DIN EN ISO 11127-7-2012 Preparation of steel substrates before application of paints and related products - Test methods for non-metallic blast-cleaning abrasives - Part 7 Determin.pdf

1、April 2012 Translation by DIN-Sprachendienst.English price group 7No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 2

2、5.220.10!$6(“1881905www.din.deDDIN EN ISO 11127-7Preparation of steel substrates before application of paints and relatedproducts Test methods for non-metallic blast-cleaning abrasives Part 7: Determination of water-soluble chlorides (ISO 11127-7:2011)English translation of DIN EN ISO 11127-7:2012-0

3、4Vorbereitung von Stahloberflchen vor dem Auftragen von Beschichtungsstoffen Prfverfahren fr nichtmetallische Strahlmittel Teil 7: Bestimmung der wasserlslichen Chloride (ISO 11127-7:2011)Englische bersetzung von DIN EN ISO 11127-7:2012-04Prparation des subjectiles dacier avant application de peintu

4、res et de produitsassimils Mthodes dessai pour abrasifs non mtalliques destins la prparation par projection Partie 7: Dtermination des chlorures solubles dans leau (ISO 11127-7:2011)Traduction anglaise de DIN EN ISO 11127-7:2012-04SupersedesDIN EN ISO 11127-7:1997-11www.beuth.deDocument comprises pa

5、gesIn case of doubt, the German-language original shall be considered authoritative.1003.12 DIN EN ISO 11127-7:2012-04 2 A comma is used as the decimal marker. National foreword This standard falls in the domain of Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat: DIN, Germany). It

6、 is identical with International Standard ISO 11127-7 which was prepared by Technical Committee ISO/TC 35/SC 12 “Preparation of steel substrates before application of paints and related products” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Norm

7、enausschuss Beschichtungsstoffe und Beschichtungen (Coatings and Coating Materials Standards Committee), Working Committee NA 002-00-11 AA Strahlmittel. DIN EN ISO 11127 consists of the following parts, under the general title Preparation of steel substrates before application of paints and related

8、products Test methods for non-metallic blast-cleaning abrasives: Part 1: Sampling Part 2: Determination of particle size distribution Part 3: Determination of apparent density Part 4: Assessment of hardness by a glass slide test Part 5: Determination of moisture Part 6: Determination of water-solubl

9、e contaminants by conductivity measurement Part 7: Determination of water soluble chlorides The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 3696 DIN ISO 3696 ISO 11126-1 DIN EN ISO 11126-1 ISO 11126-3 DIN EN ISO 11126-3 ISO 11126-4 DIN

10、EN ISO 11126-4 ISO 11126-5 DIN EN ISO 11126-5 ISO 11126-6 DIN EN ISO 11126-6 ISO 11126-7 DIN EN ISO 11126-7 ISO 11126-8 DIN EN ISO 11126-8 ISO 11126-9 DIN EN ISO 11126-9 ISO 11126-10 DIN EN ISO 11126-10 Amendments This standard differs from DIN EN ISO 11127-7:1997-11 as follows: a) in Annex A, the r

11、eference to ISO 11126-2 and ISO 11127-8 has been deleted; b) the standard has been brought in line with the current presentation rules. Previous editions DIN EN ISO 11127-7: 1997-11 DIN EN ISO 11127-7:2012-04 3 National Annex NA (informative) Bibliography DIN EN ISO 11126-1, Preparation of steel sub

12、strates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 1: General introduction and classification DIN EN ISO 11126-3, Preparation of steel substrates before application of paints and related products Specifications for non-metallic bla

13、st-cleaning abrasives Part 3: Copper refinery slag DIN EN ISO 11126-4, Preparation of steel substrates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 4: Coal furnace slag DIN EN ISO 11126-5, Preparation of steel substrates before appli

14、cation of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 5: Nickel refinery slag DIN EN ISO 11126-6, Preparation of steel substrates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 6: Iron furn

15、ace slag DIN EN ISO 11126-7, Preparation of steel substrates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 7: Fused aluminium oxide DIN EN ISO 11126-8, Preparation of steel substrates before application of paints and related products

16、Specifications for non-metallic blast-cleaning abrasives Part 8: Olivine sand DIN EN ISO 11126-9, Preparation of steel substrates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 9: Staurolite DIN EN ISO 11126-10, Preparation of steel su

17、bstrates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 10: Almandite garnet DIN ISO 3696, Water for analytical laboratory use Specification and test methods DIN EN ISO 11127-7:2012-04 4 This page is intentionally blank EUROPEAN STANDA

18、RD NORME EUROPENNE EUROPISCHE NORM EN ISO 11127-7 December 2011 ICS 25.220.10 Supersedes EN ISO 11127-7:1997English Version Preparation of steel substrates before application of paints and related products - Test methods for non-metallic blast-cleaning abrasives - Part 7: Determination of water-solu

19、ble chlorides Prparation des subjectiles dacier avant application de peintures et de produits assimils - Mthodes dessai pour abrasifs non mtalliques destins la prparation par projection - Partie 7: Dtermination des chlorures solubles dans leau (ISO 11127-7:2011) Vorbereitung von Stahloberflchen vor

20、dem Auftragen von Beschichtungsstoffen - Prfverfahren fr nichtmetallische Strahlmittel - Teil 7: Bestimmung der wasserlslichen Chloride (ISO 11127-7:2011) This European Standard was approved by CEN on 14 December 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which s

21、tipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This Europe

22、an Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are

23、the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden,

24、 Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref

25、. No. EN ISO 11127-7:2011: E(ISO 11127-7:2011) Contents Page EN ISO 11127-7:2011 (E) DIN EN ISO 11127-7:2012-04 2 Contents PageForeword 3 1 Scope 4 2 Normative references 4 3 Reagents .4 4 Apparatus .4 5 Sampling .5 6 Procedure .5 7 Calculation 5 8 Test report 5 Annex A (informative) International S

26、tandards for non-metallic blast-cleaning abrasives .6 Foreword This document (EN ISO 11127-7:2011) has been prepared by Technical Committee ISO/TC 35 Paints and varnishes” in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of which is held by DIN. This Europe

27、an Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by June 2012, and conflicting national standards shall be withdrawn at the latest by June 2012. Attention is drawn to the possibility that some of the elements of

28、 this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 11127-7:1997. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following c

29、ountries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, S

30、lovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 11127-7:2011 has been approved by CEN as a EN ISO 11127-7:2011 without any modification. “ EN ISO 11127-7:2011 (E) DIN EN ISO 11127-7:2012-04 3 1 ScopeThis is one of a number of parts of ISO 11127 dealing

31、with the sampling and testing of non-metallic abrasives for blast-cleaning.The types of non-metallic abrasive and requirements on each are contained in ISO 11126.The ISO 11126 and ISO 11127 series have been drafted as a coherent set of International Standards on non-metallic blast-cleaning abrasives

32、. Information on all parts of both series is given in Annex A.This part of ISO 11127 specifies a method for the determination of water-soluble chlorides in non-metallic blast-cleaning abrasives.2 Normative referencesThe following referenced documents are indispensable for the application of this doc

33、ument. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 3696, Water for analytical laboratory use Specification and test methodsISO 11127-1, Preparation of steel substrates before applic

34、ation of paints and related products Test methods for non-metallic blast-cleaning abrasives Part 1: Sampling3 ReagentsUse only reagents of recognized analytical grade and only water of at least grade 3 purity as defined in ISO 3696.3.1 Sulfuric acid, concentrated, approximately 96 % (by mass), 1,84

35、g/ml.3.2 Silver nitrate, standard volumetric solution, c(AgNO3) = 0,01 mol/l.4 ApparatusOrdinary laboratory apparatus and glassware, together with the following:4.1 Equipment for amperometric titration, any commercial equipment being suitable.4.2 Microburette.4.3 Balance, capable of weighing to an a

36、ccuracy of 0,1 g.EN ISO 11127-7:2011 (E) DIN EN ISO 11127-7:2012-04 4 5 SamplingTake a representative sample of the product to be tested, as described in ISO 11127-1.6 Procedure6.1 Carry out the determination in duplicate.6.2 Weigh a test portion of (100 0,1) g of the sample (m0) into a 250 ml flask

37、 and add (100 1) ml of water. Shake for 5 min and allow to stand for 1 h. Then shake again for 5 min and allow to settle. If the solution does not completely clear, filter it by any suitable method.6.3 Take 25 ml of the solution. Add 0,1 ml of sulfuric acid (3.1) and dilute to approximately 75 ml wi

38、th water.6.4 Titrate the solution with silver nitrate (3.2) from the microburette (4.2), noting the end point as the voltage at which the pointer of the galvanometer reverses direction.7 CalculationCalculate the water-soluble chloride content w(CI) of the abrasive, expressed as a percentage by mass,

39、 using the equationwVm( ),Cl = 0 000 355 41000wherem0is the mass, in grams, of the test portion;V is the volume, in millilitres, of silver nitrate solution (3.2) used;0,000 355 is the factor for the conversion of millilitres of silver nitrate solution, c(AgNO3) = 0,01 mol/l, to grams of CI.If the du

40、plicate determinations differ by more than 10 % (relative to the higher result), repeat the procedure described in Clause 6.Calculate the mean of two valid determinations and report the result to the nearest 0,000 1 %.8 Test reportThe test report shall contain at least the following information:a) a

41、ll details necessary to identify the product tested, in accordance with the appropriate part of ISO 11126 (see Annex A), if applicable;b) a reference to this part of ISO 11127 (ISO 11127-7);c) the result of the test;d) any deviation from the test method specified;e) the date of the test;f) the name

42、of the person who carried out the test.EN ISO 11127-7:2011 (E) DIN EN ISO 11127-7:2012-04 5 Annex A (informative) International Standards for non-metallic blast-cleaning abrasivesRequirements and test methods for non-metallic blast-cleaning abrasives are contained in ISO 11126 and ISO 11127, respect

43、ively.ISO 11126 consists of the following parts under the general title:Preparation of steel substrates before application of paints and related products Specifications for non-metallic blast-cleaning abrasives Part 1: General introduction and classification Part 3: Copper refinery slag Part 4: Coal

44、 furnace slag Part 5: Nickel refinery slag Part 6: Iron furnace slag Part 7: Fused aluminium oxide Part 8: Olivine sand Part 9: Staurolite Part 10: Almandite garnetISO 11127 consists of the following parts, under the general title:Preparation of steel substrates before application of paints and rela

45、ted products Test methods for non-metallic blast-cleaning abrasives Part 1: Sampling Part 2: Determination of particle size distribution Part 3: Determination of apparent density Part 4: Assessment of hardness by a glass slide test Part 5: Determination of moisture Part 6: Determination of water-soluble contaminants by conductivity measurement Part 7: Determination of water-soluble chloridesEN ISO 11127-7:2011 (E) DIN EN ISO 11127-7:2012-04 6