1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS EN 12697-39:2012Bituminous mixtures Testmethods for hot mix asphaltPart 39: Binder content by ignitionBS EN 12697-39:2012 BRITISH STANDARDNational forewordThis British Standar
2、d is the UK implementation of EN 12697-39:2012.It supersedes BS EN 12697-39:2004 which is withdrawn.The UK participation in its preparation was entrusted to TechnicalCommittee B/510/1, Asphalt products.A list of organizations represented on this committee can beobtained on request to its secretary.T
3、his publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. The British Standards Institution 2012. Published by BSI StandardsLimited 2012 ISBN 978 0 580 76410 3 ICS 93.080.20 Compliance with a British Standard cannot confe
4、r immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and Strategy Committee on 31 August 2012. Amendments issued since publicationDate T e x t a f f e c t e dBS EN 12697-39:2012EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 12697-39 Ju
5、ne 2012 ICS 93.080.20 Supersedes EN 12697-39:2004English Version Bituminous mixtures - Test methods for hot mix asphalt - Part 39: Binder content by ignition Mlanges bitumineux - Mthodes dessai pour mlange hydrocarbon chaud - Partie 39: Dtermination de la teneur en liant par calcination Asphalt - Pr
6、fverfahren fr Heiasphalt - Teil 39: Bindemittelgehalt durch Thermoanalyse This European Standard was approved by CEN on 28 April 2012. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national s
7、tandard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version i
8、n any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
9、Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMI
10、T EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2012 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 12697-39:2012: EBS EN 12697-39:2012EN 12697-39:2012 (E) 2 Contents
11、Page Foreword 31 Scope 72 Normative references 73 Terms and definitions .74 Principle 85 Apparatus .85.1 Furnace .86 Preparatory treatment of laboratory samples of bituminous mixtures. 107 Procedure 107.1 General . 107.2 Test procedure for furnace with internal balance (Method A) . 117.3 Procedure f
12、or furnace without internal balance (Method B) 128 Calculation . 128.1 Method A 128.2 Method B 139 Test report . 1410 Precision data . 14Annex A (normative) Calculation of calibration value 15A.1 General . 15A.2 Calibration based on laboratory-prepared bituminous mixtures 15A.3 Calibration based on
13、parallel analysis with extraction methods . 16A.4 Calibration based on dry analysis of constituent aggregate . 16Annex B (informative) Aggregate grading . 19Bibliography . 20BS EN 12697-39:2012EN 12697-39:2012 (E) 3 Foreword This document (EN 12697-39:2012) has been prepared by Technical Committee C
14、EN/TC 227 “Road materials”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by December 2012, and conflicting national standards shall be withdrawn at the lat
15、est by December 2012. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 12697-39:2004. The significant techn
16、ical changes made to EN 12697-39:2004 include the following: a) The need for calibration of a mixture is clarified in the scope; b) The definitions for precision concepts are removed; c) Minor clarifications in the principle; d) The nesting of baskets is clarified in the equipment; e) The tolerance
17、on the temperature of the oven is widened; f) The maximum weight requirements of the external balance are corrected; g) The note that the calibration value based on dry analysis of constituent aggregate can only be regarded as an estimate is deleted; h) The catch pan to be placed in the furnace with
18、 the sample baskets is added; i) Note added that the mass of the sample baskets and catch pan need not be measured if the binder content is to be calculated using the mass loss directly; j) In Annex A, the total binder load is limited to 150 g; k) Precision added to Annex B. This European Standard i
19、s one of a series of standards for Bituminous mixtures as listed below: EN 12697-1, Bituminous mixtures Test methods for hot mix asphalt Part 1: Soluble binder content EN 12697-2, Bituminous mixtures Test methods for hot mix asphalt Part 2: Determination of particle size distribution EN 12697-3, Bit
20、uminous mixtures Test methods for hot mix asphalt Part 3: Bitumen recovery: Rotary evaporator EN 12697-4, Bituminous mixtures Test methods for hot mix asphalt Part 4: Bitumen recovery: Fractionating column EN 12697-5, Bituminous mixtures Test methods for hot mix asphalt Part 5: Determination of the
21、maximum density BS EN 12697-39:2012EN 12697-39:2012 (E) 4 EN 12697-6, Bituminous mixtures Test methods for hot mix asphalt Part 6: Determination of bulk density of bituminous specimens EN 12697-7, Bituminous mixtures Test methods for hot mix asphalt Part 7: Determination of bulk density of bituminou
22、s specimens by gamma rays EN 12697-8, Bituminous mixtures Test methods for hot mix asphalt Part 8: Determination of void characteristics of bituminous specimens EN 12697-10, Bituminous mixtures Test methods for hot mix asphalt Part 10: Compactability EN 12697-11, Bituminous mixtures Test methods for
23、 hot mix asphalt Part 11: Determination of the affinity between aggregate and bitumen EN 12697-12, Bituminous mixtures Test methods for hot mix asphalt Part 12: Determination of the water sensitivity of bituminous specimens EN 12697-13, Bituminous mixtures Test methods for hot mix asphalt Part 13: T
24、emperature measurement EN 12697-14, Bituminous mixtures Test methods for hot mix asphalt Part 14: Water content EN 12697-15, Bituminous mixtures Test methods for hot mix asphalt Part 15: Determination of the segregation sensitivity EN 12697-16, Bituminous mixtures Test methods for hot mix asphalt Pa
25、rt 16: Abrasion by studded tyres EN 12697-17, Bituminous mixtures Test methods for hot mix asphalt Part 17: Particle loss of porous asphalt specimen EN 12697-18, Bituminous mixtures Test methods for hot mix asphalt Part 18: Binder drainage EN 12697-19, Bituminous mixtures Test methods for hot mix as
26、phalt Part 19: Permeability of specimen EN 12697-20, Bituminous mixtures Test methods for hot mix asphalt Part 20: Indentation using cube or cylindrical specimens (CY) EN 12697-21, Bituminous mixtures Test methods for hot mix asphalt Part 21: Indentation using plate specimens EN 12697-22, Bituminous
27、 mixtures Test methods for hot mix asphalt Part 22: Wheel tracking EN 12697-23, Bituminous mixtures Test methods for hot mix asphalt Part 23: Determination of the indirect tensile strength of bituminous specimens EN 12697-24, Bituminous mixtures Test methods for hot mix asphalt Part 24: Resistance t
28、o fatigue EN 12697-25, Bituminous mixtures Test methods for hot mix asphalt Part 25: Cyclic compression test EN 12697-26, Bituminous mixtures Test methods for hot mix asphalt Part 26: Stiffness EN 12697-27, Bituminous mixtures Test methods for hot mix asphalt Part 27: Sampling EN 12697-28, Bituminou
29、s mixtures Test methods for hot mix asphalt Part 28: Preparation of samples for determining binder content, water content and grading EN 12697-29, Bituminous mixtures Test methods for hot mix asphalt Part 29: Determination of the dimensions of a bituminous specimen BS EN 12697-39:2012EN 12697-39:201
30、2 (E) 5 EN 12697-30, Bituminous mixtures Test methods for hot mix asphalt Part 30: Specimen preparation by impact compactor EN 12697-31, Bituminous mixtures Test methods for hot mix asphalt Part 31: Specimen preparation by gyratory compactor EN 12697-32, Bituminous mixtures Test methods for hot mix
31、asphalt Part 32: Laboratory compaction of bituminous mixtures by vibratory compactor EN 12697-33, Bituminous mixtures Test methods for hot mix asphalt Part 33: Specimen prepared by roller compactor EN 12697-34, Bituminous mixtures Test methods for hot mix asphalt Part 34: Marshall test EN 12697-35,
32、Bituminous mixtures Test methods for hot mix asphalt Part 35: Laboratory mixing EN 12697-36, Bituminous mixtures Test methods for hot mix asphalt Part 36: Determination of the thickness of a bituminous pavement EN 12697-37, Bituminous mixtures Test methods for hot mix asphalt Part 37: Hot sand test
33、for the adhesivity of binder on precoated chippings for HRA EN 12697-38, Bituminous mixtures Test methods for hot mix asphalt Part 38: Common equipment and calibration EN 12697-39, Bituminous mixtures Test methods for hot mix asphalt Part 39: Binder content by ignition EN 12697-40, Bituminous mixtur
34、es Test methods for hot mix asphalt Part 40: In-situ drainability EN 12697-41, Bituminous mixtures Test methods for hot mix asphalt Part 41: Resistance to de-icing fluids EN 12697-42, Bituminous mixtures Test methods for hot mix asphalt Part 42: Amount of coarse foreign matter in reclaimed asphalt E
35、N 12697-43, Bituminous mixtures Test methods for hot mix asphalt Part 43: Resistance to fuel EN 12697-44, Bituminous mixtures Test methods for hot mix asphalt Part 44: Crack propagation by semi-circular bending test EN 12697-45, Bituminous mixtures Test methods for hot mix asphalt Part 45: Saturatio
36、n ageing tensile stiffness (SATS) conditioning test EN 12697-46, Bituminous mixtures Test methods for hot mix asphalt Part 46: Low temperature cracking and properties by uniaxial tension tests EN 12697-47, Bituminous mixtures Test methods for hot mix asphalt Part 47: Determination of the ash content
37、 of natural asphalts prEN 12697-48, Bituminous mixtures Test methods for hot mix asphalt Part 48: Interlayer bonding1)prEN 12697-49, Bituminous mixtures Test methods for hot mix asphalt Part 49: Determination of friction after polishing1)BS EN 12697-39:2012EN 12697-39:2012 (E) 6 prEN 12697-50, Bitum
38、inous mixtures Test methods for hot mix asphalt Part 50: Scuffing resistance of surface course1)WARNING The temperature of the oven and the different accessories is extremely high during the ignition method. Special care shall be taken when handling the equipment and the samples baskets etc. should
39、be placed, shielded and marked in a way that helps ensure any unpremeditated contact is avoided. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cypr
40、us, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. 1) In preparation. BS EN 1269
41、7-39:2012EN 12697-39:2012 (E) 7 1 Scope This document describes a test method for the determination of the binder content of samples of bituminous mixtures by ignition. As such, it is an alternative to the more traditional method of extracting the binder using solvents. The method can be used for ev
42、aluation of mixture composition because the remaining aggregate can be used for determining aggregate gradation and density, provided excessive breakdown of the aggregate particles does not occur at the temperature reached. The results can be used for process control or checks on the compliance of m
43、ixtures. However, the need for calibration of a mixture, either on the complete mixture or on each of its component materials separately, before an analysis can be carried out makes this method easier to use with regularly used mixtures rather than with an extensive range of different mixtures from
44、different aggregate sources. The test method is equally suitable for the analysis of mixtures containing unmodified or modified binders because the method has to be calibrated for each mixture being checked when calibration on mixtures is used. In case of doubt/dispute, the determination of the cali
45、bration value based on laboratory-prepared bituminous mixtures (see A.1 and A.2) is the reference method. 2 Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition
46、 cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 12597, Bitumen and bituminous binders Terminology EN 12697-1, Bituminous mixtures Test methods for hot mix asphalt Part 1: Soluble binder content EN 12697-14, Bituminous mixtu
47、res Test methods for hot mix asphalt Part 14: Water content EN 12697-27, Bituminous mixtures Test methods for hot mix asphalt Part 27: Sampling EN 12697-28, Bituminous mixtures Test methods for hot mix asphalt Part 28: Preparation of samples for determining binder content, water content and grading
48、3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 binder covers both bitumen and bituminous binder as described in EN 12597 3.2 corrected binder content calculated binder content after correction by the calibration value in order to compensate
49、for components in the asphalt material itself that, due to the high temperatures during ignition, could give rise to misinterpretations 3.3 calibration value mean difference between the actual and measured binder contents for a particular bituminous mixture, in per cent, as measured from three samples Note 1 to
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