EN 15158-2006 en Advanced technical ceramics - Mechanical properties of ceramic composites at high temperature under inert atmosphere - Determination of fatigue properties at const.pdf

1、BRITISH STANDARDBS EN 15158:2006Advanced technical ceramics Mechanical properties of ceramic composites at high temperature under inert atmosphere Determination of fatigue properties at constant amplitudeThe European Standard EN 15158:2006 has the status of a British StandardICS 81.060.30g49g50g3g38

2、g50g51g60g44g49g42g3g58g44g55g43g50g56g55g3g37g54g44g3g51g40g53g48g44g54g54g44g50g49g3g40g59g38g40g51g55g3g36g54g3g51g40g53g48g44g55g55g40g39g3g37g60g3g38g50g51g60g53g44g42g43g55g3g47g36g58BS EN 15158:2006This British Standard was published under the authority of the Standards Policy and Strategy Co

3、mmittee on 29 September 2006 BSI 2006ISBN 0 580 49054 8 National forewordThis British Standard was published by BSI. It is the UK implementation of EN 15158:2006.The UK participation in its preparation was entrusted to Technical Committee RPI/13, Advanced technical ceramics. A list of organizations

4、represented on RPI/13 can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunity from legal obligations.Amendments iss

5、ued since publicationAmd. No. Date CommentsEUROPEAN STANDARDNORME EUROPENNEEUROPISCHE NORMEN 15158August 2006ICS 81.060.30English VersionAdvanced technical ceramics - Mechanical properties of ceramiccomposites at high temperature under inert atmosphere -Determination of fatigue properties at constan

6、t amplitudeCramiques techniques avances - Proprits mcaniquesdes cramiques composites haute temprature sousatmosphre inerte - Dtermination des proprits defatigue amplitude constanteHochleistungskeramik - Mechanische Eigenschaften vonkeramischen Verbundwerkstoffen bei hoher Temperatur ininerter Atmosp

7、hre - Bestimmung derDauerschwingeigenschaften bei Belastung mit konstanterAmplitudeThis European Standard was approved by CEN on 14 July 2006.CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this EuropeanStandard the status of a nati

8、onal standard without any alteration. Up-to-date lists and bibliographical references concerning such nationalstandards may be obtained on application to the Central Secretariat or to any CEN member.This European Standard exists in three official versions (English, French, German). A version in any

9、other language made by translationunder the responsibility of a CEN member into its own language and notified to the Central Secretariat has the same status as the officialversions.CEN members are the national standards bodies of Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, F

10、rance,Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.EUROPEAN COMMITTEE FOR STANDARDIZATIONCOMIT EUROPEN DE NORMALISATIONEUROPISCHES KOMITEE FR N

11、ORMUNGManagement Centre: rue de Stassart, 36 B-1050 Brussels 2006 CEN All rights of exploitation in any form and by any means reservedworldwide for CEN national Members.Ref. No. EN 15158:2006: EEN 15158:2006 (E) 2 Contents Page Foreword3 1 Scope 4 2 Normative references 4 3 Terms, definitions and sy

12、mbols.5 4 Principle8 5 Significance and use .8 6 Apparatus .9 6.1 Fatigue test machine .9 6.2 Load train9 6.3 Test chamber10 6.4 Set-up for heating 10 6.5 Extensometer .10 6.6 Temperature measurement.11 6.7 Data recording system 11 6.8 Micrometers11 7 Test specimens11 8 Test specimen preparation.12

13、8.1 Machining and preparation.12 8.2 Number of test specimens12 9 Test procedure.12 9.1 Test set-up: temperature considerations12 9.2 Measurement of test specimen dimensions .13 9.3 Testing technique 13 9.4 Test validity 14 10 Calculation of results 15 10.1 Time to failure, tf15 10.2 Damage paramete

14、rs 15 10.3 Residual properties .17 11 Test report 17 Annex A (informative) Schematic evolution of E .18 EN 15158:2006 (E) 3 Foreword This document (EN 15158:2006) has been prepared by Technical Committee CEN/TC 184 “Advanced technical ceramics”, the secretariat of which is held by BSI. This European

15、 Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2007, and conflicting national standards shall be withdrawn at the latest by February 2007. According to the CEN/CENELEC Internal Regulations, the natio

16、nal standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Por

17、tugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EN 15158:2006 (E) 4 1 Scope This European Standard specifies the conditions for the determination of constant-amplitude of load or strain in uniaxial tension/tension or in uniaxial tension/compression cyclic fatigue p

18、roperties of ceramic matrix composite materials (CMCs) with fibre reinforcement for temperature up to 2 000 C under vacuum or a gas atmosphere which is inert to the material under test. NOTE Test environments are specified which are intended to prevent the material under test from chemically reactin

19、g with them. This European Standard applies to all ceramic matrix composites with fibre reinforcement, unidirectional (1D), bi-directional (2D), and tri-directional (xD, where 2 150 0,5 l, calibrated length 30 to 80 0,5 h, thickness 2 0,2 b1, width in the calibrated length 8 to 20 0,2 b2, width B2=

20、b1with = 1,2 to 2 0,2 r, radius 30 2 Parallelism of machined parts 0,05 - 8 Test specimen preparation 8.1 Machining and preparation During cutting out, care shall be taken to align the test specimen axis with the desired fibre related loading axis. Machining parameters which avoid damage to the mate

21、rial shall be established and documented. These parameters shall be adhered to during test specimen preparation. 8.2 Number of test specimens At least three valid test results, as specified in 9.4 are required for any condition. 9 Test procedure 9.1 Test set-up: temperature considerations 9.1.1 Gene

22、ral The following determinations shall be carried out under conditions representative of the tests, and shall be repeated every time there is a change in material, in specimen geometry, in gripping configuration etc. In establishing them, time shall be allowed for temperature stabilization. 9.1.2 Co

23、ntrolled temperature zone Prior to testing, the temperature gradient within the calibrated length inside the furnace shall be established over the temperature range of interest. This shall be done by measuring the specimen temperature at a minimum of three locations, which shall be the two extensome

24、ter reference points and a point midway between the two. To establish the length of the controlled temperature zone, it is necessary to measure the temperature also outside the gauge length. The temperature variation within the controlled temperature zone and the gauge length shall meet the requirem

25、ents of Clause 7 and 6.4, respectively. EN 15158:2006 (E) 13 Temperatures may be measured by any means conforming to 6.6. If thermocouples are used to measure the temperature at different locations of the specimen, they shall be embedded (and sealed if necessary) into the specimen to a depth approxi

26、mately equal to half the specimen dimension in the direction of insertion. 9.1.3 Temperature calibration During a series of tests, the test temperature can be determined either directly by measurement on the specimen itself, or indirectly from the temperature indicated by the temperature control dev

27、ice. In the latter case, the relationship between the control temperature and test specimen temperature at the centre of the gauge length shall be established beforehand on a dummy test specimen over the range of temperature of interest. NOTE The relationship between the temperature indicated by the

28、 temperature control system and the test temperature is usually established simultaneously with the controlled temperature zone. 9.2 Measurement of test specimen dimensions The cross-section area shall be determined at the centre of the specimen and at each end of the gauge length. The cross-section

29、 area varies with temperature and the variation is very difficult to measure. For this reason, the cross-section area shall be measured at room temperature. Dimensions shall be measured to an accuracy of 0,01 mm. The arithmetic means of the measurements shall be used for calculations. 9.3 Testing te

30、chnique 9.3.1 Specimen mounting Install the test specimen in the gripping system with its longitudinal axis coinciding with that of the test machine. Care shall be taken not to induce flexural or torsional loads in the test specimen. 9.3.2 Setting the extensometer In the case where a contacting exte

31、nsometer is positioned at ambient temperature, the extensometer output shall be adjusted to read zero after the stabilization period at the test temperature. NOTE In the case where the material has a high thermal expansion coefficient, it is recommended to mechanically pre-set the extensometer takin

32、g expansion into account in order to be close to zero when at test temperature. 9.3.3 Establishing the inert atmosphere When testing under inert gas, any air or water vapour shall be removed before setting the inert atmosphere. This can be done by establishing vacuum (below 10 MPa) in the enclosure,

33、 or by circulating inert gas. When testing under vacuum, the vacuum level shall be in accordance with 6.3. 9.3.4 Heating the test specimen Raise the test specimen temperature to the required test temperature, and maintain this temperature for a period to allow for temperature stabilization and if ap

34、plicable, for stabilization of the extensometer readout. Two procedures are possible: if test specimen temperature is measured during the test on the specimen itself, this temperature shall be used to control the furnace. If it is not possible to measure directly the test specimen temperature during

35、 the test, then it is necessary to use the relation between test specimen temperature and EN 15158:2006 (E) 14 furnace temperature which has been established in 9.1. Ensure that the test specimen stays in the initial state of stress during heating. 9.3.5 Measurements zero the load cell; zero the ext

36、ensometer, if applicable; set the maximum number of cycles, N; for method A, set the maximum and minimum stress values; for method B, set the maximum and minimum strain values; set the frequency and the wave shape; start the fatigue test: for method A, in load control mode; for method B, in strain c

37、ontrol mode; record the number of cycles N or Nf; if an extensometer is used, record the stress-strain loops up to the total number of cycles. NOTE A specific computer program is recommended to control the test. Depending on the computerized facilities used, all the loops can be recorded. If this is

38、 not possible, the following sequence can be used to record stress versus strain: every cycle for the first 10 cycles; one cycle every 10 cycles between 10 and 100 cycles; one cycle every 100 cycles between 100 and 1 000 cycles; one cycle every 1 000 cycles between 1 000 and 10 000 cycles; etc. 9.4

39、Test validity The following circumstances shall invalidate a test for the determination of the lifetime duration: failure to specify and record test conditions; specimen slippage in the grips; rupture in an area outside of the controlled temperature zone. In addition, the following circumstances sha

40、ll invalidate a test for the determination of the damage parameter: extensometer slippage; extensometer drift. EN 15158:2006 (E) 15 10 Calculation of results 10.1 Time to failure, tfCalculate the time to failure in accordance with the following equation: tf(hours) = Nf/ (f x 3 600) where Nfis the nu

41、mber of cycles required to obtain failure of the test specimen; f is the frequency, in hertz (Hz). 10.2 Damage parameters Calculate the damage parameter Dnfor each recorded cycle, n, in accordance with the following equation: app1,appn,nEED =1 where Dnis the damage parameter at the nthfatigue cycle;

42、 En,appis the secant modulus of the nthfatigue loop (see Figure 4); E1,appis the secant modulus of the first fatigue loop (see Figure 4); Enappis equal to: (max)/(max nresidual) (see Figure 4). nresidual is equal to: (unl+l)/2 (see Figure 4 b). EN 15158:2006 (E) 16 a) R = 0 b) R 0 Key 1 strain () 2

43、stress () 3 cycle 1 4 cycle n lloading unlunloading Figure 4 Fatigue stress-strain curves with a) R = 0, b) R 0 EN 15158:2006 (E) 17 The damage parameters, Dn, max,residcan be plotted versus the number of cycles, N. For N, a log scale is almost always used, although a linear scale may also be used.

44、Figures 4a) to 4c) represent three cases of cyclic fatigue of CMCs. NOTE Annex A shows the schematic evolution of E under different circumstances of damage and creep. 10.3 Residual properties When rupture does not occur before the end of the test, test specimen shall be tested to rupture in accordan

45、ce with EN 1892, EN 1893 or EN 658-1. 11 Test report The test report shall contain the following information: a) name and address of the testing establishment; b) date of the test, unique identification of report and of each page, customers name, address and signature; c) a reference to this Europea

46、n Standard, i.e. EN 15158; d) test specimen drawing or reference; e) description of the test material (material type, manufacturing code, batch number); f) description of the test set up : extensometer, gripping system, load cell; g) frequency in hertz; h) wave form; i) maximum and minimum stress (m

47、ethod A); j) maximum and minimum strain (method B); k) number of cycles to failure; if test is stopped at a specified number of cycles without failure occurring it shall be so registered; l) residual properties (if applicable); m) number of tests carried out and number of valid results obtained; n)

48、damage parameter, if applicable; o) failure location of all the specimens used for obtaining the above results, if applicable. EN 15158:2006 (E) 18 Annex A (informative) Schematic evolution of E Figure A.1 shows a schematic evolution of E where there is a) no damage, b) creep but no fatigue damage a

49、nd c) fatigue damage and eventual creep. a) No damage b) No fatigue damage only creep c) Fatigue damage plus eventual creep Key 1 first cycle 2 last cycle Figure A.1 Schematic evolution of E with a) no damage, b) creep but no fatigue damage and c) fatigue damage and eventual creep blankBS EN 15158:2006BSI389 Chiswick High RoadLondonW4 4ALBSI British Standards InstitutionBSI is the independent national body responsible for preparing British Standards. It presents the UK view on st