DIN EN ISO 1518-1-2011 Paints and varnishes - Determination of scratch resistance - Part 1 Constant-loading method (ISO 1518-1 2011) German version EN ISO 1518-1 2011《色漆和清漆 耐擦伤性的测定.pdf

1、September 2011 Translation by DIN-Sprachendienst.English price group 9No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).I

2、CS 87.040!$tG“1813661www.din.deDDIN EN ISO 1518-1Paints and varnishes Determination of scratch resistance Part 1: Constant-loading method (ISO 1518-1:2011)English translation of DIN EN ISO 1518-1:2011-09Beschichtungsstoffe Bestimmung der Kratzbestndigkeit Teil 1: Verfahren mit konstanter Last (ISO 1

3、518-1:2011)Englische bersetzung von DIN EN ISO 1518-1:2011-09Peintures et vernis Dtermination de la rsistence la rayure Partie 1: Mthode charge constante (ISO 1518-1:2011)Traduction anglaise de DIN EN ISO 1518-1:2011-09SupersedesDIN EN ISO 1518:2000-09www.beuth.deDocument comprises pagesIn case of d

4、oubt, the German-language original shall be considered authoritative.1408.11 DIN EN ISO 1518-1:2011-09 2 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes”, Subcommittee SC 9 “General test methods for paint

5、s and varnishes” (Secretariat: BSI, United Kingdom) in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat: DIN, Germany). The responsible German body involved in its preparation was the Normenausschuss Beschichtungsstoffe und Beschichtungen (Coatings and Coating Ma

6、terials Standards Committee), Working Committee NA 002-00-07 AA Allgemeine Prfverfahren fr Beschichtungsstoffe und Beschichtungen. EN ISO 1518 consists of the following parts, under the general title Paints and varnishes Determination of scratch resistance: Part 1: Constant-loading method Part 2: Va

7、riable-loading method The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 1513 DIN EN ISO 1513 ISO 1514 DIN EN ISO 1514 ISO 2808 DIN EN ISO 2808 ISO 3270 DIN EN 23270 ISO 5725-1 DIN ISO 5725-1 ISO 15528 DIN EN ISO 15528 Amendments This stan

8、dard differs from DIN EN ISO 1518:2000-09 as follows: a) the number of the standard has been changed from DIN EN ISO 1518 to DIN EN ISO 1518-1; b) Clause 3 “Principle” has been added; c) two versions of the test apparatus are now described; d) the minimum length of the scratch has been reduced from

9、60 mm to 40 mm; e) the magnification of the lens used to examine the scratch has been specified as at least 4; f) the supplementary test conditions (formerly Annex A) have been integrated in the test report; g) Clause 8 “Precision” has been added; h) Annex B specifying a procedure for re-tipping scr

10、atch-test needles has been deleted. Previous editions DIN EN ISO 1518: 2000-09 DIN EN ISO 1518-1:2011-09 3 National Annex NA (informative) Bibliography DIN EN 23270, Paints, varnishes and their raw materials Temperatures and humidities for conditioning and testing DIN EN ISO 1513, Paints and varnish

11、es Examination and preparation of test samples DIN EN ISO 1514, Paints and varnishes Standard panels for testing DIN EN ISO 2808, Paints and varnishes Determination of film thickness DIN EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes Sampling DIN ISO 5725-1, Accuracy (tru

12、eness and precision) of measurement methods and results Part 1: General principles and definitions DIN EN ISO 1518-1:2011-09 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1518-1 June 2011 ICS 87.040 Supersedes EN ISO 1518:2000English Version Paints and v

13、arnishes Determination of scratch resistance Part 1: Constant-loading method (ISO 1518-1:2011) Peintures et vernis Dtermination de la rsistance la rayure Partie 1: Mthode charge constante (ISO 1518-1:2011) Beschichtungsstoffe Bestimmung der Kratzbestndigkeit Teil 1: Verfahren mit konstanter Last (IS

14、O 1518-1:2011) This European Standard was approved by CEN on 8 January 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibli

15、ographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the respons

16、ibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Gree

17、ce, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Manageme

18、nt Centre: Avenue Marnix 17, B-1000 Brussels 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1518-1:2011: EContents Page Foreword3 1 Scope 4 2 Normative references 4 3 Principle4 4 Apparatus .5 5 Sampling.5 6 Test panels .

19、7 7 Procedure .7 8 Precision.8 9 Test report 9 Bibliography 10 DIN EN ISO 1518-1:2011-09 EN ISO 1518-1:2011 (E) 2 Foreword This document (EN ISO 1518-1:2011) has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes” in collaboration with Technical Committee CEN/TC 139 “Paints and var

20、nishes”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by December 2011, and conflicting national standards shall be withdrawn at the latest by December 201

21、1. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN ISO 1518:2000. According to the CEN/CENELEC Internal Re

22、gulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg,

23、Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 1518-1:2011 has been approved by CEN as a EN ISO 1518-1:2011 without any modification. DIN EN ISO 1518-1:2011-09 EN ISO 1518-1:2011 (E) 3 1

24、 Scope This part of ISO 1518 specifies a test method for determining under defined conditions the resistance of a single coating or a multi-coat system of paint, varnish or related product to penetration by scratching with a scratch stylus loaded with a specified load. Penetration of the stylus is t

25、o the substrate, except in the case of a multi-coat system, in which case the stylus can penetrate either to the substrate or to an intermediate coat. The method specified can be carried out a) either as a “pass/fail” test, by testing with a single specified load applied to the stylus to assess comp

26、liance with a particular specification; b) or by applying increasing loads to the stylus to determine the minimum load at which the coating is penetrated. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the

27、edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 1513, Paints and varnishes Examination and preparation of test samples ISO 1514, Paints and varnishes Standard panels for testing ISO 2808, Paints and varnishes Determ

28、ination of film thickness ISO 15528, Paints, varnishes and raw materials for paints and varnishes Sampling 3 Principle A scratch stylus loaded with a specified load is drawn over a coating at a constant speed. The following test parameters are specified: the geometry of the stylus tip; the range wit

29、hin which the test load may lie and the increments by which it may be increased; the procedure by which the stylus is lowered on to the coating; the speed at which the stylus travels and the minimum length of the scratch. DIN EN ISO 1518-1:2011-09 EN ISO 1518-1:2011 (E) 4 The scratch is examined to

30、see if the coating has been penetrated to the extent specified for a single specified test load (“pass/fail” test) or to determine the minimum test load required for penetration. 4 Apparatus 4.1 Scratch apparatus, two versions of which are illustrated in Figure 1 and Figure 2, with the following cha

31、racteristics: The test load acting on the scratch stylus fixed to the load beam can be produced either by a weight attached to the stylus (see Figure 1) or by a weight which slides along a graduated load beam (see Figure 2). The test load shall be 1 N to 20 N, shall be adjustable in increments of 0,

32、5 N and shall be accurate to within 0,2 N. The test panel held in a panel holder is moved relative to the stylus by means of a linear actuator driven by a motor. The speed at which the stylus travels shall be (35 5) mm/s and the length of the scratch shall be at least 40 mm. The length of the scratc

33、h can affect the result. A lowering device with a flat ramp brings the stylus smoothly into contact with the coating at the beginning of the movement of the panel holder. The angle of the ramp shall be (12,5 2,5). Some types of apparatus are designed so that the load beam moves and the test panel is

34、 fixed. Such types of apparatus may also be used. 4.2 Scratch stylus A, having a hemispherical hard-metal tip of radius (0,50 0,01) mm. 4.3 Scratch stylus B, having a hemispherical hard-metal tip of radius (0,25 0,01) mm. 4.4 Scratch stylus C, having a hemispherical synthetic-ruby tip of radius (0,5

35、0 0,01) mm. 4.5 Scratch stylus D, having a hemispherical synthetic-ruby tip of radius (0,25 0,01) mm. 4.6 Indicating device, based on electrical contact between the stylus and the metallic substrate, to show when the coating has been penetrated. NOTE 1 This device is not suitable for paints containi

36、ng electrically conducting pigments, for non-metallic substrates or if penetration to an intermediate non-conducting coat is required. NOTE 2 The indicating device can only be used when certain parts of the scratch apparatus are electrically insulated. 4.7 Magnifying lens, with at least 4 magnificat

37、ion. 5 Sampling Take a representative sample of the product to be tested (or of each product in the case of a multi-coat system), as described in ISO 15528. Examine and prepare each sample for testing, as described in ISO 1513. DIN EN ISO 1518-1:2011-09 EN ISO 1518-1:2011 (E) 5 Key 1 weight 2 scratc

38、h stylus 3 load beam 4 pivot bearing for load beam 5 tare weight 6 lowering device (ramp and guide pin) 7 test panel 8 test panel holder (designed to be driven by a motor to move in the direction of the arrow) 9 baseplate Figure 1 Scratch apparatus Version with the weight attached to the stylus Key

39、1 stylus 2 load beam with scale 3 sliding weight 4 pivot bearing for load beam 5 tare weight 6 lowering device (ramp and guide pin) 7 test panel 8 test panel holder (designed to be driven by a motor to move in the direction of the arrow) 9 baseplate Figure 2 Scratch apparatus Version with a sliding

40、weight DIN EN ISO 1518-1:2011-09 EN ISO 1518-1:2011 (E) 6 6 Test panels 6.1 Substrate The test panels shall be made of steel with a thickness of 0,7 mm to 1,0 mm and shall conform to the requirements of ISO 1514. The panels should preferably have a size of 200 mm 100 mm. 6.2 Preparation and coating

41、Prepare each test panel in accordance with ISO 1514 and coat it according to the specified method with the product or system under test. The method of application of the coating shall be as specified by the manufacturer or agreed between the interested parties and shall be included in the test repor

42、t see Clause 9, item c) 2). 6.3 Drying and conditioning Dry (or stove) and age, if applicable, each coated test panel for the specified time and under the specified conditions. Before testing, condition the coated panels at a temperature of (23 2) C and a relative humidity of (50 5) % (i.e. in accor

43、dance with ISO 3270) for a minimum period of 16 h. Carry out the test procedure immediately after the removal of the test panels from the conditioning chamber. The drying (or stoving) and ageing time and conditions shall be as specified by the manufacturer or agreed between interested parties and sh

44、all be included in the test report see Clause 9, item c) 3). 6.4 Thickness of coating Determine the thickness, in micrometres, of the dried coating by one of the procedures specified in ISO 2808. The dry-film thickness shall be as specified by the manufacturer or agreed between the interested partie

45、s and shall be included in the test report see Clause 9, item c) 4). 7 Procedure 7.1 Test conditions Carry out the test at (23 2) C and a relative humidity of (50 5) %. 7.2 General test procedure 7.2.1 Clamp a coated test panel on the panel holder with the coating facing upwards. Position the test p

46、anel so that the distance between the scratches to be made will be at least 5 mm and the distance from the scratches to the edge of the test panel will be at least 10 mm. 7.2.2 Fix the scratch stylus in the load beam so that, when in position on the test panel, the stylus will be perpendicular to th

47、e panel. 7.2.3 With the stylus unloaded, balance the load beam by means of the tare weight. 7.2.4 Adjust the test load to the required value by placing a weight on the stylus or by moving the sliding weight, depending on the type of apparatus used. 7.2.5 Activate the indicating device, if used, and

48、check that it is functioning correctly. DIN EN ISO 1518-1:2011-09 EN ISO 1518-1:2011 (E) 7 7.2.6 Start the motor of the apparatus and allow the scratch to be made in the coating. Observe the indicating device during the test, if appropriate, to determine whether electrical contact occurs between the

49、 stylus and the substrate. 7.2.7 Remove the panel and immediately examine the scratch, with the aid of the magnifying lens, for penetration to the extent specified. 7.3 Procedure for a single specified load (“pass/fail” test) Carry out the procedure specified in 7.2 three times on each of two test panels. If the coating has not been penetrated beyond the specified extent in any of the six test runs, report the result as “pass”. If the coating has been penetr