EN 12802-2011 en Road marking materials - Laboratory methods for identification《公路标记材料 识别用实验室方法》.pdf

1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS EN 12802:2011Road marking materials Laboratory methods foridentificationBS EN 12802:2011 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN

2、12802:2011. Itsupersedes BS EN 12802:2000 which is withdrawn.The UK participation in its preparation was entrusted to TechnicalCommittee B/509/2, Horizontal road markings and road studs.A list of organizations represented on this committee can beobtained on request to its secretary.This publication

3、does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. BSI 2011ISBN 978 0 580 72622 4ICS 93.080.20Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority

4、of theStandards Policy and Strategy Committee on 30 June 2011.Amendments issued since publicationDate Text affectedBS EN 12802:2011EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 12802 June 2011 ICS 93.080.20 Supersedes EN 12802:2000English Version Road marking materials - Laboratory methods fo

5、r identification Produits de marquage routier - Mthodes de laboratoire pour identification Straenmarkierungsmaterialien - Laborverfahren fr die Identifikation This European Standard was approved by CEN on 22 April 2011. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which

6、stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This Europ

7、ean Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are

8、 the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden

9、, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2011 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Re

10、f. No. EN 12802:2011: EBS EN 12802:2011EN 12802:2011 (E) 2 Contents Foreword . 31 Scope . 42 Normative references . 43 Terms and definitions 44 Sampling 55 Test methods . 56 Test Report 9Annex A (normative) Paint Test method for the determination of the solids content 10Annex B (normative) Paint, th

11、ermoplastics and cold plastics Test method for the determination and identification of organic constituents 12Annex C (normative) Paint, thermoplastic and cold plastic Test method for the determination and identification of inorganic constituents 16Annex D (normative) Paint, thermoplastics and cold

12、plastics Test method for the determination of the titanium (IV) dioxide content in the inorganic compound 18Annex E (normative) Paint, thermoplastics and cold plastics Test method for the determination of the glass bead content . 21Annex F (normative) Paint and cold plastics Test method for the dete

13、rmination and identification of solvents 23Annex G (normative) Paint Test method for the determination of viscosity (Krebs-Stormer method) 26Annex H (normative) Paint, thermoplastics and cold plastics Test method for the determination of the ash content . 31Bibliography . 33BS EN 12802:2011EN 12802:

14、2011 (E) 3 Foreword This document (EN 12802:2011) has been prepared by Technical Committee CEN/TC 226 “Road equipment”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at

15、 the latest by December 2011, and conflicting national standards shall be withdrawn at the latest by December 2011. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying a

16、ny or all such patent rights. This document supersedes EN 12802:2000. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark

17、, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. The Annexes A to H of this European Standard are normative. This

18、 European Standard is one of a package of inter-related European Standards with a common date of withdrawal (dow) fixed on December 2011 (including the request of an extension fo the co-existence period): EN 1790, Road marking materials Preformed road markings, EN 1824, Road marking materials Road t

19、rials, EN 1871, Road marking materials Paint, thermoplastic and cold plastic materials Specifications, EN 12802, Road marking materials Laboratory methods for identification, EN 13197, Road marking materials Wear simulator Turntable, EN 13212, Road marking materials Requirements for factory producti

20、on control, EN 13459, Road marking materials Sampling and testing. BS EN 12802:2011EN 12802:2011 (E) 4 1 Scope This document specifies laboratory methods for the identification of road marking materials used in horizontal signalization. It is not necessary, unless required, to perform all of the tes

21、ts described. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 1423, Roa

22、d marking materials Drop on materials Glass beads, antiskid aggregates and mixtures of the two EN 1424, Road marking materials Premix glass beads EN 1790, Road marking materials Preformed road markings EN 13459, Road marking materials Sampling and testing EN ISO 11890-2, Paints and varnishes Determi

23、nation of volatile organic compound (VOC) content Part 2: Gas-chromatographic method (ISO 11890-2:2006) EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes Sampling (ISO 15528:2000) ISO 5725-2, Accuracy (trueness and precision) of measurement methods and results Part 2: Basic

24、method for the determination of repeatability and reproducibility of a standard measurement method 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 paints liquid product containing binders, pigments, extenders, solvents and additives NOTE It c

25、an be supplied in single or multi-component systems. When applied it produces a cohesive film by the process of solvent evaporation, or solvent evaporation and a chemical reaction. 3.2 cold plastics viscous products supplied in two or multi-component forms (at least one main component and a hardener

26、 system) and free from solvents NOTE The cohesive film is formed after mixing of all components only by a chemical reaction. Following the reaction, the liquid becomes a solid. 3.3 thermoplastics solvent-free marking substance supplied in block, granular or powder forms NOTE It is heated to a molten

27、 state and then applied. It forms a cohesive film by cooling. BS EN 12802:2011EN 12802:2011 (E) 5 4 Sampling Samples representative of each component of the material shall be taken from storage, or prior to application, in accordance with EN 13459. Smaller representative samples, of sufficient quant

28、ity to carry out all the tests required, shall be taken from the larger samples. For paints and cold plastics approximately 1 l of the basic component shall be taken. In the case of thermoplastic in powder form, sufficient quantity shall be taken in accordance with EN 13459 so that it can be melted

29、in a metal container and mixed to a homogeneous mass. After cooling and casting into solid sheets or blocks, representative samples of approximately 1 kg of homogeneous solid material shall be taken for testing. 5 Test methods 5.1 General The standard test methods are listed in 5.2 to 5.4. Alternati

30、ve quantitative analytical test methods may be used providing that: the resulting values are comparable to those obtained using the standard methods; and, the repeatability of the alternative methods, determined in accordance with ISO 5725-2, can be shown to be not less than that of the methods give

31、n in this standard. 5.2 Paint 5.2.1 Density The density of the paint shall be determined using, either the method laid down in EN ISO 2811-1, or an alternative method complying with 5.1. 5.2.2 Solids content The solids content of the paint, expressed as a percentage, shall be determined using, eithe

32、r the method described in Annex A, or an alternative method complying with 5.1. 5.2.3 Organic content and identification The type of organic materials, and the content expressed as a percentage, of the paint shall be determined using, either the method described in Annex B, or an alternative method

33、complying with 5.1. 5.2.4 Inorganic content and identification The type of inorganic materials, and the content expressed as a percentage, of the paint shall be determined using, either the method described in Annex C, or an alternative method complying with 5.1. 5.2.5 Titanium dioxide content The t

34、itanium dioxide content of the inorganic compound of the paint, expressed as a percentage, shall be determined, either by the method described in Annex D, or an alternative method complying with 5.1. 5.2.6 Glass bead content The glass bead content of the paint, expressed as a percentage, shall be de

35、termined, either as described in Annex E, or an alternative method complying with 5.1. BS EN 12802:2011EN 12802:2011 (E) 6 5.2.7 Solvent content and identification The type of solvent, and the content expressed as a percentage, of the paint shall be determined using, either the method described in A

36、nnex F, or an alternative method complying with 5.1. 5.2.8 Viscosity The viscosity of the paint shall be determined using, either the method described in Annex G, or an alternative method complying with 5.1. 5.2.9 Ash content The ash content of the paint shall be determined using, either the method

37、described in Annex H, or an alternative method complying with 5.1. 5.3 Thermoplastics 5.3.1 Density The density of the thermoplastics shall be determined using, either the method laid down in EN ISO 2811-2, or an alternative method complying with 5.1. 5.3.2 Organic content and identification The typ

38、e of organic materials, and the content expressed as a percentage, of the thermoplastics shall be determined using, either the method described in Annex B, or an alternative method complying with 5.1. 5.3.3 Inorganic content and identification The type of inorganic materials, and the content express

39、ed as a percentage, of the thermoplastics shall be determined using, either the method described in Annex C, or an alternative method complying with 5.1. 5.3.4 Titanium dioxide content The titanium dioxide content of the inorganic compound of the thermoplastics, expressed as a percentage, shall be d

40、etermined, either by the method described in Annex D, or an alternative method complying with 5.1. 5.3.5 Glass bead content The glass bead content of the thermoplastics, expressed as a percentage, shall be determined, either as described in Annex E, or an alternative method complying with 5.1. 5.3.6

41、 Ash content The ash content of the thermoplastics shall be determined using, either the method described in Annex H, or an alternative method complying with 5.1. 5.4 Cold plastics 5.4.1 Density The density of the cold plastics shall be determined using, either the method laid down in EN ISO 2811-2,

42、 or an alternative method complying with 5.1. BS EN 12802:2011EN 12802:2011 (E) 7 5.4.2 Organic content and identification The type of organic materials, and the content expressed as a percentage, of the cold plastics shall be determined using, either the method described in Annex B, or an alternati

43、ve method complying with 5.1. 5.4.3 Inorganic content and identification The type of inorganic materials, and the content expressed as a percentage, of the cold plastics shall be determined using, either the method described in Annex C, or an alternative method complying with 5.1. 5.4.4 Titanium dio

44、xide content The titanium dioxide content of the inorganic compound of the cold plastics, expressed as a percentage, shall be determined, either by the method described in Annex D, or an alternative method complying with 5.1. 5.4.5 Glass bead content The glass bead content of the cold plastics, expr

45、essed as a percentage, shall be determined, either as described in Annex E, or an alternative method complying with 5.1. 5.4.6 Solvent content and identification The type of solvent, and the content expressed as a percentage, of the cold plastics shall be determined using, either the method describe

46、d in Annex F, or an alternative method complying with 5.1. 5.4.7 Viscosity The viscosity of the cold plastics shall be determined using, either the method laid down in EN ISO 2555 with a Type A viscosimeter, or an alternative method complying with 5.1. 5.4.8 Ash content The ash content of the cold p

47、lastics shall be determined using, either the method described in Annex H, or an alternative method complying with 5.1. 5.5 Preformed road markings The identification methods for preformed road markings are laid down in EN 1790. 5.6 Premix glass beads 5.6.1 Granulometry The granulometry of the glass

48、 beads shall be determined using the method laid down in EN 1424. 5.6.2 Refractive index The refractive index class of the glass beads shall be determined using the method laid down in EN 1424. 5.6.3 Resistance to water, hydrochloric acid, calcium chloride and sodium sulphide The glass beads shall n

49、ot develop any surface haze or dulling when in contact with any of the following: water, hydrochloric acid, calcium chloride and sodium sulphide, using the method laid down in EN 1423. BS EN 12802:2011EN 12802:2011 (E) 8 5.6.4 Defective beads The percentage of defective glass beads shall be determined using the method laid down in EN 1424. 5.6.5 Surface Treatment The surface treatment of the glass beads shall be determined using the method laid down in EN 1424. 5.7