EN 15267-4-2017 en Air quality - Certification of automated measuring systems - Part 4 Performance criteria and test procedures for automated measuring systems for periodic measure.pdf

1、BS EN 15267-4:2017Air quality Certification of automated measuring systemsPart 4: Performance criteria and test procedures for automated measuring systems for periodic measurements of emissions from stationary sourcesBSI Standards PublicationWB11885_BSI_StandardCovs_2013_AW.indd 1 15/05/2013 15:06BS

2、 EN 15267-4:2017 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN 15267-4:2017. The UK participation in its preparation was entrusted to TechnicalCommittee EH/2/1, Stationary source emission.A list of organizations represented on this committee can be obtained on

3、 request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2017.Published by BSI Standards Limited 2017ISBN 978 0 580 89191 5 ICS 13.040.99 Compliance with a B

4、ritish Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of the Standards Policy and Strategy Committee on 31 January 2017.Amendments/corrigenda issued since publicationDate T e x t a f f e c t e dBS EN 15267-4:2017EUROPEAN STANDARD NORME

5、EUROPENNE EUROPISCHE NORM EN 15267-4 January 2017 ICS 13.040.99 English Version Air quality - Certification of automated measuring systems - Part 4: Performance criteria and test procedures for automated measuring systems for periodic measurements of emissions from stationary sources Qualit de lair

6、- Certification des systmes de mesurage automatiss - Partie 4 : Spcifications de performance et modes opratoires dessai des systmes de mesurage automatiss pour le mesurage priodique des missions de sources fixes Luftbeschaffenheit - Zertifizierung von automatischen Messeinrichtungen - Teil 4: Mindes

7、tanforderungen und Prfprozeduren fr automatische Messeinrichtungen fr wiederkehrende Messungen von Emissionen aus stationren Quellen This European Standard was approved by CEN on 26 September 2016. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditio

8、ns for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in

9、 three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standard

10、s bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia

11、, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2017 CEN All rights of exploitation in any form and by any means re

12、served worldwide for CEN national Members. Ref. No. EN 15267-4:2017 EBS EN 15267-4:2017EN 15267-4:2017 (E) 2 Contents Page European foreword . 5 0 Introduction 6 0.1 General 6 0.2 Legal drivers . 6 0.3 Periodic measurements 6 0.4 Relationship to EN 14181 . 6 0.5 Processes 7 0.6 Performance character

13、istics . 7 0.7 Relationship to EN 15267-3 . 8 1 Scope 9 2 Normative references 9 3 Terms and definitions . 9 4 Symbols and abbreviations 15 4.1 Symbols 15 4.2 Abbreviations 17 5 General requirements 17 5.1 Application of performance criteria . 17 5.2 Ranges to be tested 17 5.2.1 Certification range

14、. 17 5.2.2 Supplementary ranges . 18 5.2.3 Lower limit of ranges 18 5.2.4 Expression of performance criteria with respect to ranges . 18 5.2.5 Ranges of optical insitu P-AMS with variable optical length 18 5.3 Performance testing of P-AMS based on certified AMS previously tested according to EN 1526

15、7-3 . 18 5.4 Equivalence with the SRM . 18 5.5 Manufacturing consistency and changes to P-AMS design 19 5.6 Qualifications of test laboratories . 19 6 Performance criteria common to all P-AMS for laboratory testing . 19 6.1 P-AMS for testing 19 6.2 CE labelling . 19 6.3 Output ranges and zero-point

16、. 19 6.4 Display of operational status signals 20 6.5 Degrees of protection provided by enclosures . 20 6.6 Response time . 20 6.7 Repeatability standard deviation at zero point 20 6.8 Repeatability standard deviation at span point . 20 6.9 Lack of fit . 20 6.10 Short-term zero and span drift . 20 6

17、.11 Set-up time after transport and influence of ambient temperature . 20 6.12 Influence of voltage variations 21 6.13 Influence of vibration . 21 BS EN 15267-4:2017EN 15267-4:2017 (E) 3 6.14 Influence of sample gas flow for extractive P-AMS . 21 6.15 Influence of sample gas pressure 21 6.16 Cross-s

18、ensitivity 21 6.17 Converter efficiency for P-AMS measuring NOx. 21 6.18 Response factors for TOC measuring P-AMS. 21 6.19 Influences on P-AMS with in-stack sampling chamber . 22 6.20 Influences related to storage and transportation . 22 7 Performance criteria common to all P-AMS for field testing 2

19、2 7.1 Response time 22 7.2 Short-term zero and span drift 23 7.3 Reproducibility 23 8 Performance criteria specific to measured components . 23 8.1 General . 23 8.2 Gas monitoring P-AMS 23 8.2.1 Performance criteria . 23 8.2.2 P-AMS for total organic carbon 25 8.3 Particulate matter monitoring P-AMS

20、 . 26 9 General test requirements 27 10 Test procedures for laboratory tests . 28 10.1 P-AMS for testing . 28 10.2 CE labelling 28 10.3 Output ranges and zero point 28 10.4 Display of operational status signals . 29 10.5 Degrees of protection provided by enclosures 29 10.6 Response time 29 10.7 Repe

21、atability standard deviation at zero point . 31 10.8 Repeatability standard deviation at span point 31 10.9 Lack of fit 32 10.10 Short-term zero and span drift 33 10.11 Set-up time after transportation and influence of ambient temperature 33 10.12 Influence of voltage variations 34 10.13 Influence o

22、f vibration 35 10.14 Influence of sample gas pressure 36 10.15 Influence of the sample gas flow for extractive P-AMS . 36 10.16 Cross-sensitivity 37 10.17 Converter efficiency for P-AMS measuring NOx. 38 10.18 Response factors . 39 10.19 Influences on P-AMS with in-stack sampling chamber . 40 10.20

23、Influences related to storage and transportation . 40 11 Requirements for the field test 41 12 Test procedures common to all P-AMS for field tests 41 12.1 Response time 41 12.2 Short-term zero and span drift 41 12.3 Reproducibility 42 13 Equivalence with the SRM . 43 14 Measurement uncertainty . 43

24、15 Test report 43 Annex A (normative) Minimum requirements for a test bench 44 BS EN 15267-4:2017EN 15267-4:2017 (E) 4 Annex B (normative) Interferents . 45 Annex C (normative) Test of linearity . 46 C.1 Description of the test procedure 46 C.2 Establishment of the regression line 46 C.3 Calculation

25、 of the residuals of the average concentrations 47 Annex D (normative) Determination of the total uncertainty 48 D.1 Determination of uncertainty contributions . 48 D.2 Elements required for the uncertainty determinations 48 D.3 Example of an uncertainty calculation for a CO measuring P-AMS 50 D.4 D

26、etermination of uncertainty contributions by use of sensitivity coefficients . 52 Annex E (informative) Elements of performance testing report . 53 Annex F (informative) European standard reference methods . 56 Bibliography . 57 BS EN 15267-4:2017EN 15267-4:2017 (E) 5 European foreword This document

27、 (EN 15267-4:2017) has been prepared by Technical Committee CEN/TC 264 “Air quality”, the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by July 2017, and confli

28、cting national standards shall be withdrawn at the latest by July 2017. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document

29、is Part 4 of a series of European Standards: EN 15267-1, Air quality Certification of automated measuring systems Part 1: General principles EN 15267-2, Air quality Certification of automated measuring systems Part 2: Initial assessment of the AMS manufacturers quality management system and post cer

30、tification surveillance for the manufacturing process EN 15267-3, Air quality Certification of automated measuring systems Part 3: Performance criteria and test procedures for automated measuring systems for monitoring emissions from stationary sources EN 15267-4, Air quality Certification of automa

31、ted measuring systems Part 4: Performance criteria and test procedures for automated measuring systems for periodic measurements of emissions from stationary sources According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implem

32、ent this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania,

33、Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. BS EN 15267-4:2017EN 15267-4:2017 (E) 6 0 Introduction 0.1 General CEN has established standards for the certification of automated measuring systems (AMS) used for monitoring emissions from stationary sources and

34、 ambient air quality. This product certification is based on the following four sequential stages: a) performance testing of the AMS; b) initial assessment of the AMS manufacturers quality management system; c) certification of the AMS; d) post certification surveillance. This European Standard spec

35、ifies the performance criteria and test procedures for performance testing of portable automated measuring systems (P-AMS) used for periodic measurements of stationary source emissions. Testing applies to complete measuring systems. NOTE 1 Portable electrical apparatus designed to measure combustion

36、 flue gas parameters of heating appliances are specified in EN 503791 to EN 503793. The application of P-AMS for periodic measurements of stationary source emissions is based on specification of the standard reference method (SRM) and validation of the SRM; specification of the alternative method (A

37、M) if the P-AMS is based on an AM; certification of the P-AMS in accordance with EN 15267-1, EN 15267-2 and EN 15267-4 including demonstration of equivalence with the SRM in the field if the P-AMS is based on an AM; on-going quality management by the user of the P-AMS in line with EN ISO/IEC 17025.

38、NOTE 2 Examples for standard reference methods for different measured components are listed in Annex F. The overall assessment for the purposes of certification is conformity testing, while the evaluation of performance against specified performance criteria is performance testing. 0.2 Legal drivers

39、 This European Standard supports the requirements of the following EU Directives: Directive 2010/75/EU on industrial emissions (integrated pollution prevention and control) Directive 2003/87/EC on processes emitting greenhouse gases. However, this European Standard can also be applied to the monitor

40、ing requirements specified in other EU Directives. 0.3 Periodic measurements Certified P-AMS can be used as SRM or AM for periodic measurements of stationary source emissions. 0.4 Relationship to EN 14181 Certified P-AMS can be used as SRM or AM for the calibration and validation of stationary AMS f

41、or QAL2 and AST purposes. BS EN 15267-4:2017EN 15267-4:2017 (E) 7 0.5 Processes Field testing of P-AMS is ordinarily carried out on industrial processes representative of the range of application of the SRM or AM. The premise is that if the P-AMS performs acceptably on these processes, then experien

42、ce has shown that the P-AMS generally performs well on the majority of other processes. However, there are always exceptions and it is the responsibility of the user to ensure that the P-AMS performs adequately on a specific process. The necessary field test of P-AMS is specified in this European St

43、andard. 0.6 Performance characteristics A combination of laboratory and field tests is detailed within this European Standard. Laboratory testing is designed to assess whether a P-AMS can meet, under controlled conditions, the relevant performance criteria. Field testing, is designed to assess wheth

44、er a P-AMS can continue to work and meet the relevant performance criteria in real applications including transportation to the measurement site, set-up of the P-AMS and measurement. The main P-AMS performance characteristics are: response time; repeatability standard deviation; lack of fit (lineari

45、ty); short-term drift; influence of ambient temperature; influence of voltage variations; influence of vibration; influence of sample gas pressure; influence of sample gas flow for extractive P-AMS; cross-sensitivity to likely interferents contained in the stack gas other than the measured component

46、; converter efficiency for NOxP-AMS; response factors for P-AMS measuring TOC; reproducibility under field conditions; trueness and precision of the P-AMS against the SRM under field conditions if the P-AMS is based on an AM. Additional performance characteristics specific to the SRM or AM are inclu

47、ded in the performance test. The quality assurance and quality control (QA/QC) procedures to be applied by the user of the P-AMS are also assessed in the performance test. BS EN 15267-4:2017EN 15267-4:2017 (E) 8 This European Standard is an application and elaboration of EN ISO 9169 with additional

48、and alternative provisions for the performance test of P-AMS. Where this European Standard appears to differ from EN ISO 9169, it either elaborates upon the requirements of EN ISO 9169 or differs in minor ways owing to the necessity to conduct the performance test of P-AMS. 0.7 Relationship to EN 15

49、267-3 This European Standard is based on EN 15267-3, which specifies the performance testing of stationary AMS for the continuous monitoring of emissions from stationary sources. Many requirements of this European Standard are identical to those of EN 15267-3. This European Standard deviates from EN 15267-3 only where the portable use and the use as SRM or AM require different or additional requirements. Therefore, this European Standard allows a combined testing where an AMS is designed for stati