DIN EN ISO 2417-2016 Leather - Physical and mechanical tests - Determination of the static absorption of water (ISO 2417 2016) German version EN ISO 2417 2016《皮革 物理和机械试验 静态吸水性的测定(I.pdf

1、English price group 7No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 59.140.30!%X9y“2532286www.din.deDIN EN ISO 241

2、7Leather Physical and mechanical tests Determination of the static absorption of water (ISO 2417:2016);English version EN ISO 2417:2016,English translation of DIN EN ISO 2417:2016-07Leder Physikalische und mechanische Prfungen Bestimmung der statischen Wasseraufnahme (ISO 2417:2016);Englische Fassun

3、g EN ISO 2417:2016,Englische bersetzung von DIN EN ISO 2417:2016-07Cuir Essais physiques et mcaniques Dtermination de labsorption statique deau (ISO 2417:2016);Version anglaise EN ISO 2417:2016,Traduction anglaise de DIN EN ISO 2417:2016-07SupersedesDIN EN ISO 2417:2003-10www.beuth.deDocument compri

4、ses 9 pagesDTranslation by DIN-Sprachendienst.In case of doubt, the German-language original shall be considered authoritative.July 201607.16DIN EN ISO 2417:2016-07 2 A comma is used as the decimal marker. National foreword This document (EN ISO 2417:2016) has been prepared by Technical Committee IU

5、LTCS “International Union of Leather Technologists and Chemists Societies” in collaboration with Technical Committee CEN/TC 289 “Leather” (Secretariat: UNI, Italy). The responsible German body involved in its preparation was DIN-Normenausschuss Materialprfung (DIN Standards Committee Materials Testi

6、ng), Working Committee NA 062-05-51 AA Anforderungen und physikalische Prfverfahren fr Leder und seine Ausgangsprodukte. The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 2418 DIN EN ISO 2418 ISO 2419 DIN EN ISO 2419 ISO 2420 DIN EN ISO 2

7、420 ISO 3696 DIN ISO 3696 Amendments This standard differs from DIN EN ISO 2417:2003-10 as follows: a) in Clause 8 “Test report”, item c) has been revised so that the reference to ISO 2419 is undated; b) the standard has been editorially revised. Previous editions DIN 53330: 1944-02, 1970-12, 1978-0

8、5 DIN EN ISO 2417: 2003-10 National Annex NA (informative) Bibliography DIN EN ISO 2418, Leather Chemical, physical and mechanical and fastness tests Sampling location DIN EN ISO 2419, Leather Physical and mechanical tests Sample preparation and conditioning DIN EN ISO 2420, Leather Physical and mec

9、hanical tests Determination of apparent density DIN ISO 3696, Water for analytical laboratory use Specification and test methods EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 2417 March 2016 ICS 59.140.30 Supersedes EN ISO 2417:2002 English Version Leather Physical and mechanical tests De

10、termination of the static absorption of water (ISO 2417:2016) Cuir Essais physiques et mcaniques Dtermination de labsorption statique deau (ISO 2417:2016) Leder Physikalische und mechanische Prfungen Bestimmung der statischen Wasseraufnahme (ISO 2417:2016) This European Standard was approved by CEN

11、on 23 January 2016. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards

12、may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notifie

13、d to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Icela

14、nd, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Manage

15、ment Centre: Avenue Marnix 17, B-1000 Brussels 2016 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 2417:2016 E EN ISO 2417:2016 (E) 2 Contents Page European foreword . 3 Foreword 4 1 Scope 5 2 Normative references 5 3 Principl

16、e . 5 4 Apparatus . 5 5 Sampling and sample preparation 6 6 Procedure. 6 7 Expression of results 7 8 Test report . 7 DIN EN ISO 2417:2016-07 EN ISO 2417:2016 (E) 3 European Foreword This document (EN ISO 2417:2016) has been prepared by Technical Committee IULTCS “International Union of Leather Techn

17、ologists and Chemists Societies” in collaboration with Technical Committee CEN/TC 289 “Leather” the secretariat of which is held by UNI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2

18、016, and conflicting national standards shall be withdrawn at the latest by September 2016. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent ri

19、ghts. This document supersedes EN ISO 2417:2002. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, F

20、ormer Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 241

21、7:2016 has been approved by CEN as EN ISO 2417:2016 without any modification. DIN EN ISO 2417:2016-07 ForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally

22、 carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the w

23、ork. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the dif

24、ferent approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).Attention is drawn to the possibility that some of the elements of this document m

25、ay be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www.iso.org/pate

26、nts).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adherence to the WTO principl

27、es in the Technical Barriers to Trade (TBT) see the following URL: Foreword - Supplementary informationISO 2417 was prepared by the Physical Test Commission of the International Union of Leather Technologists and Chemists Societies (IUP Commission, IULTCS) in collaboration with the European Committe

28、e for Standardization (CEN) Technical Committee CEN/TC 289, Leather, the secretariat of which is held by UNI, in accordance with the Agreement on technical cooperation between ISO and CEN (Vienna Agreement).It is based on IUP 7 originally published in J. Soc. Leather Trades Chemists 44, p. 367, (196

29、0) and declared an official method of the IULTCS in 1961. This updated version was published in J. Soc. Leather Tech. Chem. 84, p. 323, (2000) and reconfirmed as an official method in March 2001. The same principle is used but the text has been updated and includes the number of test pieces to be ta

30、ken.IULTCS, originally formed in 1897, is a world-wide organization of professional leather societies to further the advancement of leather science and technology. IULTCS has three Commissions, which are responsible for establishing international methods for the sampling and testing of leather. ISO

31、recognizes IULTCS as an international standardizing body for the preparation of test methods for leather.This third edition cancels and replaces the second edition (ISO 2417:2002), of which it constitutes a minor revision to align item c) of Clause 8 with ISO 2419:2012.EN ISO 2417:2016 (E) 4DIN EN I

32、SO 2417:2016-07 1 ScopeThis International Standard specifies a method for determining the water absorption of leather under static conditions. The method is applicable to all leather, particularly heavy leather.2 Normative referencesThe following documents, in whole or in part, are normatively refer

33、enced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 2418, Leather Chemical, physical and mechanical and fastness tests Samp

34、ling locationISO 2419, Leather Physical and mechanical tests Sample preparation and conditioningISO 2420, Leather Physical and mechanical tests Determination of apparent densityISO 3696, Water for analytical laboratory use Specification and test methods3 PrincipleA test piece of known mass or volume

35、 is immersed in water for a known period of time and the volume of water absorbed measured.4 Apparatus4.1 Glass Kubelka apparatus, as shown in Figure 1. The graduated scale shall be readable to 0,1 ml with an accuracy of 0,1 ml. The total volume of the bulb (A) and the graduated tube shall be 75 ml

36、2 ml.4.2 Rubber stopper (C), fitted with a glass rod or a nickel or stainless steel wire of diameter about 1 mm and of sufficient length to keep the test piece at the end of the cylinder (B) distant from the stopper (C).Dimensions in millimetresFigure 1 Kubelka apparatus and stopperEN ISO 2417:2016

37、(E) 5DIN EN ISO 2417:2016-07 4.3 Press knife, the inner wall of which is a right angled circular cylinder of diameter 70 mm 1 mm as specified in ISO 2419.4.4 Balance, reading to 0,001 g.4.5 Distilled or de-ionised water, conforming to the requirements of grade 3 of ISO 3696.5 Sampling and sample pre

38、paration5.1 Sample in accordance with ISO 2418. From the sample, cut three test pieces by applying the press knife (4.3) to the grain surface. Condition the test pieces in accordance with ISO 2419.If there is a requirement for more than two hides or skins to be tested in one batch, then only one sam

39、ple need be taken from each hide or skin, provided that the overall total is not less than three test pieces.5.2 Weigh the test piece to the nearest 0,001 g or determine its volume in accordance with ISO 2420.5.3 Carry out all further operations at a temperature of 20 C 2 C or 23 C 2 C. There is no

40、further need for humidity control.6 Procedure6.1 Ensure that the Kubelka apparatus (4.1) is clean and free of grease. Wet the interior surfaces with distilled or de-ionized water (4.5) and pour out the excess.6.2 Place the apparatus with the bulb (A) directly below the cylinder (B) and fill with suf

41、ficient distilled or de- ionized water (4.5) at 20 C 2 C or 23 C 2 C to give a water level between 0 ml and 1 ml on the graduated scale. Record the scale reading.6.3 Place the test piece in the cylinder (B) and pour the water from the bulb (A) into the cylinder. Close the cylinder with the stopper (

42、C) to prevent evaporation losses and place the apparatus on a level surface.6.4 After the test piece has been immersed for a specific time (see Note 1 to 6.5) turn the apparatus so that the water drains into the bulb. One min after drainage, note the scale reading at the water level and calculate th

43、e volume of water absorbed.6.5 If the water absorption is required at other time intervals, turn the apparatus immediately so that the water flows back into the cylinder (B) and again covers the test piece. Repeat the operation in 6.4.NOTE 1 For most purposes, measurements after two periods of immer

44、sion are sufficient. If possible, the periods are taken from the following, 15 min 0,2 min; 30 min 0,2 min; 60 min 0,5 min; 120 min 0,5 min; 24 h 0,1 h.NOTE 2 The periods of 1 min during which the water is being drained back are not to be considered as part of periods of immersion which precede them

45、, but are considered as parts of subsequent periods of immersion. For example, if the water absorptions during periods of immersion of 15 min and 60 min are to be measured on the same test piece, and the instant of first immersion is at time zero, subsequent actions will be as follows: at 15 min, be

46、gin draining, at 16 min, read off the residual volume and immediately re-immerse the test piece, at 60 min, begin draining, at 61 min, read off the residual volume.EN ISO 2417:2016 (E) 6DIN EN ISO 2417:2016-07 7 Expression of resultsCalculate the water absorption, Q, (%V/m) in millilitres per 100 g,

47、 using Formula (1); or calculate the water absorption, P, (%V/V) in millilitres per 100 ml, using Formula (2).QVm=1100 (1)PVV=12100 (2)whereV1is the volume of water absorbed in millilitres as determined in 6.4;V2is the volume of the test piece in millilitres as determined in 5.2 (see Note);m is the

48、mass of the test piece in grams as determined in 5.2.NOTE ISO 2420 determines the volume in cubic millimetres. Thus it is divided by 1 000 to give the correct value of V2in millilitres.8 Test reportThe test report shall include the following:a) a reference to this International Standard, i.e. ISO 24

49、17;b) the mean water absorption (in millilitres per 100 g, Q, or in millilitres per 100 ml, P) for each period of immersion;c) the standard atmosphere used for conditioning and testing as given in ISO 2419;d) any deviations from the method specified in this International Standard;e) full details for identification of the sample and any deviation from ISO 2418 with respect to sampling.EN ISO 2417:2016 (E) 7DIN EN ISO 2417:2016-07