1、BSI Standards PublicationBS EN 16457:2014Characterization of waste Framework for the preparationand application of a testingprogramme Objectives,planning and reportBS EN 16457:2014 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN 16457:2014.The UK participation i
2、n its preparation was entrusted to TechnicalCommittee B/508/3, Characterization of waste.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for
3、its correctapplication. The British Standards Institution 2014. Published by BSI StandardsLimited 2014ISBN 978 0 580 79083 6ICS 13.030.01Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and
4、Strategy Committee on 31 March 2014.Amendments issued since publicationDate Text affectedBS EN 16457:2014EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN 16457 March 2014 ICS 13.030.01 English Version Characterization of waste - Framework for the preparation and application of a testing programm
5、e - Objectives, planning and report Caractrisation des dchets - Procdure-cadre pour llaboration et la mise en oeuvre dun programme dessai -Objectifs, planification et rapport Charakterisierung von Abfllen - Rahmenbedingungen fr die Vorbereitung und Anwendung eines Untersuchungsprogramms - Ziele, Pla
6、nung und Bericht This European Standard was approved by CEN on 20 December 2013. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and b
7、ibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the res
8、ponsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav R
9、epublic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NO
10、RMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 16457:2014 EBS EN 16457:2014EN 16457:2014 (E) 2 Contents Page Foreword
11、 3 Introduction .4 1 Scope 5 2 Normative references 5 3 Terms and definitions7 4 Defining a waste testing programme .9 4.1 Principles 9 4.2 Structure of a waste testing programme .10 4.3 Parameters to be tested for a waste 12 4.4 Responsibilities and programme manager .13 4.5 Standards to be used 14
12、 5 Carrying out a waste testing programme 15 6 Overall testing report .15 Annex A (normative) Matrix testing steps versus parameters specifying the standards to be used in a waste testing programme .17 Annex B (informative) A-deviations .25 Bibliography 26 BS EN 16457:2014EN 16457:2014 (E) 3 Forewor
13、d This document (EN 16457:2014) has been prepared by Technical Committee CEN/TC 292 “Characterization of waste”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the late
14、st by September 2014 and conflicting national standards shall be withdrawn at the latest by September 2014. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or al
15、l such patent rights. It is to be noted that for Germany an A-deviation applies (see Annex B). This document has been prepared by the ad hoc group “Testing programme” of CEN/TC 292. It has been decided by CEN/TC 292 to prepare the present document and to consider separately other issues supporting t
16、his document. This would finally result in a set of four documents on waste testing as listed in the Introduction. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulga
17、ria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Tur
18、key and the United Kingdom. BS EN 16457:2014EN 16457:2014 (E) 4 Introduction This European Standard was elaborated as a help for those who have to organize and apply a waste testing programme. Often several parameters need to be determined in a waste sample and for each parameter different testing s
19、teps of a different nature need to be coordinated and performed. This is done in accordance with dedicated standards developed by CEN/TC 292 (e.g. standards for the steps of sampling, extraction, leaching and analysis of eluates or extracts). In order to cope with these different parameters to be te
20、sted and with these different testing steps of different nature, the testing of a waste generally refers to different standards which should be used (and elaborated) in a coherent and coordinated way in a testing programme. This European Standard is designed for specifying such overall testing progr
21、ammes. This European Standard may be used by different interested parties in waste testing: plant operators, testing institutes, accreditation bodies, etc. as well as by industries to address the waste testing part of their contracts and by regulators to address the waste testing part of their regul
22、ations. This European Standard can be used to: produce a standardized testing programme for use in regular or routine circumstances (elaboration of daughter/derived standards dedicated to well defined testing scenarios); incorporate the specific testing requirements of European and national legislat
23、ion; design and develop a waste testing programme for use on a case by case basis. This European Standard provides requirements on the programme, objective, plan and report for the execution of a waste testing programme. This is done with the intent to ensure reliable and comparable results when usi
24、ng the reference methods that have been developed by CEN/TC 292 in accordance with the principles specified in this standard and in the supporting documents (listed below). As shown in Figures 2 and 3, for waste testing, the tests to be performed consist (see also the supporting documents listed bel
25、ow) of two main works: the sampling in the field and the analysis-quantification in the laboratory. The needed coordination and interface is the responsibility of the programme manager (see 4.4). It is also the responsibility of the programme manager to design the testing programme, to authorize the
26、 testing report and to submit it to the customer. This European Standard includes one normative annex and one informative annex which are part of this standard. This European Standard is intended to become a part of a set of documents consisting of the present document: EN 16457, Characterization of
27、 waste Framework for the preparation and application of a testing programme Objective, planning and report and of three supporting documents providing important information: CEN/TS (WI 00292082), Characterization of waste Framework for the preparation and application of a testing programme Applicati
28、on of EN ISO/IEC 17025 (in preparation) CEN/TS (WI 00292085), Characterization of waste Framework for the preparation and application of a testing programme Guidelines for the elaboration of standardised testing methods (in preparation) CEN/TR (WI 00292084), Characterization of waste Framework for t
29、he preparation and application of a testing programme General information on content tests and leaching tests (in preparation) BS EN 16457:2014EN 16457:2014 (E) 5 1 Scope This European Standard specifies requirements for a waste testing programme regarding mainly objectives, planning and report with
30、 the intent to ensure reliable and comparable results when using the reference methods that have been developed and/or adopted by CEN/TC 292. The planning and report aspects of this European Standard are applicable to any waste testing programme dedicated to the determination of one or several param
31、eters. They are also applicable to all testing steps for each parameter from sampling up to reporting whether these steps are taking place in the field (e.g. sampling) or in the laboratory (e.g. analysis-quantification). This European Standard does not address aspects of safety for activities in the
32、 field and inside laboratory. NOTE The term planning a testing programme is used here with the general meaning of organizing a testing programme and being in accordance with the terms testing plan, sampling plan, laboratory plan used in the present European Standard. 2 Normative references The follo
33、wing documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.1)EN 12457-1, Cha
34、racterisation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 1: One stage batch test at a liquid to solid ratio of 2 l/kg for materials with high solid content and with particle size below 4 mm (without or with size reduction) EN 12457-2, Characteri
35、sation of waste - Leaching - Compliance test for leaching of granular waste materials and sludges - Part 2: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 4 mm (without or with size reduction) EN 12457-3, Characterisation of waste - Leaching - Compl
36、iance test for leaching of granular waste materials and sludges - Part 3: Two stage batch test at a liquid to solid ratio of 2 l/kg and 8 l/kg for materials with high solid content and with particle size below 4 mm (without or with size reduction) EN 12457-4, Characterisation of waste - Leaching - C
37、ompliance test for leaching of granular waste materials and sludges - Part 4: One stage batch test at a liquid to solid ratio of 10 l/kg for materials with particle size below 10 mm (without or with size reduction) EN 13137, Characterization of waste - Determination of total organic carbon (TOC) in
38、waste, sludges and sediments EN 13656, Characterization of waste - Microwave assisted digestion with hydrofluoric (HF), nitric (HNO3) and hydrochloric (HCl) acid mixture for subsequent determination of elements EN 13657, Characterization of waste - Digestion for subsequent determination of aqua regi
39、a soluble portion of elements EN 14039, Characterization of waste - Determination of hydrocarbon content in the range of C10 to C40 by gas chromatography EN 14345, Characterization of waste - Determination of hydrocarbon content by gravimetry 1) Useful information may be found in several CEN/TRs as
40、mentioned in Annex A. The use of CEN/TRs is not mandatory and other sources of information may be used provided that the requirements of the basic EN or CEN/TS are fulfilled. The list of such CEN/TR is given in the Bibliography, references 5 to 15. BS EN 16457:2014EN 16457:2014 (E) 6 EN 14346, Chara
41、cterization of waste - Calculation of dry matter by determination of dry residue or water content CEN/TS 14405, Characterization of waste - Leaching behaviour tests - Up-flow percolation test (under specified conditions) prEN 14429, Characterisation of waste - Leaching behaviour test - Influence of
42、pH on leaching with initial acid/base addition EN 14582, Characterization of waste - Halogen and sulfur content - Oxygen combustion in closed systems and determination methods EN 14735, Characterization of waste - Preparation of waste samples for ecotoxicity tests EN 14899, Characterization of waste
43、 - Sampling of waste materials - Framework for the preparation and application of a Sampling Plan prEN 14997, Characterisation of waste - Leaching behaviour test - Influence of pH on leaching with continuous pH control EN 15002, Characterization of waste - Preparation of test portions from the labor
44、atory sample EN 15169, Characterization of waste - Determination of loss on ignition in waste, sludge and sediments EN 15192, Characterisation of waste and soil - Determination of Chromium(VI) in solid material by alkaline digestion and ion chromatography with spectrophotometric detection EN 15308,
45、Characterization of waste - Determination of selected polychlorinated biphenyls (PCB) in solid waste by using capillary gas chromatography with electron capture or mass spectrometric detection EN 15309, Characterization of waste and soil - Determination of elemental composition by X-ray fluorescence
46、 EN 15216, Characterization of waste - Determination of total dissolved solids (TDS) in water and eluates CEN/TS 15364, Characterization of waste - Leaching behaviour tests - Acid and base neutralization capacity test EN 15527, Characterization of waste - Determination of polycyclic aromatic hydroca
47、rbons (PAH) in waste using gas chromatography mass spectrometry (GC/MS) CEN/TS 15862, Characterisation of waste - Compliance leaching test - One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions prEN 15863, Characteris
48、ation of waste - Leaching behaviour test for basic characterisation - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions CEN/TS 15864, Characterisation of waste - Leaching behaviour test for basic characterisation - Dynamic monolithic leaching test with continuou
49、s leachant renewal under conditions relevant for specified scenario(s) EN 15875, Characterization of waste - Static test for determination of acid potential and neutralisation potential of sulfidic waste CEN/TS 16023, Characterization of waste - Determination of gross calorific value and calculation of net calorific value EN 16192, Characterization of waste - Analysis of eluates CEN/TS 16229, Characterization of waste - Sampling and analysis of weak acid dissociable cyanide discharged into tailings ponds EN 16377, Characterization of was
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