DIN EN ISO 8986-2-2010 Plastics - Polybutene-1 (PB-1) moulding and extrusion materials - Part 2 Preparation of test specimens and determination of properties (ISO 8986-2 2009) Germ.pdf

1、April 2010 Translation by DIN-Sprachendienst.English price group 9No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 8

2、3.080.20!$aZ“1625559www.din.deDDIN EN ISO 8986-2Plastics Polybutene-1 (PB-1) moulding and extrusion materials Part 2: Preparation of test specimens and determination of properties(ISO 8986-2:2009)English translation of DIN EN ISO 8986-2:2010-04Kunststoffe Polybuten-1 (PB-1)-Formmassen Teil 2: Herste

3、llung von Probekrpern und Bestimmung von Eigenschaften(ISO 8986-2:2009)Englische bersetzung von DIN EN ISO 8986-2:2010-04Plastiques Matriaux base de polybutne-1 (PB-1) pour moulage et extrusion Partie 2: Prparation des prouvettes et dtermination des proprits (ISO 8986-2:2009)Traduction anglaise de D

4、IN EN ISO 8986-2:2010-04SupersedesDIN EN ISO 8986-2:2000-12www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.Document comprises 13 pages04.10 DIN EN ISO 8986-2:2010-04 2 A comma is used as the decimal marker. National foreword This standard has been prepare

5、d by Technical Committee ISO/TC 61 “Plastics” in collaboration with Technical Committee CEN/TC 249 “Plastics”, (Secretariat: NBN, Belgium) The responsible German body involved in its preparation was the Normenausschuss Kunststoffe (Plastics Standards Committee), Working Committee NA 054-02-06 AA For

6、mmassen aus Polyolefinen. The DIN Standards corresponding to the International Standards referred to in this document are as follows: ISO 11357-2 DIN 53765 ISO 11357-3 DIN 53765 ISO 11357-6 there is no national standard available IEC 60112 DIN EN 60112 IEC 60243-1 DIN EN 60243-1 IEC 60250 there is n

7、o national standard available IEC 60296 DIN EN 60296 IEC 60695-11-10 DIN EN 60695-11-10 All other International Standards referred to in clause 2 have been published as the corresponding DIN EN ISO or DIN IEC Standards with the same number. Amendments This standard differs from DIN EN ISO 8986-2:200

8、0-12 as follows: a) The standard has been technically revised to reflect the changes made in Part 1, i.e. “MFR” replaced by “MVR” and “density” deleted. b) “Polybutene (PB) moulding and extrusion materials” has been changed to “Polybutene-1 (PB-1) moulding and extrusion materials”. c) The normative

9、references have been updated; they are now undated. d) Subclause 3.3 “Compression moulding” and clause 4 “Conditioning of test specimens” have been extended. e) Table 2 has been revised. f) Additional mechanical properties have been deleted from Table 3. g) Table 3 now includes “Density” as an addit

10、ional property. h) The standard has been editorially revised. Previous editions DIN EN ISO 8986-2: 1995-11, 2000-12 DIN EN ISO 8986-2:2010-04 3 National Annex NA (informative) Bibliography DIN 53765, Testing of plastics and elastomers Thermal analysis DSC-method DIN EN 60112, Method for the determin

11、ation of the proof and the comparative tracking indices of solid insulating materials DIN EN 60243-1, Electrical strength of insulating materials Test methods Part 1: Test at power frequencies DIN EN 60296, Fluids for electrotechnical applications Unused mineral insulating oils for transformers and

12、switchgear DIN EN 60695-11-10, Fire hazard testing Part 11-10: Test flames 50 W horizontal and vertical flame test methods DIN EN ISO 8986-2:2010-04 4 This page is intentionally blank EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 8986-2 November 2009 ICS 83.080.20 Supersedes EN ISO 8986-2

13、:1995English Version Plastics - Polybutene-1 (PB-1) moulding and extrusion materials - Part 2: Preparation of test specimens and determination of properties (ISO 8986-2:2009) Plastiques - Matriaux base de polybutne-1 (PB-1) pour moulage et extrusion - Partie 2: Prparation des prouvettes et dterminat

14、ion des proprits (ISO 8986-2:2009) Kunststoffe - Polybuten-1 (PB-1)-Formmassen - Teil 2: Herstellung von Probekrpern und Bestimmung von Eigenschaften (ISO 8986-2:2009) This European Standard was approved by CEN on 21 October 2009. CEN members are bound to comply with the CEN/CENELEC Internal Regulat

15、ions which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. This Eu

16、ropean Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are the

17、national standards bodies of Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland

18、and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2009 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO

19、8986-2:2009: EContents Page Foreword3 1 Scope 4 2 Normative references 4 3 Preparation of test specimens .6 3.1 General6 3.2 Treatment of the material before moulding 6 3.3 Compression moulding.6 4 Conditioning of test specimens .7 5 Determination of properties7 EN ISO 8986-2:2009 (E) DIN EN ISO 898

20、6-2:2010-04 2 Foreword collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by May 2010, and conflicti

21、ng national standards shall be withdrawn at the latest by May 2010. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supe

22、rsedes EN ISO 8986-2:1995. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary

23、, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 8986-2:2009 has been approved by CEN as a EN ISO 8986-2:2009 without any modifica

24、tion. EN ISO 8986-2:2009 (E) DIN EN ISO 8986-2:2010-04 3 This document (EN ISO 8986-2:2009) has been prepared by Technical Committee ISO/TC 61 “Plastics” in 1 Scope This part of ISO 8986 specifies the methods of preparation of test specimens and the test methods to be used in determining the propert

25、ies of polybutene-1 (PB-1) moulding and extrusion materials. For the sake of simplicity, the designation polybutene and the abbreviation PB are used in both parts of ISO 8986. Requirements for handling test material and for conditioning both the test material before moulding and the specimens before

26、 testing are also specified. Procedures and conditions for the preparation of test specimens and procedures for measuring properties of the materials from which these specimens are made are given. Properties and test methods which are suitable and necessary to characterize PB moulding and extrusion

27、materials are listed. The properties have been selected from the general test methods in ISO 10350-1. Other test methods in wide use for or of particular significance to these moulding and extrusion materials are also included in this part of ISO 8986, as is the designatory property specified in Par

28、t 1. In order to obtain reproducible and comparable test results, it is necessary to use the methods of specimen preparation and conditioning, the specimen dimensions and the test procedures specified herein. Values determined will not necessarily be identical to those obtained using specimens of di

29、fferent dimensions or prepared using different procedures. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (in

30、cluding any amendments) applies. ISO 62, Plastics Determination of water absorption ISO 75-2, Plastics Determination of temperature of deflection under load Part 2: Plastics and ebonite ISO 178, Plastics Determination of flexural properties ISO 179-1, Plastics Determination of Charpy impact properti

31、es Part 1: Non-instrumented impact test ISO 179-2, Plastics Determination of Charpy impact properties Part 2: Instrumented impact test ISO 291, Plastics Standard atmospheres for conditioning and testing ISO 293, Plastics Compression moulding of test specimens of thermoplastic materials EN ISO 8986-2

32、:2009 (E) DIN EN ISO 8986-2:2010-04 4 ISO 527-2, Plastics Determination of tensile properties Part 2: Test conditions for moulding and extrusion plastics ISO 527-4, Plastics Determination of tensile properties Part 4: Test conditions for isotropic and orthotropic fibre-reinforced plastic composites

33、ISO 899-1, Plastics Determination of creep behaviour Part 1: Tensile creep ISO 1133, Plastics Determination of the melt mass-flow rate (MFR) and the melt volume-flow rate (MVR) of thermoplastics ISO 1183-1, Plastics Methods for determining the density of non-cellular plastics Part 1: Immersion metho

34、d, liquid pyknometer method and titration method ISO 1183-2, Plastics Methods for determining the density of non-cellular plastics Part 2: Density gradient column method ISO 1183-3, Plastics Methods for determining the density of non-cellular plastics Part 3: Gas pyknometer method ISO 1628-3, Plasti

35、cs Determination of the viscosity of polymers in dilute solution using capillary viscometers Part 3: Polyethylenes and polypropylenes ISO 2818, Plastics Preparation of test specimens by machining ISO 3167, Plastics Multipurpose test specimens ISO 4589-2, Plastics Determination of burning behaviour b

36、y oxygen index Part 2: Ambient-temperature test ISO 8256, Plastics Determination of tensile-impact strength ISO 8986-1, Plastics Polybutene-1 (PB-1) moulding and extrusion materials Part 1: Designation system and basis for specifications ISO 10350-1, Plastics Acquisition and presentation of comparab

37、le single-point data Part 1: Moulding materials ISO 11357-2, Plastics Differential scanning calorimetry (DSC) Part 2: Determination of glass transition temperature ISO 11357-3, Plastics Differential scanning calorimetry (DSC) Part 3: Determination of temperature and enthalpy of melting and crystalli

38、zation ISO 11357-6, Plastics Differential scanning calorimetry (DSC) Part 6: Determination of oxidation induction time (isothermal OIT) and oxidation induction temperature (dynamic OIT) IEC 60093, Methods of test for volume resistivity and surface resistivity of solid electrical insulating materials

39、 IEC 60112, Method for the determination of the proof and the comparative tracking indices of solid insulating materials IEC 60243-1, Electrical strength of insulating materials Test methods Part 1: Tests at power frequencies IEC 60250, Recommended methods for the determination of the permittivity a

40、nd dielectric dissipation factor of electrical insulating materials at power, audio and radio frequencies including metre wavelengths IEC 60296, Fluids for electrotechnical applications Unused mineral insulating oils for transformers and switchgear EN ISO 8986-2:2009 (E) DIN EN ISO 8986-2:2010-04 5

41、IEC 60695-11-10, Fire hazard testing Part 11-10: Test flames 50 W horizontal and vertical flame test methods 3 Preparation of test specimens 3.1 General The test specimens shall be prepared by compression moulding. It is essential that the specimens are always prepared by the same procedure using th

42、e same processing conditions. The material shall be kept in moisture-proof containers until it is required for use. The moisture content of filled or reinforced materials shall be expressed as a percentage of the total mass of the compound. 3.2 Treatment of the material before moulding Before proces

43、sing, no pretreatment of the material sample is normally necessary. 3.3 Compression moulding Compression-moulded sheets shall be prepared in accordance with ISO 293, using the conditions specified in Table 1. Table 1 Conditions for compression moulding of test specimens Moulding temperatureAverage c

44、ooling rate Demoulding temperatureFull pressure Full-pressure time Preheating pressure Preheating time Material C C/min C MPa min MPa min All grades 200 30 30 5 5 or 10a5 1 Contact 5 to 15 aUse 5 MPa with a frame mould and 10 MPa with a positive mould. The test specimens required for the determinati

45、on of the properties shall be machined from the compression-moulded sheets in accordance with ISO 2818 or punched out. A type 1 (frame) mould may be used, but it is necessary to start cooling whilst simultaneously applying the full pressure. This avoids the melt being pressed out of the frame and av

46、oids sink marks. For thicker sheet ( 4 mm), a type 2 (positive) mould has been found to work satisfactorily. The preheating time depends on the type of mould and the type of energy input (steam or electricity). For frame moulds, 5 min is usually sufficient but for positive moulds, due to the bigger

47、mass, a preheating time of up to 15 min may be necessary, especially if electric heating is used. NOTE 1 Since only the average cooling rate is specified, the actual cooling rate during crystallization is not fixed. This can lead to significant deviations in properties related to crystallinity, such

48、 as density and mechanical properties. NOTE 2 Since for frame moulds full pressure is only applied upon cooling, compression-moulded sheets may suffer from insufficient homogeneity and pellet boundaries may be preserved if the heating time or the pressure is insufficient. EN ISO 8986-2:2009 (E) DIN

49、EN ISO 8986-2:2010-04 6 4 Conditioning of test specimens Before testing, test specimens shall be conditioned at atmospheric pressure in one of the standard atmospheres specified in ISO 291 for the length of time recommended by the material manufacturer. The conditioning atmosphere and conditioning time used shall be reported along with the test conditions in the test report. Due to the temperature dependence of the conditioning pro