DIN EN ISO 13803-2015 Paints and varnishes - Determination of haze on paint films at 20 (ISO 13803 2014) German version EN ISO 13803 2014《色漆和清漆 20漆膜光泽度的测定》.pdf

1、February 2015 Translation by DIN-Sprachendienst.English price group 11No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).I

2、CS 87.040!%B+“2293108www.din.deDDIN EN ISO 13803Paints and varnishes Determination of haze on paint films at 20 (ISO 13803:2014);English version EN ISO 13803:2014,English translation of DIN EN ISO 13803:2015-02Beschichtungsstoffe Bestimmung des Schleiers von Beschichtungen bei 20 (ISO 13803:2014);En

3、glische Fassung EN ISO 13803:2014,Englische bersetzung von DIN EN ISO 13803:2015-02Peintures et vernis Dtermination du voile sur des feuils de peinture 20 (ISO 13803:2014);Version anglaise EN ISO 13803:2014,Traduction anglaise de DIN EN ISO 13803:2015-02SupersedesDIN EN ISO 13803:2004-09www.beuth.de

4、Document comprises 19 pagesIn case of doubt, the German-language original shall be considered authoritative.01.15 DIN EN ISO 13803:2015-02 2 A comma is used as the decimal marker. National foreword This document (EN ISO 13803:2014) has been prepared by Technical Committee ISO/TC 35 “Paints and varni

5、shes”, Subcommittee SC 9 “General test methods for paints and varnishes” (Secretariat: BSI, United Kingdom) in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat: DIN, Germany). The responsible German body involved in its preparation was the DIN-Normenausschuss Bes

6、chichtungsstoffe und Beschichtungen (DIN Standards Committee Coatings and Coating Materials), Working Committee NA 002-00-07 AA Allgemeine Prfverfahren fr Beschichtungsstoffe und Beschichtungen. The DIN Standards corresponding to the International Standards referred to in this document are as follow

7、s: ISO 1513 DIN EN ISO 1513 ISO 2808 DIN EN ISO 2808 ISO 2813 DIN EN ISO 2813 ISO 4618:2014 DIN EN ISO 4618:2015-01 ISO 11664-3 DIN EN ISO 11664-3 ISO/IEC GUIDE 99 1 Amendments This standard differs from DIN EN ISO 13803:2004-09 as follows: a) the symbols have been brought in line with the revised v

8、ersion of ISO 2813; b) an Introduction and Clause 4 “Principle” have been added; c) the supplementary test conditions have been included in the test report; d) normative references have been updated. Previous editions DIN EN ISO 13803: 2004-09 DIN EN ISO 13803:2015-02 3 National Annex NA (informativ

9、e) Bibliography DIN EN ISO 1513, Paints and varnishes Examination and preparation of test samples DIN EN ISO 2808, Paints and varnishes Determination of film thickness DIN EN ISO 2813, Paints and varnishes Determination of gloss reading at 20, 60 and 85 DIN EN ISO 4618:2015-01, Paints and varnishes

10、Terms and definitions DIN EN ISO 11664-3, Colorimetry Part 3: CIE tristimulus values 1 International vocabulary of metrology Basic and general concepts and associated terms (VIM), Bilingual German-English version ISO/IEC-Guide 99:2007, Beuth Wissen, 3. Auflage 2012, Beuth Verlag GmbH, Berlin DIN EN

11、ISO 13803:2015-02 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13803 October 2014 ICS 87.040 Supersedes EN ISO 13803:2004English Version Paints and varnishes - Determination of haze on paint films at 20 (ISO 13803:2014) Peintures et vernis - Dterminatio

12、n du voile sur des feuils de peinture 20 (ISO 13803:2014) Beschichtungsstoffe - Bestimmung des Schleiers von Beschichtungen bei 20 (ISO 13803:2014) This European Standard was approved by CEN on 24 August 2014. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate

13、the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standa

14、rd exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the natio

15、nal standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slov

16、akia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014 CEN All rights of exploitation in any form and by any mean

17、s reserved worldwide for CEN national Members. Ref. No. EN ISO 13803:2014 EContents PageForeword 3Introduction 41 Scope . 52 Normative references 53 Terms and definitions . 54 Principle 55 Apparatus and materials65.1 Hazemeter .65.2 Measurement standards (certified reference material, working measur

18、ement standards). 106 Test panels . 116.1 Substrate . 116.2 Preparation and coating . 116.3 Drying and conditioning 116.4 Thickness of coating 117 Calibration and adjustment of the hazemeter 117.1 Preparation of the apparatus . 117.2 Zero point check . 117.3 Calibration and adjustment 118 Procedure

19、128.1 General 128.2 Haze measurement of coatings from liquid paints and powder coating materials on glass plates. 128.3 Haze measurement on other coated dry substrates 129 Precision 129.1 General 129.2 Repeatability limit r . 129.3 Reproducibility limit R . 1310 Test report 13Annex A (normative) Cal

20、culation of linear haze .14Bibliography .15DIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 2 Foreword This document (EN ISO 13803:2014) has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes” in collaboration with Technical Committee CEN/TC 139 “Peintures et vernis” the secretariat

21、of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2015, and conflicting national standards shall be withdrawn at the latest by April 2015. Attention is drawn to the po

22、ssibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 13803:2004. According to the CEN-CENELEC Internal Regulations, the national standa

23、rds organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Lux

24、embourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 13803:2014 has been approved by CEN as EN ISO 13803:2014 without any modification. DIN EN ISO 13803:2015-02 EN ISO 13803:2

25、014 (E) 3 IntroductionHigh quality surfaces are expected to have a clear and brilliant appearance. Microstructures can cause a milky appearance. This effect is described as haze. A high gloss surface with microscopic texture has diffused light with low intensity adjacent to the main direction of ref

26、lection. The majority of the incident light is reflected in the specular direction which will make the surface appear high glossy with image forming qualities, but with a milky haziness on top of it.The phenomenon haze can be seen on high gloss surfaces only. Therefore, the 20 geometry is used like

27、with a gloss meter. The aperture range of a 20 gloss meter is 1,8. Two additional sensors next to the gloss detector measure the intensity of the diffused light responsible for haze. Thus, the specularly reflected and the scattered light are measured simultaneously. In order to better correlate with

28、 the visual perception, haze is displayed in a logarithmic scale the lower the haze reading the better the surface.DIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 4 1 ScopeThis International Standard specifies a test method for determining the haze of coatings. The method is suitable for the haze mea

29、surement of non-textures coatings on plane, opaque substrates.The use of the 20 geometry means that the method is closely related to the measurement of gloss at 20 in ISO 2813. The application of this method is intended to give improved differentiation between high-gloss surfaces, for example in the

30、 field of assessment of dispersion characteristics.2 Normative referencesThe following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest editi

31、on of the referenced document (including any amendments) applies.ISO 1514, Paints and varnishes Standard panels for testingISO 2808, Paints and varnishes Determination of film thicknessISO 2813, Paints and varnishes Determination of gloss value at 20, 60and 853 Terms and definitionsFor the purposes

32、of this document, the following terms and definitions apply.3.1hazemilky opalescence in high-gloss or clear coatingsSOURCE: ISO 4618:2014, 2.1373.2geometryidentification of a method of haze measurement using a specified angle with assigned aperturesSOURCE: ISO 2813:2014, 3.2, modified the term “glos

33、s” has been replaced with “haze”.3.3haze valueratio of the luminous flux reflected and diffusely scattered from an object adjacent to the specular direction for a specified source and receptor angle to the luminous flux reflected from glass with a refractive index of 1,567 in the specular direction,

34、 this glass being assigned the value of 100 on the linear haze scaleNote 1 to entry: The measurement of haze value is related to the measurement of gloss in accordance with ISO 2813.4 PrincipleWith a reflectometric apparatus haze values are determined on coated surfaces, correlating with the visual

35、haze perception.DIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 5 The method of haze measurement is specified by the following parameters: measuring angles; field stop apertures; spectral adaptation; reference refractive index.5 Apparatus and materials5.1 Hazemeter5.1.1 GeneralThe hazemeter shall con

36、sist of a light source and a lens that directs a parallel beam of light onto the surface under test, plus a receptor housing containing a lens, a field stop and a photoelectric cell to receive the required cone of reflected light. The source of the hazemeter is shown in Figure 1.Key1 light source2 s

37、ensor3 gloss4 haze5 test surfaceFigure 1 Measuring angle of 205.1.2 GeometriesThe axis of the incident beam shall be at an angle 1= (20,0 0,1) (see Figure 1) to the normal to the surface under test. With a flat piece of polished black glass or a front reflecting mirror instead of the test panel posi

38、tion, the source field stop shall be reproduced at the centre of the receptor field stop (see Figure 3).The optical axis of the receptor shall be coincident with the mirror image of the axis of the incident beam to within 0,1, i.e. the condition 1- 2 0,1 shall be fulfilled (see Figure 2).The dimensi

39、ons of the source aperture and the receptor aperture and the permissible tolerances shall be as indicated in Table 1.In order to average out the entire surface, the width of the illuminated area on the test panel shall be significantly larger than possible surface irregularities: a generally accepte

40、d value is 10 mm.DIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 6 The angular dimensions of the receptor field stop shall be measured from the receptor lens.There shall be no vignetting of rays that lie with the specified angular fields.The photoelectric cell shall give a reading proportional to the

41、 light flux passing the receptor field stop, to a deviation within 1 % of the full-scale readingDIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 7 Key1 light source2 source image aperture3 source lens4 receptor lens5 test surface6 receptor area7 image of the source aperture in the receptor field stop1

42、angle of the beam against surface normal2reflection angle of the beam refracted from medium 2 (against surface normal)1receptor aperture2central opaque zone of the receptor aperture3source image aperture angleFigure 2 Course of beam of the hazemeterDIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 8 Ke

43、y1 plane of measurement2 plane perpendicular to plane of measurement3 receptor area4 receptor field stop5 image of the source aperture in the receptor field stopFigure 3 Receptor field stop5.1.3 Filtering at the receptorFiltering at the receptor shall be done in such a way that the transmittance of

44、the filter () is given by Formula 1:()=()()()()kVSLLCrelS(1)whereV() is the CIE photopic luminous efficiency;SC() is the spectral power distribution of CIE illuminant C;L()relis the relative spectral sensitivity of the receptor;LS() is the spectral power distribution of the light source;k is the cal

45、ibration constant.DIN EN ISO 13803:2015-02 EN ISO 13803:2014 (E) 9 Table 1 Angles of source image aperture and receptor apertureAnglein parallel to plane of reflectionperpendicular to plane of reflectionSource image aperture 30,75 0,10 2,50 0,1Receptor aperture 15,50 0,25 5,50 0,25Central opaque par

46、t of receptor aperture 22,00 0,1 5,50 0,25NOTE 1 In Figure 3 the plane of reflection corresponds to the plane of illustration.NOTE 2 In Figure 3 only the aperture angles in parallel to the plane of reflection are illustrated.5.2 Measurement standards (certified reference material, working measurement standards)1)5.2.1 High gloss standard A (working measurement standard)Plane black glass plate