DIN EN ISO 8510-2-2010 Adhesives - Peel test for a flexible-bonded-to-rigid test specimen assembly - Part 2 180 degree peel (ISO 8510-2 2006) German version EN ISO 8510-2 2010《粘合剂 .pdf

1、December 2010 Translation by DIN-Sprachendienst.English price group 8No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).IC

2、S 83.180!$ldF“1736535www.din.deDDIN EN ISO 8510-2Adhesives Peel test for a flexible-bonded-to-rigid test specimen assembly Part 2: 180 degree peel (ISO 8510-2:2006)English translation of DIN EN ISO 8510-2:2010-12Klebstoffe Schlprfung fr flexibel/starr geklebte Proben Teil 2: 180-Grad-Schlversuch (IS

3、O 8510-2:2006)Englische bersetzung von DIN EN ISO 8510-2:2010-12Adhsifs Essai de pelage pour un assemblage coll flexible-sur-rigide Partie 2: Pelage 180 degrs (ISO 8510-2:2006)Traduction anglaise de DIN EN ISO 8510-2:2010-12SupersedesDIN EN 28510-2:1993-05www.beuth.deDocument comprises pagesIn case

4、of doubt, the German-language original shall be considered authoritative.1112.10 DIN EN ISO 8510-2:2010-12 2 A comma is used as the decimal marker. National foreword This standard has been prepared by Technical Committee ISO/TC 61 “Plastics” in collaboration with Technical Committee CEN/TC 193 “Adhe

5、sives” (Secretariat: AENOR, Spain). The responsible German body involved in its preparation was the Normenausschuss Materialprfung (Materials Testing Standards Committee), Working Committee NA 062-04-55 AA Prfung von Konstruktions-klebstoffen, -klebverbindungen und Kernverbunden. This document super

6、sedes DIN EN 28510-2:1993-05. The DIN Standard corresponding to the International Standard referred to in this document is as follows: ISO 291 DIN EN ISO 291 Amendments This standard differs from DIN EN 28510-2:1993-05 as follows: a) the number of the standard has been changed; b) safety precautions

7、 have been included; c) normative references have been updated; d) Figure 1 relating to the preparation of test specimens has been modified. Previous editions DIN EN 28510-2: 1993-05 National Annex NA (informative) Bibliography DIN EN ISO 291, Plastics Standard atmospheres for conditioning and testi

8、ng EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 8510-2 September 2010 ICS 83.180 Supersedes EN 28510-2:1993English Version Adhesives - Peel test for a flexible-bonded-to-rigid test specimen assembly - Part 2: 180 degree peel (ISO 8510-2:2006) Adhsifs - Essai de pelage pour un assemblage

9、coll flexible-sur-rigide - Partie 2: Pelage 180 degrs (ISO 8510-2:2006) Klebstoffe - Schlprfung fr flexibel/starr geklebte Proben - Teil 2: 180 Grad-Schlversuch (ISO 8510-2:2006) This European Standard was approved by CEN on 12 August 2010. CEN members are bound to comply with the CEN/CENELEC Intern

10、al Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN membe

11、r. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN member

12、s are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, S

13、weden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Member

14、s. Ref. No. EN ISO 8510-2:2010: EContents DIN EN ISO 8510-2:2010-12 EN ISO 8510-2:2010 (E) 2 Page Foreword3 1 Scope 4 2 Normative references 4 3 Principle4 4 Apparatus .4 5 Test specimens5 6 Conditioning and testing atmosphere.6 7 Procedure .6 8 Expression of results 6 9 Precision.7 10 Test report 7

15、 Bibliography 9 Foreword The text of ISO 8510-2:2006 has been prepared by Technical Committee ISO/TC 61 “Plastics” of the International Organization for Standardization (ISO) and has been taken over as EN ISO 8510-2:2010 by Technical Committee CEN/TC 193 “Adhesives” the secretariat of which is held

16、by AENOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by March 2011, and conflicting national standards shall be withdrawn at the latest by March 2011. Attention is drawn to the possibility that

17、some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 28510-2:1993. According to the CEN/CENELEC Internal Regulations, the national standards organizations

18、 of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, R

19、omania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 8510-2:2006 has been approved by CEN as a EN ISO 8510-2:2010 without any modification. DIN EN ISO 8510-2:2010-12 EN ISO 8510-2:2010 (E) 3 SAFETY PRECAUTIONS Persons using this document s

20、hould be familiar with normal laboratory practice, if applicable. This document does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any regulat

21、ory conditions. 1 Scope This part of ISO 8510 specifies a 180 peel test for the determination, under specified conditions, of the peel resistance of a bonded assembly of two adherends where one adherend is flexible and the other is rigid. A 90 peel test, more suitable for use with less flexible adhe

22、rends that crack, break or delaminate in the 180 peel test, is described in ISO 8510-1. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition o

23、f the referenced document (including any amendments) applies. ISO 291, Plastics Standard atmospheres for conditioning and testing ISO 17212, Structural adhesives Guidelines for the surface preparation of metals and plastics prior to adhesive bonding 3 Principle A bonded assembly of two adherends is

24、prepared using the adhesive under test. The adherends are then pulled apart at a substantially steady rate, starting at the open end of the bond, in such a way that separation occurs progressively along the length of the bonded adherends. The force is applied substantially parallel to the plane of t

25、he bond, through the separated part of the flexible adherend. 4 Apparatus 4.1 Tensile testing machine, capable of supplying a tensile force with a constant rate of grip separation. The machine shall be equipped with a force-measuring system complete with an indicator and/or a recorder. The indicated

26、 force shall not differ from the true applied force by more than 2 %. The response time of the machine shall be short enough not to affect the accuracy with which the force applied at the time of rupture can be measured. The force at rupture of the specimen shall lie in the range between 10 % and 80

27、 % of the full-scale reading. DIN EN ISO 8510-2:2010-12 EN ISO 8510-2:2010 (E) 4 4.2 Grips, one of which shall be suitable for firmly clamping the rigid adherend (5.1.2) so that the plane of the bond is parallel to the applied force, while the other shall be suitable for holding the flexible adheren

28、d (5.1.3), as shown in Figure 1. The latter grip shall be self-aligning, so that the force will be exerted parallel to the plane of the bond, and linked to the sensor of the tensile testing machine (4.1). 5 Test specimens 5.1 Adherends 5.1.1 General The adherends shall be thick enough to withstand t

29、he expected tensile force and their dimensions shall be measured accurately and reported in full in the test report. The recommended thicknesses of test specimens are: metals 1,5 mm; plastics 1,5 mm; wood 3 mm; compounded rubbers 2 mm. Other thicknesses agreed on between the purchaser and the suppli

30、er of the adhesive may be used. 5.1.2 Rigid adherend The rigid adherend shall consist of a strip of flat material of width 25,0 mm 0,5 mm and minimum length 200 mm. 5.1.3 Flexible adherend The flexible adherend shall be capable of being bent through an angle of 180 without gross irreversible dimensi

31、onal change. Unless specified otherwise, the flexible adherend shall be not less than 350 mm in length. Its width shall be either a) the same width as the rigid adherend, or b) for materials prone to fraying, e.g. cotton duck, 5 mm wider at each edge. NOTE Flexible adherends may cause difficulties i

32、n test specimen assembly and give rise to a greater dispersion of results than would otherwise be the case, because of distortion or fraying of the weave during assembly and testing. The use of a flexible adherend 5 mm wider at each edge than the rigid adherend is designed to reduce these effects. 5

33、.2 Preparation of test specimens The procedure used in preparing the test specimens shall be such as to minimize variations. The use of a pneumatic or hydraulic press, hand or power-operated, that can apply a pressure of up to 1 MPa, is recommended. Surface treatments shall be in accordance with ISO

34、 17212, or, if this is not feasible, in accordance with the manufacturers instructions. Apply the adhesive, in accordance with the manufacturers instructions, over the whole width of the adherends to a length of 150 mm on each adherend. NOTE A convenient method of obtaining a sharp adhesive boundary

35、 is to place a thin strip of material to which the adhesive does not adhere (anti-adhesive strip) at the end at which separation of one of the adherends will commence (see Figure 1). Allow the adhesive to set and, if necessary, cure it, in accordance with the manufacturers instructions. Bond the adh

36、erends using the method recommended by the manufacturer of the adhesive. DIN EN ISO 8510-2:2010-12 EN ISO 8510-2:2010 (E) 5 If a press is used to make the test specimens, it shall be capable of applying an even pressure over the entire bonded area and should preferably be fitted with a timer-control

37、led release mechanism. In order to provide a uniform distribution of pressure over the bonded area, the platens of the press shall be parallel. When this is impracticable, one platen shall be covered with a resilient pad. A 10 mm thick pad of rubber of Shore A hardness approximately 45 has been foun

38、d to be satisfactory, using a press that applies a pressure of up to 700 kPa. As an alternative to preparing individual test specimens, panels of suitable size may be bonded to each other and test specimens cut from the bonded assembly, discarding from the bonded assembly the 12 mm strip along each

39、of the outer edges parallel to the longer sides of the test specimens. Determine the average thickness of the applied adhesive as accurately as practicable, by weighing or another suitable technique. 5.3 Number of test specimens A minimum of 5 specimens shall be tested. 6 Conditioning and testing at

40、mosphere The test specimens shall be conditioned and tested in one of the standard atmospheres specified in ISO 291. 7 Procedure Bend back the unbonded end of the flexible adherend. Clamp the rigid adherend in the fixed grip and the flexible adherend in the other grip, taking care that the test spec

41、imen is accurately positioned between the grips so that the tension applied is distributed uniformly across the width of the test specimen (see Figure 1). Set the machine in motion at a constant rate of grip separation. The recommended rate of grip separation is 100 mm/min 10 mm/min. If this is not

42、practicable, other rates may be agreed on between the purchaser and supplier of the adhesive. Record the rate of grip separation. Also record the force as a function of grip separation, preferably autographically. Continue the test until at least 125 mm of the bonded length has separated. Note the t

43、ype of failure, i.e. adhesive failure, cohesive failure or adherend failure. NOTE The peeled part of the flexible adherend will rub on the adhering part as separation progresses. To reduce friction, a suitable lubricant, such as glycerol or soap solution, may be used, provided it does not affect the

44、 adherends. 8 Expression of results For each specimen, determine from the curve of force versus grip separation, the average peel force in newtons, over a peel length of at least 100 mm, but not including the first 25 mm. This may be done by drawing an estimated average line (see Figure 2) or by pla

45、nimetry, or by another suitable means if a more accurate result is required. Record the maximum and minimum force in this range. Calculate the arithmetic mean of the average peel forces for all the specimens tested, as well as the arithmetic means of the maximum and minimum forces. NOTE For the stat

46、istical treatment of results, see appropriate parts of ISO 5725. If required, initial peak values occurring outside the test peel length may be recorded separately, but are excluded from the averaging procedure. DIN EN ISO 8510-2:2010-12 EN ISO 8510-2:2010 (E) 6 9 Precision The precision of this tes

47、t method is not known because inter-laboratory data are not available. Inter-laboratory data are being obtained and a precision statement will be added at the next revision. 10 Test report The test report shall include the following information: a) a reference to this part of ISO 8510; b) a complete

48、 identification of the adhesive tested, including type, source, manufacturers code number, batch or lot number, form, etc.; c) a complete description of the adherends, including dimensions, type of material and surface preparation; d) a description of the bonding process, including the method of app

49、lication of adhesive, drying or pre-curing conditions and curing time (where applicable), and bonding temperature and pressure; e) the average thickness of the adhesive layer after formation of the bond; f) a complete description of the test specimen, including dimensions, construction and number tested; g) the conditioning procedure prior to testing, and the test atmosphere; h) the rate of separation of the grips; i) the method of determining the average peel force; j) the maximum, minimum and average values of the peel force, in new