DIN EN 16602-70-29-2015 Space product assurance - Determination of offgassing products from materials and assembled articles to be used in a manned space vehicle crew compartment E.pdf

1、Juni 2015DEUTSCHE NORM DIN-Normenausschuss Luft- und Raumfahrt (NL)Preisgruppe 13DIN Deutsches Institut fr Normung e. V. Jede Art der Vervielfltigung, auch auszugsweise, nur mit Genehmigung des DIN Deutsches Institut fr Normung e. V., Berlin, gestattet.ICS 49.140!%B-“2311010www.din.deDDIN EN 16602-7

2、0-29Raumfahrtproduktsicherung Bestimmung der Abgabe von Fremdstoffen durch Werkstoffe undBauteile im Mannschaftsraum von Raumfahrzeugen;Englische Fassung EN 16602-70-29:2014Space product assurance Determination of offgassing products from materials and assembled articles to be used ina manned space

3、vehicle crew compartment;English version EN 16602-70-29:2014Assurance produit des projets spatiaux Dtermination des produits de dgazage sous atmosphre pour les matriaux et lmentsassembls utiliss dans le poste dquipage du satellite habit;Version anglaise EN 16602-70-29:2014Alleinverkauf der Normen du

4、rch Beuth Verlag GmbH, 10772 BerlinErsatz frDIN EN 14100:2002-10www.beuth.deGesamtumfang 25 SeitenDIN EN 16602-70-29:2015-06 2 Nationales Vorwort Dieses Dokument (EN 16602-70-29:2014) wurde vom Technischen Komitee CEN/CLC/TC 5 Raumfahrt“ erarbeitet, dessen Sekretariat vom DIN (Deutschland) gehalten

5、wird. Das zustndige deutsche Normungsgremium ist der Arbeitsausschuss NA 131-10-01 AA Interoperabilitt von Informations-, Kommunikations- und Navigationssystemen“ im DIN-Normenausschuss Luft- und Raumfahrt (NL). Dieses Dokument ersetzt DIN EN 14100:2002-10. Dieses Dokument (EN 16602-70-29:2014) basi

6、ert auf ECSS-Q-ST-70-29C. Dieses Dokument enthlt unter Bercksichtigung des DIN-Prsidialbeschlusses 1/2004 nur die englische Originalfassung von EN 16602-70-29:2014. Dieses Dokument wurde speziell zur Behandlung von Raumfahrtsystemen erarbeitet und hat daher Vorrang vor jeglicher Europischer Norm, da

7、 es denselben Anwendungsbereich hat, jedoch ber einen greren Geltungsbereich (z. B. Luft- und Raumfahrt) verfgt. nderungen Gegenber wird DIN EN 14100:2002-10 wurden folgende nderungen vorgenommen: a) Norm-Nummer gendert; b) keinerlei nderungen des Textes. Frhere Ausgaben DIN EN 14100: 2002-10 DIN EN

8、 16602-70-29:2015-06 3 Nationaler Anhang NA (informativ) Begriffe und Abkrzungen 3 Begriffe und Abkrzungen 3.1 Begriffe aus anderen Normen Fr die Anwendung dieses Dokuments gelten die Begriffe nach ECSS-S-ST-00-01 und ECSS-Q-ST-70. 3.2 Fr diese Norm spezifische Begriffe 3.2.1 Bauteil Bauelement mit

9、unbekannten Bestandteilen oder Einheit, die fr die in einem Raumfahrzeug eingesetzte Einheit reprsentativ ist 3.2.2 Prfaufbau fr einen bestimmten Zweck entwickelte und gebaute Einheit, die zerlegt werden kann und ihre Eigenschaften nach einem Wieder-Zusammenbau beibehlt 3.2.3 Fremdstoffabgabe Abgabe

10、 gasfrmiger Substanzen durch ein Bauteil, das in einer festgelegten Prfatmosphre schwacher Wrmestrahlung ausgesetzt wird 3.2.4 Fremdstoff aus einem Werkstoff, Bauteil, Prfaufbau oder Gestell freigesetzte organische oder anorganische Verbindung 3.2.5 Gestell Struktur, an der whrend einer bemannten Mi

11、ssion verschiedene Experimente vorgenommen werden 3.2.6 hchstzulssige Konzentration in einem Raumfahrzeug SMAC (en: Spacecraft Maximum Allowable Concentration) hchste Konzentration an einem flchtigen Fremdstoff, die fr eine festgelegte Flugdauer in der Atmosphre eines Raumfahrzeugs zulssig ist 3.2.7

12、 Toxizittsfaktor T Verhltnis der projizierten Konzentration der einzelnen Fremdstoffe zu deren SMAC-Wert und Addition der Verhltnisse aller Fremdstoffe, unabhngig von deren toxikologischer Kategorie ANMERKUNG Weitere Einzelheiten zur Berechnung dieses T-Werts knnen NASA-STD-6001 entnommen werden. DI

13、N EN 16602-70-29:2015-06 4 3.3 Abkrzungen Fr die Anwendung dieses Dokuments gelten die Abkrzungen in ECSS-S-ST-00-01 und die folgenden Abkrzungen: Abkrzung Bedeutung C Konzentration, angegeben in g/m3(en: concentration expressed in g/m3) C1Konzentration, angegeben in ppm (en: concentration expressed

14、 in ppm) CIchemische Ionisation (en: chemical ionization) EI elektronische Ionisation (en: electron ionization) eV Elektronenvolt (en: electron volt) GC Gaschromatograph (en: gas-chromatograph) MS Massenspektrometer (en: mass-spectrometer) MWt Moleklmasse (en: molecular weight) m/z Masse-zu-Ladung-V

15、erhltnis (en: ratio mass to charge) ppm Teile je Million (en: parts per million) SMAC hchstzulssige Konzentration in einem Raumfahrzeug (en: Spacecraft Maximum Allowable Concentration) T Toxizittsfaktor (en: toxic hazard index) ANMERKUNG Fr g/m3erfolgt die Umrechnung in ppm nach der Formel (3-1) in

16、3.4. 3.4 Umrechnungsformel Formel (3-1) gibt die Umrechnung von g/m3in ppm an: tPMWCC+=273298013147,24103t1(3-1) Dabei ist C die Konzentration (g/m3); C1die Konzentration (ppm); MWt die Moleklmasse (g); P der Druck (hPa); t die Raumtemperatur (C) (Ende der Prfung); 24,47 das Moleklvolumen bei 25 C (

17、l). EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 16602-70-29 October 2014 ICS 49.140 Supersedes EN 14100:2001 English version Space product assurance - Determination of offgassing products from materials and assembled articles to be used in a manned space vehicle crew compartment Assurance p

18、roduit des projets spatiaux - Dtermination des produits de dgazage sous atmosphre pour les matriaux et lments assembls utiliss dans le poste dquipage du satellite habit Raumfahrtproduktsicherung - Bestimmung der Abgabe von Fremdstoffen durch Werkstoffe und Bauteile im Mannschaftsraum von Raumfahrzeu

19、gen This European Standard was approved by CEN on 11 April 2014. CEN and CENELEC members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibli

20、ographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN and CENELEC member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under

21、 the responsibility of a CEN and CENELEC member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN and CENELEC members are the national standards bodies and national electrotechnical committees of Austria, Belgium, Bulgaria, Croa

22、tia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and U

23、nited Kingdom. CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014 CEN/CENELEC All rights of exploitation in any form and by any means reserved worldwide for CEN national Members and for CENELEC Members. Ref. No. EN 16602-70-29:2014 E EN 16602-70-29:2014 (E) 2 Table of contents For

24、eword 4 1 Scope . 5 2 Normative references . 6 3 Terms, definitions and abbreviated terms 7 3.1 Terms defined in other standards . 7 3.2 Terms specific to the present standard . 7 3.3 Abbreviated terms. 8 3.4 Formula for conversion . 8 4 Requirements 9 4.1 Preparatory conditions 9 4.1.1 Test specime

25、n preparation 9 4.1.2 Cleaning 11 4.1.3 Identification 11 4.2 Test facility 11 4.2.1 General requirements . 11 4.2.2 Test chamber 11 4.2.3 Sampling equipment . 12 4.2.4 Analytical equipment . 12 4.2.5 Resolution (Static): at the slit settings provided, the resolution definition (10 % valley) is with

26、in the values listed in Gas supplies . 13 4.2.6 Gas supplies . 13 4.3 Test chamber certification procedure 13 4.4 Test procedure . 14 4.4.1 Test conditions 14 4.4.2 Test execution . 14 4.4.3 Analysis of samples 15 4.5 Acceptance limits 15 4.5.1 Materials . 15 4.5.2 Assembled articles, experiments an

27、d racks. 15 4.6 Quality assurance . 16 4.6.1 Data 16 DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 3 4.6.2 Calibration . 16 Annex A (normative) Offgassing evaluation report - DRD 17 Annex B (informative) Example of test method procedure . 19 Bibliography . 21 Tables Table 4-1: Slits setting 13

28、DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 4 Foreword This document (EN 16602-70-29:2014) has been prepared by Technical Committee CEN/CLC/TC 5 “Space”, the secretariat of which is held by DIN. This standard (EN 16602-70-29:2014) originates from ECSS-Q-ST-70-29C. This European Standard shall

29、 be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2015, and conflicting national standards shall be withdrawn at the latest by April 2015. Attention is drawn to the possibility that some of the elements of this document

30、may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 14100:2001. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association

31、. This document has been developed to cover specifically space systems and has therefore precedence over any EN covering the same scope but with a wider domain of applicability (e.g. : aerospace). According to the CEN-CENELEC Internal Regulations, the national standards organizations of the followin

32、g countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norw

33、ay, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 5 1 Scope All non-metallic materials release trace contaminants into the surrounding environment; the extent to which this occurs is depend

34、ent on the nature of the material concerned. In the closed environment of a manned spacecraft contaminants within the atmosphere are potentially dangerous with respect to toxicity and its consequences for the safety of the crew. This Standard defines a test procedure for the determination of the tra

35、ce contaminants release by non-metallic materials under a set of closely controlled conditions. The test procedure covers both individual materials and assembled articles. In this Standard the supplier means the testing authority that is responsible for specifying and executing the offgassing tests.

36、 This Standard describes a test to provide data for aid in the evaluation of the suitability of assembled articles and materials for use in a space vehicle crew compartment. The data obtained are in respect of the nature and quantity of organic and inorganic volatile contaminants evolved when subjec

37、ted to the crew compartment environment. This standard may be tailored for the specific characteristics and constrains of a space project in conformance with ECSS-S-ST-00. DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 6 2 Normative references The following normative documents contain provisions

38、 which, through reference in this text, constitute provisions of this ECSS Standard. For dated references, subsequent amendments to, or revision of any of these publications do not apply, However, parties to agreements based on this ECSS Standard are encouraged to investigate the possibility of appl

39、ying the more recent editions of the normative documents indicated below. For undated references, the latest edition of the publication referred to applies. EN reference Reference in text Title EN 16601-00-01 ECSS-S-ST-00-01 ECSS system Glossary of terms EN 16602-10-09 ECSS-Q-ST-10-09 Space product

40、assurance Nonconformance control system EN 16602-70 ECSS-Q-ST-70 Space product assurance Materials, mechanical parts and processes DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 7 3 Terms, definitions and abbreviated terms 3.1 Terms defined in other standards For the purpose of this Standard, th

41、e terms and definitions from ECSS-S-ST-00-01 and ECSS-Q-ST-70 apply. 3.2 Terms specific to the present standard 3.2.1 assembled article any component “black box” or assembly of components which represents the article to be used in a spacecraft 3.2.2 experiment item designed and built to accomplish a

42、 specific purpose which can be disassembled and retain its capabilities after re-assembly 3.2.3 offgassing evolution of gaseous products for an assembled article subjected to slight radiant heat in the specified test atmosphere 3.2.4 offgassing product organic or inorganic compound evolved from a ma

43、terial or assembled article or experiment or rack 3.2.5 rack structure in which different experiments take place during a manned mission 3.2.6 SMAC (Spacecraft Maximum Allowable Concentration) maximum concentration of a volatile offgassed product that is allowed in the spacecraft atmosphere for a sp

44、ecified flight duration 3.2.7 toxic hazard index (T) ratio of the projected concentration of each offgassed product to its SMAC value and summing the ratios for all offgassed products without separation into toxicological categories NOTE Further details on the calculation of this T-value can also be

45、 obtained in NASA-STD-6001. DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 8 3.3 Abbreviated terms For the purpose of this Standard, the abbreviated terms from ECSS-S-ST-00-01 and the following apply: Abbreviation Meaning C concentration expressed in g/m3C1 concentration expressed in ppm CIchemi

46、cal ionization EI electron ionization eV electron volt GC gas-chromatograph MS mass-spectrometer MWt molecular weight m/z ratio mass to charge ppm part per million SMAC Spacecraft Maximum Allowable Concentration T toxic hazard index NOTE For g/m3, the conversion to ppm is done, using the formula (3-

47、1) given in clause 3.4 3.4 Formula for conversion Formula (3-1) shows the conversion from g/m3to ppm: tPMWCCt+=273298013147,241031(3-1) Where: C is the concentration (g/m3) C1 is the concentration (ppm) MWt is the molecular weight (g) P is the pressure (hPa) t is the room temperature (C) (End of tes

48、t) 24,47 is the molecular volume at 25 C (l) DIN EN 16602-70-29:2015-06 EN 16602-70-29:2014 (E) 9 4 Requirements 4.1 Preparatory conditions 4.1.1 Test specimen preparation 4.1.1.1 General preferences a. The supplier shall classify all materials to be tested into one of the three categories “Surface”

49、, “Volume” and “Mass” described in 4.1.1.2, 4.1.1.3 and 4.1.1.4, respectively. 4.1.1.2 Samples of category “Surface” a. The category “Surface” shall include films, fabrics, coatings, finishes, inks, primers, adhesives, thin film lubricants, tapes and electrical insulating materials. NOTE This category is defined for materials that are essentially two dimensional. b. The supplier shall select test samples with a surface of (300 10) cm2per litre of test c