edge (see Figure 3). NOTE 1 The thickness is not critical. NOTE 2 Depending on the source of the fibre cement panels the surfaces can differ with respect to gloss, absorbency and strength. In this case, it is important to do some preliminary assessment (i.e. peel tests)

32、of the panels to identify the preferred side for testing. The preferred side will be called the upper side of the substrate in this standard. Dimensions in millimetres Key 1 grain direction a measurements between studs b edge to edge measurements Figure 3 Measurements Where edge to edge measurements

33、 are being carried out, recommended dimensions are approximately 300 mm 300 mm. 5.7 Suitable measuring devices, capable of measuring to the nearest 0,01 mm over a length of either 200 mm or 250 mm, e.g. an elongation meter. 5.8 Adhesives, for fixing gauge studs to the covering surface if required by

34、 the measuring method. DIN EN 1903:2015-07 EN 1903:2015(E)7 6 Preparation of test specimens 6.1 Conditioning of fibre cement substrate Place the test panels (5.6) in a heating chamber (5.3) for 6 h at (80 2) C. Ensure that the test panels are spaced in such a way as to enable a free passage of air o

35、ver them. At the end of this period, remove the test panels from the heating oven and store in a standard atmosphere of (23 2) C and (50 5) % relative humidity for at least 48 h prior to use. 6.2 Conditioning of test covering 6.2.1 Room temperature storage Condition all test pieces (5.5) in a standa

36、rd atmosphere of (23 2) C and (50 5) % relative humidity for at least 24 h prior to use. 6.2.2 Elevated temperature pre-treatment Place the test pieces (5.5) on a firm horizontal substrate (5.6) and heat for 6 h in a heating chamber (5.3) at (80 2) C. Ensure that the test pieces and substrate are sp

37、aced in such a way as to enable a free passage of air over them. At the end of this period, remove the test pieces and supports from the heating chamber and store for 48 h in a standard atmosphere of (23 2) C and (50 5) % relative humidity prior to use. The pre-treatment will release any stresses in

38、 the covering so that it is in a relaxed state when the actual test is commenced. The pre-treatment of the test coverings may be run together with the conditioning of the substrate (6.2). In most cases a more practical assessment is required. Pre-conditioning of the floor or wall covering materials

39、at elevated temperature (6.2.2) may not be regarded as necessary. If knowledge of dimensional changes after this pre-treatment is required, dimensions should be measured as given in 6.5 before and after the pre-treatment. 6.3 Sampling and conditioning of adhesive Take a sample in accordance with EN

40、ISO 15605 of the adhesive to be tested and examine and prepare it in accordance with EN 1067. Condition the adhesive in a standard atmosphere of (23 2) C and (50 5) % relative humidity for at least 24 h before making the test specimens, in accordance with ISO 554. 6.4 Datum points 6.4.1 Fixing of ga

41、uge positions Using the appropriate adhesive, fix the gauge studs in four positions, each being (25 1) mm from the outer edge of the covering (see Figure 3). 6.4.2 Edge to edge measurements Test specimens shall be marked at positions (25 1) mm from each edge. 6.5 Initial measurements of dimensions p

42、rior to bonding Measure the dimension of each test piece along the two datum lines LL and MM parallel to its grain, when this can be identified, (longitudinally) and the two datum lines PP and QQ at right angles to these lines (transversely). Record as measurement A. DINEN 1903:2015-07EN 1903:2015 (

43、E) 8 Depending on the type of measuring device to be used, the measurements may be made from edge to edge or from scribe datum marks as described previously (see Figure 3). 6.6 Preparation of bonded test specimens 6.6.1 Cleaning Ensure that all floor coverings and fibre cement panels are clean and f

44、ree from dust, loose particles or other contamination. NOTE For unbonded control test specimens, if required, test pieces are laid directly onto the fibre cement panels. 6.6.2 Application of adhesive Apply the adhesive (5.4) to the upper side of the substrate (5.6) using a notched trowel (5.1) held

45、at an angle of approximately 60 to the slab, comb the adhesive to provide a uniform application. Hold the trowel at a right angle to one edge of the slab and draw it across the slab parallel to that edge in a straight line. When applying the adhesive, it is essential that the serrated blade is kept

46、clean and free of adhesive build-up. Clean the blade regularly (no more than three fibre cement panels to be prepared without cleaning). In addition, regularly check the notch size and depth, especially where non-hardened steel blades are in use. 6.6.3 Bonding After a time recommended by the adhesiv

47、e manufacturer (i.e. minimum open time in accordance with EN 923), place a test piece on the prepared panel ensuring that the machine direction of the test piece is at right angles to the adhesive ridges. Smooth with light hand pressure and then roll with a roller (5.2) starting at one edge rolling

48、up and down and gradually moving across the panel ensuring all areas are rolled. Repeat the rolling in a direction at right angles to the first rolling. NOTE For coverings which show a tendency to curl after rolling, a dead load of (5,0 0,25) kg mass can be applied (3,0 0,5) h onto the test specimens. The load is spread evenly over the whole surface thus ensuring a contact over the total bonded area. 7 Procedure 7.1 Preconditioning Condition test s