EN 15860-2010 en Plastics - Thermoplastic semi-finished products for machining - Requirements and test methods《塑料 热塑性半成品加工 要求和试验方法》.pdf

1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS EN 15860:2010Plastics Thermoplasticsemi-finished products formachining Requirementsand test methodsBS EN 15860:2010 BRITISH STANDARDNational forewordThis British Standard is t

2、he UK implementation of EN 15860:2010.The UK participation in its preparation was entrusted to TechnicalCommittee PRI/82, Thermoplastic materials.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the nece

3、ssaryprovisions of a contract. Users are responsible for its correctapplication. BSI 2010ISBN 978 0 580 63638 7ICS 83.080.20Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and Strategy Comm

4、ittee on 31 July 2010Amendments issued since publicationDate Text affectedBS EN 15860:2010EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 15860 June 2010 ICS 83.080.20 English Version Plastics - Thermoplastic semi-finished products for machining - Requirements and test methods Plastiques - Prod

5、uits semi-finis thermoplastiques pour usinage - Exigences et mthodes dessai Kunststoffe - Thermoplastische Halbzeuge fr die spanende Verarbeitung - Anforderungen und PrfmethodenThis European Standard was approved by CEN on 19 May 2010. CEN members are bound to comply with the CEN/CENELEC Internal Re

6、gulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member. Th

7、is European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions. CEN members are

8、 the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden

9、, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Re

10、f. No. EN 15860:2010: EBS EN 15860:2010EN 15860:2010 (E) 2 Contents Page Foreword .4 1 Scope 5 2 Normative references5 3 Terms and definitions .6 4 Materials .6 5 Requirements.8 5.1 As-delivered condition8 5.2 Surface appearance.8 5.3 Dimensions and tolerances for rods .8 5.3.1 Diameter .8 5.3.2 Len

11、gth.10 5.3.3 Roundness .10 5.3.4 Straightness .11 5.4 Dimensions and tolerances for hollow bars.12 5.4.1 Diameters .12 5.4.2 Length.14 5.4.3 Roundness .14 5.4.4 Straightness .14 5.4.5 Concentricity15 5.5 Dimensions and tolerances for panels/plates 16 5.5.1 Thickness .16 5.5.2 Length and width.17 5.5

12、.3 Straightness .17 5.6 Properties .20 5.6.1 Physical properties20 5.6.2 Dimensional stability after heat treatment24 5.6.3 Physiological behaviour .26 6 Test methods .26 6.1 Test conditions 26 6.2 Sampling size.26 6.3 Test specimen preparation.26 6.3.1 Mechanical properties.26 6.3.2 Density28 6.3.3

13、 Melt volume-flow rate, viscosity number, melting temperature/glass transition temperature 28 6.3.4 Dimensional stability after heat treatment28 6.4 As-delivered condition29 6.5 Surface appearance.29 6.6 Accuracy of the dimension measuring instruments29 6.7 Density29 6.8 Tensile stress at yield and

14、elongation at break29 6.9 Tensile modulus of elasticity .30 6.10 Vicat softening temperature .30 6.11 Melt volume-flow rate (MVR) 30 6.12 Melting temperature/glass transition temperature.31 6.13 Viscosity number.31 6.14 Dimensional stability after heat treatment31 6.15 Preparation of test results 35

15、 BS EN 15860:2010EN 15860:2010 (E) 3 7 Designation 35 7.1 Rods35 7.2 Hollow bars 35 7.3 Panels/plates36 8 Marking.36 Annex A (normative) Procedure for the determination of microporosity in semi-finished products .37 Annex B (normative) Tables for the conversion of deflection values (straightness)41

16、Annex C (informative) Examples of calculation of dimensional stability after heat treatment.44 C.1 Rods44 C.2 Hollow bars 44 C.3 Panels/plates45 Bibliography46 BS EN 15860:2010EN 15860:2010 (E) 4 Foreword This document (EN 15860:2010) has been prepared by Technical Committee CEN/TC 249 “Plastics”, t

17、he secretariat of which is held by NBN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by December 2010, and conflicting national standards shall be withdrawn at the latest by December 2010. Attenti

18、on is drawn to the possibility that some of the elements of this document may be the subject of patent rights other than those identified above. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. According to the CEN/CENELEC Internal Regulations, the nati

19、onal standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands,

20、 Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. BS EN 15860:2010EN 15860:2010 (E) 5 1 Scope This European Standard specifies the requirements and associated test methods that apply to semi-finished products such as rods, hollow bars and plat

21、es made from thermoplastic materials. These semi-finished products are used predominantly for the manufacture of finished parts by means of machining. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edit

22、ion cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN ISO 291:2008, Plastics Standard atmospheres for conditioning and testing (ISO 291:2008) EN ISO 306, Plastics Thermoplastic materials Determination of Vicat softening temper

23、ature (VST) (ISO 306:2004) EN ISO 307, Plastics Polyamides Determination of viscosity number (ISO 307:2007) EN ISO 527-1, Plastics Determination of tensile properties Part 1: General principles (ISO 527-1:1993 including Corr. 1:1994) EN ISO 527-2:1996, Plastics Determination of tensile properties Pa

24、rt 2: Test conditions for moulding and extrusion plastics (ISO 527-2:1993 including Corr.1:1994) EN ISO 1043-1:2001, Plastics Symbols and abbreviated terms Part 1: Basic polymers and their special characteristics (ISO 1043-1:2001) EN ISO 1133, Plastics Determination of the melt mass-flow rate (MFR)

25、and the melt volume-flow rate (MVR) of thermoplastics (ISO 1133:2005) EN ISO 1183-1, Plastics Methods for determining the density of non-cellular plastics Part 1: Immersion method, liquid pyknometer method and titration method (ISO 1183-1: 2004) EN ISO 1183-2, Plastics Methods for determining the de

26、nsity of non-cellular plastics Part 2: Density gradient column method (ISO 1183-2:2004) EN ISO 2818, Plastics Preparation of test specimens by machining (ISO 2818:1994) EN ISO 10350-1, Plastics Acquisition and presentation of comparable single-point data Part 1: Moulding materials (ISO 10350-1:2007)

27、 EN ISO 11357-1, Plastics Differential scanning calorimetry (DSC) Part 1: General principles (ISO 11357-1:2009) ISO 1628-5, Plastics Determination of the viscosity of polymers in dilute solution using capillary viscometers Part 5: Thermoplastic polyester (TP) homopolymers and copolymers ISO 11357-2,

28、 Plastics Differential scanning calorimetry (DSC) Part 2: Determination of glass transition temperature ISO 11357-3, Plastics Differential scanning calorimetry (DSC) Part 3: Determination of temperature and enthalpy of melting and crystallization ISO 15527:2007, Plastics Compression-moulded sheets o

29、f polyethylene (PE-UHMW, PE-HD) Requirements and test methods BS EN 15860:2010EN 15860:2010 (E) 6 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. 3.1 semi-finished products rods, hollow bars and panels/plates from which finished parts are manufac

30、tured by means of machining 3.2 rods long, straight and solid products manufactured by means of extrusion, casting or compression moulding and having a uniform circular cross-section over their entire length 3.3 hollow bars long, straight and hollow products manufactured by means of extrusion, casti

31、ng or compression moulding and having a uniform circular cross-section, with concentric inside and outside diameter, over their entire length 3.4 panels plates flat, rectangular, solid products manufactured by means of extrusion, extrusion, calendering, casting or compression moulding and having a t

32、hickness of at least 0,2 mm which is uniform over their full cross- section 4 Materials The semi-finished products shall be made of thermoplastic materials (see Table 1). These materials may contain additives such as processing aids, reinforcing agents, fillers, stabilizers or colorants, in which ca

33、se, they are further referred to in this standard as “modified materials“. The nature and the quantity of these additives can influence the mechanical, thermal and electrical properties of the semi-finished products. The choice and the quantities of additives used are left to the discretion of the m

34、anufacturer of the semi-finished products. BS EN 15860:2010EN 15860:2010 (E) 7 Table 1 List of the thermoplastic materials most commonly used for the manufacture of semi-finished products Abbreviated terms (according to EN ISO 1043-1:2001) Materials ABS Acrylonitrile-butadiene-styrene ECTFE Ethylene

35、-chlorotrifluoroethylene copolymer PA 6 Polyamide 6 PA 6 Ca Polyamide 6, cast PA 66 Polyamide 66 PA 12 Polyamide 12 PA 12 Ca Polyamide 12, cast PA 46 Polyamide 46 PA 6/12 Cab Polyamide 6/12, cast PBT Polybutylene terephthalate PC Polycarbonate PEEK Polyetheretherketone PE-HD Polyethylene, high densi

36、ty (Group 2.1 or 3.1 of ISO 15527:2007) PE-LD Polyethylene, low density PE-UHMW Polyethylene, ultra high molecular weight (Group 1.1 or 1.2 of ISO 15527:2007) PEI Polyetherimide PESU Polyethersulfone PET Polyethylene terephthalate POM-C Polyoxymethylene, copolymer POM-H Polyoxymethylene, homopolymer

37、 PP-B Polypropylene, block copolymer PP-H Polypropylene, homopolymer PP-R Polypropylene, random copolymer PPE+PS Polystyrene modified polyphenylene ether PPS Polyphenylene sulfide PPSU Polyphenylene sulfone PSU Polysulfone PVC-C Polyvinyl chloride, chlorinated PVC-HI Polyvinyl chloride, high-impact

38、modified PVC-U Polyvinyl chloride, unplasticized PVDF Polyvinylidene fluoride a “C“ means “cast “ b PA 6/12 with max. 15 % laurinlactam BS EN 15860:2010EN 15860:2010 (E) 8 5 Requirements 5.1 As-delivered condition Semi-finished products shall be free of blisters, voids, cracks, foreign matter and ot

39、her defects which make the product unfit for the intended use. Specific requirements in this respect shall be agreed upon between supplier and customer. The semi-finished products shall be manufactured in such a way that their internal stress level is minimal (see 5.6.2). Natural coloured materials:

40、 slight variations in hue originating from raw materials and/or manufacturing process are allowed. Natural colour means that no additives (colorants) are added to the raw materials during their manufacture and processing into semi-finished products for the purpose of obtaining another colour. Colora

41、tion: this shall be uniform and shall be agreed upon between supplier and customer. Slight variations in hue originating from raw materials and/or manufacturing process are allowed. The testing of the as-delivered condition shall be performed according to 6.4. NOTE Semi-finished products made from P

42、A are dry after manufacture, but absorb moisture during storage. The moisture content in the as-delivered condition is a function of the type of moulding material, the cross-section (plate thickness, rod diameter or hollow bar wall thickness) of the semi-finished product concerned, as well as the ty

43、pe and period of storage. Semi-finished products made from POM, PEEK and PP are permitted to have light patches in the centre of the cross-section. Microporosity in the centre of the cross-section may occur in semi-finished products made from POM-H and PP. The largest diameter or the widest part of

44、the microporosity line(s) shall, however, not exceed 4 %. The procedure for the determination and measurement of microporosity is described in Annex A. When semi-finished products made from POM and PP are subject to specific requirements, e. g. pressure tightness and/or dielectric strength, they sha

45、ll be agreed upon between supplier and customer. 5.2 Surface appearance Semi-finished products shall essentially have smooth surfaces. Shallow marks, grooves and irregularities resulting from the manufacturing process are allowed provided that the product meets the dimensional requirements according

46、 to 5.3, 5.4 and 5.5. Testing of the surface appearance shall be performed according to 6.5. Specific requirements with respect to the surface appearance are to be agreed upon between supplier and customer. 5.3 Dimensions and tolerances for rods 5.3.1 Diameter The diameters commonly available are gi

47、ven in the delivery programmes of the suppliers. The tolerances on the diameters are given in Table 2 for different diameter ranges. BS EN 15860:2010EN 15860:2010 (E) 9 Table 2 Tolerances on diameters for rods Dimensions in millimetres Column 1 Column 2 Column 3 Column 4 Column 5 Diameter ranges ECT

48、FE PEEK PA 6 PET PA 66 POM PA 12 PPS PA 46 PVDF PBT PA 6 C PA 6/12 C PA 12 C ABS PC PEI PESU PPE+PS PPSU PSU PE-LD PE-HD PE-UHMW PP-B PP-H PP-R PVC-C PVC-HI PVC-U up to 4 + 0,3 + 0,1 over 4 up to 6 + 0,6 + 0,1 + 0,7 + 0,1 + 0,4 + 0,1 over 6 up to 8 + 0,5 + 0,1 over 8 up to 10 + 0,7 + 0,1 + 0,8 + 0,1

49、 + 0,6 + 0,1 over 10 up to 12 + 0,7 + 0,2 over 12 up to 16 + 0,8 + 0,2 over 16 up to 18 + 0,9 + 0,2 over 18 up to 20 + 0,8 + 0,2 + 0,9 + 0,2 over 20 up to 25 over 25 up to 30 + 1,0 + 0,2 + 1,2 + 0,2 + 1,2 + 0,2 over 30 up to 32 + 1,2 + 0,2 over 32 up to 36 + 1,3 + 0,2 over 36 up to 40 + 1,2 + 0,2 + 1,4 + 0,2 + 1,6 + 0,2 + 1,5 + 0,2 over 40 up to 45 over 45 up to 56 + 1,3 + 0,3 + 1,9 + 0,3 + 2 + 0,3 + 2 + 0,3 over 56 up to 63 + 2,3 + 0,3 over 63 up to 70 + 1,6 + 0,3 + 2,5 + 0,3 + 2,5 + 0,3 +