1、July 2013 Translation by DIN-Sprachendienst.English price group 11No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 7
2、5.160.20!%e“2042966www.din.deDDIN EN 16329Diesel and domestic heating fuels Determination of cold filter plugging point Linear cooling bath method;English version EN 16329:2013,English translation of DIN EN 16329:2013-07Dieselkraftstoffe und Haushaltsheizle Bestimmung des Temperaturgrenzwertes der F
3、iltrierbarkeit Verfahren mit einem linearen Khlbad;Englische Fassung EN 16329:2013,Englische bersetzung von DIN EN 16329:2013-07Combustibles pour moteurs diesel et pour installations de chauffages domestiques Dtermination de la temprature limite de filtrabilit Mthode au bain refroidissement linaire;
4、Version anglaise EN 16329:2013,Traduction anglaise de DIN EN 16329:2013-07www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.Document comprises 20 pages 07.13 DIN EN 16329:2013-07 2 A comma is used as the decimal marker. National foreword This document (EN 1
5、6329:2013) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin” (Secretariat: NEN, Netherlands). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Mat
6、erials Testing Standards Committee), Working Committee NA 062-06-42 AA Prfung von flssigen Kraft-stoffen und Heizlen of the Fachausschuss Minerall- und Brennstoffnormung. The DIN Standards corresponding to the International Standards referred to in this document are as follows, whereby EN ISO Standa
7、rds are only listed below if these have not been published as DIN EN ISO Standards with the same number: ISO 261 DIN ISO 261 ISO 3310-1 DIN ISO 3310-1 National Annex NA (informative) Bibliography DIN ISO 261, ISO general purpose metric screw threads General plan DIN ISO 3310-1, Test sieves Technical
8、 requirements and testing Part 1: Test sieves of metal wire cloth EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 16329 May 2013 ICS 75.160.20 English Version Diesel and domestic heating fuels - Determination of cold filter plugging point - Linear cooling bath method Combustibles pour moteurs d
9、iesel et pour installations de chauffages domestiques - Dtermination de la temprature limite de filtrabilit - Mthode au bain refroidissement linaire Dieselkraftstoffe und Haushaltsheizle - Bestimmung des Temperaturgrenzwertes der Filtrierbarkeit - Verfahren mit einem linearen Khlbad This European St
10、andard was approved by CEN on 21 March 2013. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning
11、 such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its
12、 own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, German
13、y, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR N
14、ORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2013 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16329:2013: EEN 16329:2013 (E) 2 Contents Page Foreword 3 1 Scope 5 2 Normative references 5 3 Terms and definitions .
15、5 4 Principle 6 5 Reagents and materials 6 6 Apparatus .6 7 Sampling 14 8 Preparation of the test sample 14 9 Preparation of apparatus . 14 10 Procedure 14 11 Calibration . 15 11.1 General . 15 11.2 Thermometers calibration 15 11.3 Cooling unit . 15 11.4 Vacuum unit 15 12 Expression of results . 15
16、13 Precision 16 13.1 General . 16 13.2 Repeatability 16 13.3 Reproducibility 16 14 Test report . 16 Annex A (normative) Thermometer requirements 17 Bibliography . 18 DIN EN 16329:2013-07 EN 16329:2013 (E) 3 Foreword This document (EN 16329:2013) has been prepared by Technical Committee CEN/TC 19 “Ga
17、seous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by Nov
18、ember 2013, and conflicting national standards shall be withdrawn at the latest by November 2013. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such pat
19、ent rights. According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
20、 France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 16329:2013-07 EN 16329:2013 (E) 4 Introduction This document specifi
21、es in detail an automated method as an alternative technique to EN 116:1997 1. The cooling bath is no longer operated in several temperature stages (as in EN 116), but is replaced by a refrigeration unit with linear cooling. Round Robin studies conducted for this determination method 2 showed improv
22、ed precision compared to EN 116:1997. The studies covered currently marketed fuels, including non-fossil components (FAME-blends) or biofuels. Although a bias has been identified during the statistical comparison of EN 116 and this document, this is not considered to be significant because the bias
23、is within the repeatability of both methods. The range of CFPP values for the fuels for the Round Robin therefore the basis of the determined precision was from 47 C to +11 C, but the results also showed indications of issues for fuel samples with a CFPP below 30 C. Further CEN studies are planned t
24、o assess the magnitude of these issues and the bias in additional market samples. A separate study is planned to further confirm the precision for paraffinic diesel fuels as the amount of these samples included in the Round Robin had been limited. A report with further statistical details of the Rou
25、nd Robin is under development within CEN. At the same time, EN 116 1 will be revised as well following conclusions from the Round Robin studies. DIN EN 16329:2013-07 EN 16329:2013 (E) 5 1 Scope This European Standard specifies an automated method for the determination of the cold filter plugging poi
26、nt (CFPP) of diesel and domestic heating fuels using linear cooling. This European Standard is applicable to fatty-acid methyl esters (FAME) and to distillate fuels as well as paraffinic diesel fuels, including those containing FAME, flow-improvers or other additives, intended for use in diesel engi
27、nes and domestic heating installations. The results obtained from the method specified in this European Standard are suitable for estimating the lowest temperature at which a fuel will give trouble-free flow in the fuel system. NOTE In the case of diesel fuels, the results are usually close to the t
28、emperature of failure in service except when the fuel system contains, for example, a paper filter installed in a location exposed to the weather or if the filter plugging temperature is more than 12 C below the cloud point of the fuel. Domestic heating installations are usually less critical and of
29、ten operate at a satisfactory level at temperatures somewhat lower than those indicated by the test results. WARNING The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is
30、 the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indis
31、pensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN ISO 3170, Petroleum liquids Manual sampling (ISO 3170) EN ISO 3171, Petroleum liquids Automatic pipeline sa
32、mpling (ISO 3171) ISO 261, ISO general purpose metric screw threads General plan 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 cold filter plugging point CFPP highest temperature at which a given volume of fuel fails to pass through a stand
33、ardized filtration device in a specified time, when cooled under standardized conditions DIN EN 16329:2013-07 EN 16329:2013 (E) 6 4 Principle This European Standard describes the use of automated test equipment only. A test portion of the fuel is cooled under the specified conditions and is drawn at
34、 intervals of 1 C into a pipette under a controlled vacuum of 2 kPa through a standardized wire mesh filter. The procedure is repeated, as the fuel continues to cool, for each 1 C below the first test temperature. Testing is continued until the amount of wax crystals, which have separated out of sol
35、ution, is sufficient to stop or slow down the flow so that the time taken to fill the pipette exceeds 60 s or the fuel fails to return completely to the test jar before the fuel has cooled by a further 1 C. The indicated temperature at which the last filtration was commenced is recorded as the cold
36、filter plugging point (CFPP). 5 Reagents and materials 5.1 Hydrocarbon solvents, technical grade, e.g. Heptane 5.2 Light hydrocarbon solvents, technical grade, e.g. Isopentane 5.3 Lintless filter paper, with particle retention of 30 m 5.4 Certified reference materials NOTE Certified reference materi
37、als can be obtained from the European Commission, JRC. The Institute for Reference Materials and Measurements (IRMM), Retieseweg 111, B-2440 Geel, Belgium, can be contacted to obtain further information. 6 Apparatus 6.1 General The equipment is described in detail in 6.2 to 6.12. Unless otherwise st
38、ated, all dimensions in the figures are given in mm. IMPORTANT Parts of the apparatus made of copper, zinc or brass can interact with bio-components like Fatty Acid Methyl Ester (FAME). Care shall be taken. Parts made from alternative materials are available. 6.2 Test jar, cylindrical, of clear glas
39、s, flat bottomed, with an outside diameter of (34 0,5) mm, a wall thickness of (1,20 0,15) mm and a height of (120 5) mm. The jar shall have a permanent mark at the 45 ml level. 6.3 Jacket, watertight, cylindrical, flat bottomed, to be used as an air bath. It shall have an inside diameter of (45 0,2
40、5) mm and a height of (115 3) mm. 6.4 Spacer, made from POM-C1), except for the stainless steel rods with 2 mm diameter, to be placed into the jacket (6.3), conforming to the dimensions as shown in Figure 1. 1) POM-C Polyoxymethylen Copolymer, trademarks e.g. DELRIN. DIN EN 16329:2013-07 EN 16329:20
41、13 (E) 7 Dimensions in millimetres Key 1 rod (3 in total) Figure 1 Spacer 6.5 Stopper, of oil-resistant and non-thermal conductive material, having three holes to accommodate the pipette with filter unit (6.6), the thermometer (6.9) and to allow venting of the system, and able to ensure that pipette
42、 and thermometer are safely positioned in the test jar. DIN EN 16329:2013-07 EN 16329:2013 (E) 8 6.6 Pipette with filter unit 6.6.1 A pipette of clear glass with a volume of (20 0,2) ml at a point (149 0,5) mm from the bottom of the pipette (see Figure 2). It shall be connected to the filter unit. D
43、imensions in millimetres Figure 2 Pipette DIN EN 16329:2013-07 EN 16329:2013 (E) 9 6.6.2 A filter unit as in Figure 3, with general purpose metric screw threads according to ISO 261, further consisting of a filter holder as in Figure 4 and a disc, 15 mm diameter, stainless steel wire mesh gauze with
44、 a nominal aperture size of 45 m in basket weave (not twill). The nominal diameter of the wire shall be 32 m and the tolerance for the size of an individual aperture shall be as follows: a) no aperture size shall exceed the nominal size by more than 22 m; b) the average aperture size shall be within
45、 3,1 m of the nominal size; and c) not more than 6 % of the apertures shall be above the nominal size by more than 13 m. NOTE The requirements for the wire mesh are taken from ISO 3310-1 3, to which reference may be made for methods for testing the gauze. DIN EN 16329:2013-07 EN 16329:2013 (E) 10 Di
46、mensions in millimetres Key 1 pipette (6.6.1) 2 filter holder (see Figure 4) Figure 3 Filter unit DIN EN 16329:2013-07 EN 16329:2013 (E) 11 Dimensions in millimetres Figure 4 Filter holder 6.7 An automated detection system comprising one sensor to record the filling of the pipette at a volume of (20
47、 0,2) ml, and a second sensor positioned (85 4) mm from the bottom of the pipette to check for the complete flow back of the sample to the test jar before the start of the next aspiration cycle. 6.8 A valve unit that connects the pipette either to the vacuum regulator, to allow sample to be drawn un
48、der vacuum into the pipette, or to the atmosphere to allow backflow of the sample to the test jar. The connecting line between the valve unit and the pipette should have a maximum length of 2 m, and an internal diameter of between 4 mm and 6 mm. 6.9 The following thermometers shall be used: 6.9.1 A platinum resistance thermometer conforming to the essential dimensions set out in Annex A, with digital display, shall be used for measuring the sample temperature
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