DIN ISO 16000-25-2012 Indoor air - Part 25 Determination of the emission of semi-volatile organic compounds by building products - Micro-chamber method (ISO 16000-25 2011)《室内空气 第25.pdf

1、Translation by DIN-Sprachendienst.English price group 14No part of this translation may be reproduced without prior permission ofDIN Deutsches Institut fr Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,has the exclusive right of sale for German Standards (DIN-Normen).ICS 13.040.20!$

2、y+N“1860843www.din.deDDIN ISO 16000-25Indoor air Part 25: Determination of the emission of semi-volatile organiccompounds by building products Micro-chamber method (ISO 16000-25:2011)English translation of DIN ISO 16000-25:2012-01Innenraumluftverunreinigungen Teil 25: Bestimmung der Emission von sch

3、werflchtigen organischen Verbindungen ausBauprodukten Mikro-Prfkammerverfahren (ISO 16000-25:2011)Englische bersetzung von DIN ISO 16000-25:2012-01Air intrieur Partie 25: Dosage de lmission de composs organiques semi-volatils des produits deconstruction Mthode de la micro-chambre (ISO 16000-25:2011)

4、Traduction anglaise de DIN ISO 16000-25:2012-01www.beuth.deIn case of doubt, the German-language original shall be considered authoritative.This standard has been included in the VDI/DIN Handbooks on air quality, Volume 5. Document comprises 31 pages12.110 January 2012Contents Page National foreword

5、 . 3 National Annex NA (informative) Bibliography 5 Introduction . 8 1 Scope . 9 2 Normative references 9 3 Terms and definitions 9 4 Symbols 12 5 Principle 12 6 Micro-chamber system 12 7 Apparatus and materials . 16 8 Test conditions . 16 9 Verification of test conditions . 17 10 Test specimens 18

6、11 Micro-chamber preparation . 18 12 Test method 18 13 Calculation of area specific emission rates and expression of results . 19 14 Performance characteristics . 19 15 Test report . 19 Annex A (normative) System for quality assurance and quality control (QA/QC) . 21 Annex B (informative) Examples o

7、f micro-chambers and procedure . 23 Annex C (informative) Example of a method of micro-chamber recovery Measurement . 27 Annex D (informative) Selection of test specimens 29 Bibliography 31 20 DIN ISO 16000-25:2012-01A comma is used as the decimal marker. 30 DIN ISO 16000-25:2012-01National foreword

8、 International technical regulation pertaining to indoor air This standard has been prepared by Technical Committee ISO/TC 146 “Air quality”, Subcommittee SC 6 “Indoor air” (Secretariat: DIN, Germany). The responsible German body involved in its preparation was the Kommission Reinhaltung der Luft (K

9、RdL) im VDI und DIN Normenausschuss (Commission on Air Pollution Prevention of VDI and DIN Standards Committee), Section IV Umweltmesstechnik. General and substance-specific aspects which should be taken into account before and during sampling, as well as methods for determining individual substance

10、s or groups of substances and microorganisms in indoor air are described in the various parts of ISO 16000. The DIN Standards corresponding to the International Standards referred to in clause 2 of this standard are as follows: ISO 554 DIN EN ISO 554 ISO 16000-6 DIN ISO 16000-6 ISO 16000-11 DIN EN I

11、SO 16000-11 ISO 16017-1 DIN EN ISO 16017-1 Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. DIN shall not be held responsible for identifying any or all such patent rights. National technical regulation pertaining to indoor air Gen

12、eral conditions and other aspects to be taken into consideration when planning indoor air measurements are described for individual substances and substance groups in the VDI 4300 series (see also “National Annex NA”). Many of these served as the sole basis for parts of the ISO 16000 series (e.g. IS

13、O 16000-1, ISO 16000-2, ISO 16000-5, ISO 16000-7, ISO 16000-12, ISO 16000-15, ISO 16000-16, ISO 16000-17 and ISO 16000-18). The specific procedures (sampling, analysis) are described in the VDI 4301 series for individual substances and substance groups. Methods which can be used for both indoor and

14、ambient air measurements are described in further VDI guidelines. The DIN ISO 16000 series and DIN EN ISO 16000 series consist of the following parts, under the general title Indoor air: DIN EN ISO 16000-1, General aspects of sampling strategy DIN EN ISO 16000-2, Sampling strategy for formaldehyde D

15、IN ISO 16000-3, Determination of formaldehyde and other carbonyl compounds Active sampling method DIN ISO 16000-4, Determination of formaldehyde Diffusive sampling method DIN EN ISO 16000-5, Sampling strategy for volatile organic compounds (VOCs) DIN ISO 16000-6, Determination of volatile organic co

16、mpounds in indoor and test chamber air by active sampling on Tenax TAsorbent, thermal desorption and gas chromatography using MS/FID DIN EN ISO 16000-7, Sampling strategy for determination of airborne asbestos fibre concentrations DIN ISO 16000-8, Determination of local mean ages of air in buildings

17、 for characterizing ventilation conditions DIN EN ISO 16000-9, Determination of the emission of volatile organic compounds from building products and furnishing Emission test chamber method DIN EN ISO 16000-10, Determination of the emission of volatile organic compounds from building products and fu

18、rnishing Emission test cell method DIN EN ISO 16000-11, Determination of the emission of volatile organic compounds from building products and furnishing Sampling, storage of samples and preparation of test specimens DIN EN ISO 16000-12, Sampling strategy for polychlorinated biphenyls (PCBs), polych

19、lorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polycyclic aromatic hydrocarbons (PAHs) DIN ISO 16000-13: Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs) Coll

20、ection on sorbent-backed filters DIN ISO 16000-14, Determination of total (gas and particle-phase) polychlorinated dioxin-like biphenyls (PCBs) and polychlorinated dibenzo-p-dioxins/dibenzofurans (PCDDs/PCDFs) Extraction, clean-up and analysis by high-resolution gas chromatography/mass spectrometry

21、DIN EN ISO 16000-15, Sampling strategy for nitrogen dioxide (NO2) DIN ISO 16000-16, Detection and enumeration of moulds Sampling by filtration DIN ISO 16000-17, Detection and enumeration of moulds Culture-based method DIN ISO 16000-18, Detection and enumeration of moulds Sampling by impaction DIN IS

22、O 16000-19, Sampling strategy for moulds DIN ISO 16000-23, Performance test for evaluating the reduction of formaldehyde concentrations by sorptive building materials DIN ISO 16000-24, Performance test for evaluating the reduction of volatile organic compounds and carbonyl compounds without formalde

23、hyde concentrations by sorptive building materials DIN ISO 16000-25, Determination of the emission of semi-volatile organic compounds by building products Micro-chamber method DIN EN ISO 16000-26, Sampling strategy for carbon dioxide (CO2) DIN ISO 16000-28, Determination of odour emissions from buil

24、ding products using test chambers The following parts are under preparation: DIN ISO 16000-21, Detection and enumeration of moulds Sampling from materials DIN ISO 16000-27, Determination of settled fibrous dust on surfaces by SEM (scanning electron micros-copy) (direct method) DIN ISO 16000-29, Test

25、 methods for VOC detectors 40 DIN ISO 16000-25:2012-01 DIN ISO 16000-30, Sensory testing of indoor air DIN ISO 16000-31, Measurement of flame retardants and plasticizers based on organophosphorus compounds Phosphoric acid ester DIN ISO 16000-32, Investigation of constructions on pollutants and other

26、 injurious factors Inspections The following parts are planned: DIN ISO 16000-20, Detection and enumeration of moulds Sampling from house dust DIN ISO 16000-22, Detection and enumeration of moulds Molecular methods National Annex NA (informative) Bibliography DIN EN ISO 5492, Sensory analysis Vocabu

27、lary DIN EN ISO 8589, Sensory analysis General guidance for the design of test rooms DIN 50014, Climates and their technical application Standard atmospheres DIN EN ISO 8199, Water quality General guidance on the enumeration of micro-organisms by culture DIN EN ISO 9169, Air quality Definition and d

28、etermination of performance characteristics of an automatic measuring system DIN ISO 12219-1, Indoor air of road vehicles Part 1: Whole vehicle test chamber Specification and method for the determination of volatile organic compounds in cabin interiors (under preparation) DIN ISO 12219-2, Indoor air

29、 of road vehicles Part 2: Screening method for the determination of the emissions of volatile organic compounds from vehicle interior parts and materials Bag method (under preparation) DIN ISO 12219-3, Indoor air of road vehicles Part 3: Screening method for the determination of the emissions of vol

30、atile organic compounds from vehicle interior parts and materials Micro-chamber method (under preparation) DIN ISO 12219-4, Indoor air of road vehicles Part 4: Method for determination of the emissions of volatile organic compounds from car trim components Small chamber method (under preparation) DI

31、N ISO 12884, Ambient air Determination of total (gas and particle phase) polycyclic aromatic hydrocarbons Collection on sorbent-backed filters with gas chromatographic/mass spectrometric analysis DIN V ENV 13005, Guide to the expression of uncertainty in measurement DIN EN 14412, Indoor air quality

32、Diffusive samplers for the determination of concentrations of gases and vapours Guide for selection, use and maintenance 50 DIN ISO 16000-25:2012-01DIN EN ISO 16017-1, Indoor, ambiant and workplace air Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary g

33、as chromatography Part 1: Pumped sampling DIN EN ISO 16017-2, Indoor, ambient and workplace air Sampling and analysis of volatile organic compounds by sorbent tube/thermal desorption/capillary gas chromatography Part 2: Diffusive sampling DIN ISO 16362, Ambient air Determination of particle-phase po

34、lycyclic aromatic hydrocarbons by high performance liquid chromatography DIN EN ISO/IEC 17025, General requirements for the competence of testing and calibration laboratories VDI 2464 Part 1, Ambient air measurement Indoor air measurement Measurement of polychlorinated biphynyls (PCBs); GC/MS method

35、 for PCB 28, 52, 101, 138, 153, 180 VDI 2464 Part 2, Ambient air measurement Indoor air measurement Measurement of polychlorinated biphenyls (PCBs); HR-GC/HR-MS method for coplanar PCBs VDI 2464 Part 3, Ambient air measurement Indoor air measurement Measurement of polybrominated diphenylether, hexab

36、romocyclododecane and hexabromobenzene VDI 3484 Part 1, Gaseous ambient air measurements Indoor-air pollution measurements Test gases measurements; Measurement of the formaldehyde concentration with the sulfite pararosaniline method VDI 3484 Part 2, Gaseous ambient air measurements Indoor-air pollut

37、ion measurements Measurement of the formaldehyde concentration with the acatylacetone method VDI 3498 Part 1, Ambient air measurement Indoor air measurement Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans Method using large filters VDI 3498 Part 2, Ambient air measurement Indoor a

38、ir measurement Measurement of polychlorinated dibenzo-p-dioxins and dibenzofurans Method using small filters VDI 4252 Part 2, Measurement of airborne microorganisms and viruses in ambient air Active sampling of bioaerosols Separation of airborne mould on gelatine/polycarbonate filters VDI 4253 Part

39、2, Measurement of airborne microorganisms and viruses in ambient air Culture based method for the determination of the concentration of mould in air Indirect method after sampling with gelatine/polycarbonate filters VDI 4300 Part 1, Indoor-air pollution measurement General aspects of measurement str

40、ategy VDI 4300 Part 2, Indoor-air pollution measurement Measurement strategy for polycyclic aromatic hydrocarbons (PAHs), polychlorinated dibenzo-p-dioxins (PCDDs), polychlorinated dibenzofurans (PCDFs) and polychlorinated biphenyls (PCBs) VDI 4300 Part 4, Indoor air pollution measurement Measuremen

41、t strategy for pentachlorophenol (PCP) and -hexachlorocyclohexane (lindane) in indoor air VDI 4300 Part 5, Indoor air pollution measurement Measurement strategy for nitrogen dioxide (NO2) VDI 4300 Part 6, Measurement of indoor air pollution Measurement strategy for volatile organic compounds (VOCs)

42、VDI 4300 Part 7, Indoor-air pollution measurement Measurement of indoor air change rate VDI 4300 Part 8, Measurement of indoor air pollution Sampling of house dust 60 DIN ISO 16000-25:2012-01VDI 4300 Part 9, Measurement of indoor air pollution Measurement strategy for carbon dioxide (CO2) VDI 4300 P

43、art 10, Measurement of indoor air pollution Measurement strategies for determination of mould fungi in indoor environment VDI 4301 Part 1, Indoor air pollution measurement Determination of the concentration of nitrogen dioxide Manual photometric method (Saltzman) VDI 4301 Part 2, Indoor air pollutio

44、n measurement Measurement of pentaclorophenol (PCP) and -hexachlorocyclohexane (lindane) GC/MS-method VDI 4301 Part 3, Measurement of indoor air pollution Measurement of pentaclorophenol (PCP) and -hexachlorocyclohexane (lindane) GC/ECD method VDI 4301 Part 4, Measurement of indoor air pollution Mea

45、surement of pyrethroids and piperonyl butoxide in air, house dust and solvent wipe samples VDI 4301 Part 5, Measurement of indoor air pollution Measurement of flame retardants and plasticizers based on phosphor organic compounds Phosphoric acid ester VDI 4301 Part 6, Measurement of indoor air pollut

46、ion Measurement of phthalates The following VDI Guidelines are under preparation: VDI 4300 Part 11, Measurement of indoor air pollution Measurement strategies for determination of airborne particles in indoor environment Particles with equivalent diameter 2,5 m VDI 4301 Part 7, Measurement of indoor

47、 air pollution Measurement of carboxylic acids 70 DIN ISO 16000-25:2012-01Introduction The determination of semi-volatile organic compounds (SVOCs) emitted from building products using micro-chambers in conjunction with standardized sampling, storage of samples and preparation of test specimens aims

48、, for example, to: provide manufacturers, builders, and end-users with emission data useful for the evaluation of the impact of building products on the indoor air quality; promote the development of improved products. The measurement method specified in this part of ISO 16000 is applicable to produ

49、cts used in construction such as board materials, wallpapers, flooring materials, insulation materials, adhesives, paints, and their combinations. SVOCs such as phthalic esters are found in many construction materials. If emitted into the indoor environment they adhere to many surfaces and can become a persistent indoor air contaminant. This p