DIN EN ISO 1927-8-2013 Monolithic (unshaped) refractory products - Part 8 Determination of complementary properties (ISO 1927-8 2012) German version EN ISO 1927-8 2012《整体(粗制)耐火材料产品.pdf

1、April 2013 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 8

2、1.080!$“1999329www.din.deDDIN EN ISO 1927-8Monolithic (unshaped) refractory products Part 8: Determination of complementary properties (ISO 1927-8:2012);English version EN ISO 1927-8:2012,English translation of DIN EN ISO 1927-8:2013-04Ungeformte (monolithische) feuerfeste Erzeugnisse Teil 8: Bestim

3、mung zustzlicher Eigenschaften (ISO 1927-8:2012);Englische Fassung EN ISO 1927-8:2012,Englische bersetzung von DIN EN ISO 1927-8:2013-04Produits rfractaires monolithiques (non faonns) Partie 8: Dtermination des caractristiques complmentaires (ISO 1927-8:2012);Version anglaise EN ISO 1927-8:2012,Trad

4、uction anglaise de DIN EN ISO 1927-8:2013-04SupersedesDIN EN 1402-8:2004-01www.beuth.deDocument comprises 12 pagesIn case of doubt, the German-language original shall be considered authoritative.03.13 DIN EN ISO 1927-8:2013-04 2 A comma is used as the decimal marker. National foreword ISO 1927-8 has

5、 been prepared by Technical Committee ISO/TC 33 “Refractories” and has been taken over as EN ISO 1927-8 by Technical Committee CEN/TC 187 “Refractory products and materials” (Secretariat: BSI, United Kingdom). The responsible German body involved in its preparation was the Normenausschuss Materialpr

6、fung (Materials Testing Standards Committee), Working Committee NA 062-02-57 AA Ungeformte, dichte geformte und wrmedmmende feuerfeste Erzeugnisse und Werkstoffe. EN ISO 1927 consists of the following parts, under the general title Monolithic (unshaped) refractory products: Part 1: Introduction and

7、classification Part 2: Sampling for testing Part 3: Characterization as received Part 4: Determination of consistency of castables Part 5: Preparation and treatment of test pieces Part 6: Measurement of physical properties Part 7: Tests on pre-formed shapes Part 8: Determination of complementary pro

8、perties The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 1927-1 DIN EN ISO 1927-1 ISO 1927-2 DIN EN ISO 1927-2 ISO 1927-3 DIN EN ISO 1927-3 ISO 1927-5 DIN EN ISO 1927-5 ISO 1927-6 DIN EN ISO 1927-6 ISO 8894-1 DIN EN ISO 8894-1 ISO 8894-2

9、 DIN EN 993-15 ISO 12676 DIN EN ISO 12676 ISO 16282 DIN EN ISO 16282 Amendments This standard differs from DIN EN 1402-8:2004-01 as follows: a) the content of EN ISO 1927-8 (based on EN 1402-8) has been adopted in full; b) references to EN Standards have been replaced by references to the relevant I

10、SO Standards and have been updated, e.g. in Clause 3. Previous editions DIN V ENV 1402-8: 1999-04 DIN EN 1402-8: 2004-01 DIN EN ISO 1927-8:2013-04 3 National Annex NA (informative) Bibliography DIN EN 993-15, Methods of test for dense shaped refractory products Part 15: Determination of thermal cond

11、uctivity by the hot-wire (parallel) method DIN EN 1402-1, Unshaped refractory products Part 1: Introduction and classification DIN EN ISO 1927-2, Monolithic (unshaped) refractory products Part 2: Sampling for testing DIN EN ISO 1927-3, Monolithic (unshaped) refractory products Part 3: Characterizati

12、on as received DIN EN ISO 1927-5, Monolithic (unshaped) refractory products Part 5: Preparation and treatment of test pieces DIN EN ISO 1927-6, Monolithic (unshaped) refractory products Part 6: Measurement of physical properties DIN EN ISO 8894-1, Refractory materials Determination of thermal conduc

13、tivity Part 1: Hot-wire methods (cross-array and resistance thermometer) DIN EN ISO 12676, Refractory products Determination of resistance to carbon monoxide DIN EN ISO 16282, Methods of test for dense shaped refractory products Determination of resistance to abrasion at ambient temperature DIN EN I

14、SO 1927-8:2013-04 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1927-8 December 2012 ICS 81.080 Supersedes EN 1402-8:2003 English Version Monolithic (unshaped) refractory products Part 8: Determination of complementary properties (ISO 1927-8:2012) Produi

15、ts rfractaires monolithiques (non faonns) Partie 8: Dtermination des caractristiques complmentaires (ISO 1927-8:2012) Ungeformte (monolithische) feuerfeste Erzeugnisse Teil 8: Bestimmung zustzlicher Eigenschaften (ISO 1927-8:2012) This European Standard was approved by CEN on 30 November 2012. CEN m

16、embers are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on applic

17、ation to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Mana

18、gement Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvi

19、a, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000

20、 Brussels 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1927-8:2012: E Contents PageForeword .1 Scope .2 Normative references 3 Principle 4 Determination of permeability to gases 4.1 Principle 4.2 Test pieces .4.3 Proced

21、ure 5 Determination of the resistance to thermal shock .5.1 Principle 5.2 Test pieces .5.3 Procedure 6 Determination of thermal conductivity 6.1 Principle 6.2 Test pieces .6.3 Procedure 7 Determination of sulfuric acid resistance 7.1 Principle 7.2 Test pieces .7.3 Procedure 8 Tests for products cont

22、aining carbon .8.1 Principle 8.2 Test pieces .8.3 Procedure 9 Determination of the resistance to carbon monoxide .10 Determination of resistance to abrasion at ambient temperature 11 Test report .2344455555555666666666677777DIN EN ISO 1927-8:2013-04 EN ISO 1927-8:2012 (E) Foreword This document (EN

23、ISO 1927-8:2012) has been prepared by Technical Committee ISO/TC 33 Refractoriesin collaboration with Technical Committee CEN/TC 187 “Refractory products and materials” the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publica

24、tion of an identical text or by endorsement, at the latest by June 2013, and conflicting national standards shall be withdrawn at the latest by June 2013. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall no

25、t be held responsible for identifying any or all such patent rights. This document supersedes EN 1402-8:2003. According to the CEN/CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,

26、Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey a

27、nd the United Kingdom. Endorsement notice The text of ISO 1927-8:2012 has been approved by CEN as a EN ISO 1927-8:2012 without any modification. ”“3DIN EN ISO 1927-8:2013-04 EN ISO 1927-8:2012 (E) 1 ScopeThis part of ISO 1927 specifies methods for the determination of the properties of unshaped refr

28、actory materials from test pieces prepared and stored in accordance with ISO 1927-5. The methods complement those described in ISO 1927-6.The methods have been adapted from standards for shaped refractory products to make them applicable to dense and insulating castables, and ramming materials as de

29、fined in ISO 1927-1, before and after firing.2 Normative referencesThe following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any ame

30、ndments) applies.ISO 8841, Dense, shaped refractory products Determination of permeability to gasesISO 1927-1, Monolithic (unshaped) refractory products Part 1: Introduction and classificationISO 1927-2, Monolithic (unshaped) refractory products Part 2: Sampling for testingISO 1927-3, Monolithic (un

31、shaped) refractory products Part 3: Characterization as receivedISO 1927-5, Monolithic (unshaped) refractory products Part 5: Preparation and treatment of test piecesISO 1927-6, Monolithic (unshaped) refractory products Part 6: Measurement of physical propertiesISO 8894-1, Refractory materials Deter

32、mination of thermal conductivity Part 1: Hot-wire methods (cross-array and resistance thermometer)ISO 8894-2, Refractory materials Determination of thermal conductivity Part 2: Hot-wire method (parallel)ISO 8890, Dense shaped refractory products Determination of resistance to sulfuric acidISO 10060,

33、Dense, shaped refractory products Test methods for products containing carbonISO 12676, Refractory products Determination of resistance to carbon monoxideISO 16282, Methods of test for dense shaped refractory products Determination of resistance to abrasion at ambient temperatureEN 993-11:2007, Meth

34、ods of test for dense shaped refractory products Part 11: Determination of resistance to thermal shock3 PrincipleThe complementary properties of unshaped refractory products are determined by the procedures given in ISO 8890, ISO 8841, ISO 8894-1, ISO 8894-2, ISO 10060, ISO 16282, ISO 1927-1, ISO 19

35、27-2, ISO 1927-3, ISO 1927-5, ISO 1927-6, ISO 12676 and EN 993-11.4DIN EN ISO 1927-8:2013-04 EN ISO 1927-8:2012 (E) The methods complement those described in ISO 1927-6. It is not necessary to use all the methods to characterize a material.4 Determination of permeability to gases4.1 PrincipleThis de

36、termination shall be carried out on test pieces after drying or after firing at a temperature and time to be agreed between the parties involved.4.2 Test piecesUse cylindrical test pieces with dimensions as defined in ISO 8841 and obtained from shapes A, B or C by sawing or coring, and prepared, sto

37、red, dried and/or fired according to the relevant sections of ISO 1927-5. The direction from which the test pieces are cut with regard to the direction of shaping shall be stated in the test report; the plane faces of the cylinder shall be at least at 4 mm away from the initial faces of the shape.If

38、 the test pieces cannot be obtained by sawing or coring, due to the nature of the material, they may be prepared directly and this shall be noted in the test report.In all cases, the test pieces shall be dried at 110 C 5 C for a minimum of 24 h and fired at a temperature and time to be defined betwe

39、en the parties and noted in the test report.4.3 ProcedureDetermine the permeability to gases in accordance with ISO 8841.5 Determination of the resistance to thermal shock5.1 PrincipleThis determination shall be carried out on test pieces fired at a temperature equal to or higher than the temperatur

40、e of the test.The standard quenching temperature shall be 950 C and prefiring of the test pieces shall be carried out at 950 C or above for 5 h.Other quenching and prefiring temperatures and times may be agreed upon by the parties concerned and shall be noted in the test report.5.2 Test piecesTest p

41、ieces with dimensions of shape B, i.e. 230 mm 64 mm 54 mm shall be used. They shall be prepared and prefired according to ISO 1927-5 at a temperature and time agreed between the involved parties (see 5.1).NOTE The use of other shapes may be agreed by the parties, but the results are not comparable w

42、ith those using the test pieces stated above.5.3 ProcedureDetermine the resistance to thermal shock of the prefired test pieces in accordance with method B of EN 993-11:2007.5DIN EN ISO 1927-8:2013-04 EN ISO 1927-8:2012 (E) 6 Determination of thermal conductivity6.1 PrincipleThis determination may b

43、e carried out on fired or unfired, dried test pieces in accordance with ISO 8894-1 (hot wire, cross array) or with ISO 8894-2 (hot wire, parallel).For both fired and unfired, dried test pieces, variation in thermal conductivity can occur due to time-dependent mineralogical and microstructural change

44、s if the test piece has not been prefired to a temperature equal to or higher than the measurement temperature.It is therefore necessary to take special care to ensure that equilibrium is attained when testing such test pieces. This can entail holding the test furnace at the measurement temperature

45、for prolonged periods.6.2 Test piecesTest pieces shall be used corresponding to shape A as defined in ISO 1927-5.For fired test pieces, the firing shall be carried out in accordance with ISO 1927-5 or as agreed between the parties.6.3 ProcedureDetermine the thermal conductivity at each defined measu

46、rement temperature in accordance with ISO 8894-1 (hot wire, cross array) or ISO 8894-2 (hot wire, parallel). For unfired test pieces, the rate of rise of the test furnace shall be in accordance with that specified in ISO 1927-5 for the type of material under test.In all cases where the test piece ha

47、s been prefired, (either before or during the test) to a lower temperature than the measurement temperature, it may be necessary to maintain the furnace at this temperature for extended periods to attain equilibrium. In some cases, it is advisable to maintain the temperature overnight.7 Determinatio

48、n of sulfuric acid resistance7.1 PrincipleDetermination of sulfuric acid resistance consists of the chemical attack by sulfuric acid on test pieces crushed to a specific grain size.7.2 Test piecesUse shape A test pieces prepared in accordance with ISO 1927-5, stored and dried at 110 C 5 C for a minimum of 24 h. Samples shall be taken out from test pieces in accordance with ISO 8890.Any pre-treatment of the test pieces shall be agreed between the