1、STD*BSI BS EN IS0 LOS-ZOb-ENGL 2000 I Lb24bb7 0705bLb 59L I 1s EN IS0 BRITISH STANDARD Textiles - Tests for colour fastness - Part Z06: Evaluation of dye and pigment migration The European Standard EN IS0 105206:2 has the status of a British Standard ICs 59.080.01 .05-206:2000 NO COPYING WITBOUT BSI
2、 PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW STDOBSI BS EN IS0 LOS-ZOb-ENGL 2000 Lb24bb9 070Cb17 428 BS EN IS0 105-2062000 been prepared under the Committee for Materials and Chemicals, was published under the authority of the Standards Committee and comes into effect on 15 December 2000 directi
3、on of the Sector Amd. No. Date Q BSI 12-2000 ISBN O 580 36772 X National foreword Comments This British Standard is the official English language version of EN IS0 105-206:2000. It is identical with IS0 105-Z06:1998. The UK participation in its preparation was entrusted to Technical Committee TcI/81
4、, Colour fastness and colour measurement, which has the responsibility to: - aid enquirers to understand the text; - present to the responsible inkdonaVEuropean committee any enquiries on the interpretation, or proposals for change, and keep the UK interests informed; - monitor related international
5、 and European developments and promulgate them in the UK. A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references Attention is drawn to the fact that CEN and CENELEC Standards nomially include an annex which lists normative references to in
6、ternational publications with their corresponding European publications. The British Standards which implement international or European publications referred to in this document may be found in the BSI Stanbds Catalogue under the section entitled “International Standards Correspondence Index”, or b
7、y using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessary provisions of a contsact. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not of itself confer imm
8、unity from legal obligations. Summary of pages This document comprises a hnt cover, an inside front cover, the EN IS0 title page, the EN IS0 foreword page,the IS0 title page, page i, pages 1 to 7, the annex ZA page, an inside back cover and a back cover. The BSI copyright notice displayed in this do
9、cument indicata when the document was last issued. sTD.BS1 BS EN IS0 205-ZOb-ENGL 2000 = LbZ4bb7 0905bL8 3b4 EUROPEAN STANDARD EN IS0 105206 NORME EUROPENNE EUROPISCHE NORM August 2000 ICs 59.080.01 English version Textiles - Tests for colour fastness - Part Z06: Evaluation of dye and pigment migrat
10、ion (IS0 105-ZO6:1998) Textiles - Essais de solidit des teintures - Partie Z06: Evaluation de la migration des teintures et pigments (IS0 105-Z06:1998) Textilien - Farbechtheitsprfungen - Teil 206: Bewertung der Migration von Farbstoffen und Pigmenten (IS0 105- Z06:1998) This European Standard was a
11、pproved by CEN on 12 July 2000. CEN members are bound to comply with the CENICENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such nationa
12、l standards may be obtained on application to the Central Secretariat or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notif
13、ied to the Central Secretariat has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland an
14、d United Kingdom. EUROPEAN COMMlTE FOR STANDARDIZATION COMITE EUROPEEN DE NORMALISATION EUROPISCHES KOMITEE FUR NORMUNG Central Secretariat: rue de Stassart. 36 6-1050 Brussels Q 2000 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN
15、 IS0 105-Z06:2000 E sTD.BS1 BS EN IS0 LOS-ZOb-ENGL 2000 lb24bb9 0905bL9 2TO EN IS0 105-206:2000 Foreword The text of the International Standard from Technical Committee ISO/TC 38 “Textiles“ of the International Organization for Standardization (ISO) has been taken over as an European Standard by Tec
16、hnical Committee CEN/TC 248 “Textiles and textile products“, the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2001, and conflicting national standa
17、rds shall be withdrawn at the latest by February 2001. According to the CENKENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland
18、, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International Standard IS0 105-ZO6:1998 has been approved by CEN as a European Standard without any modification. NOTE: Normative references to Internati
19、onal Standards are listed in annex ZA (normative). STDmBSI BS EN IS0 LOS-ZUb-ENGL 2000 = Lb24bb9 0905b20 TL2 0 EN IS0 105-206:2000 I NTE R NATIONAL STANDARD IS0 105-206 First edition 1998-06-01 Textiles - Tests for colour fastness - Part Z06: Evaluation of dye and pigment migration Textiles - Essais
20、 de solidit des teintures - Partie Z6: valuation de la migration des teintures et pigments Reference number IS0 105-206:1998( E) - - - - STD.BS1 BS EN IS0 305-ZOb-ENGL ZOO0 LbZ4bb9 0905623 959 EN IS0 105-206:2000 Foreword IS0 (the International Organization for Standardization) is a worldwide federa
21、tion of national standards bodies (IS0 member bodies). The work of preparing International Standards is normally carried out through IS0 technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committ
22、ee. International organizations, governmental and non- governmental, in liaison with ISO, also take part in the work. IS0 collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Drafi International Standards adopted by the tec
23、hnical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. International Standard IS0 105-206 was prepared by Technical Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for
24、cooured textiles and colorants. IS0 105 was previously published in thirteen “parts”, each designated by a letter (e.g. “Part A), with publication dates between 1978 and 1985. Each part contained a series of “sections”, each designated by the respective part letter and by a two-digit serial number (
25、e.g. Section A01)”). These sections are now being republished as separate documents, themselves designated “parts” but retaining their earlier alphanumeric designations. A complete list of these parts is given in IS0 105-A01. Annex A of this part of IS0 105 is for information only. STD.BSI BS EN IS0
26、 105-ZOb-ENGL 2000 m Lb24bb7 0705b22 895 m EN IS0 105-206:2000 Textiles - Tests for colour fastness - Part 206: Evaluation of dye and pigment migration 1 Scope This part of IS0 105 describes a method for assessing the migration propensity of a pad liquor system containing dyes or pigments, subsequen
27、tly referred to as colorants, and which may also contain different types and amounts of migration inhibitors. The degree of migration is obtained by visual examination or by reflectance measurements. The test method may be used to compare the migration propensity of dyes and the effect on migration
28、of different types of migration inhibitors, thickeners and electrolyte. The method may also be used to evaluate a pad liquor with which migration has been found on a continuous dye range. 2 Normative reference The following standard contains provisions which, through reference in this text, constitu
29、tes provisions of this part of IS0 105. At the time of publication, the edition indicated was valid. All standards are subject to revision and parties to agreements based on this part of IS0 105 are encouraged to investigate the possibility of applying the most recent edition of the standard listed
30、below. Members of IEC and IS0 maintain registers of currently valid International Standards. IS0 105-A02: 1993, Textiles - Tests for colour fastness - Part A02 Grey scale for assessing change in colour. 3 Definitions For the purposes of this part of IS0 105, the following definitions apply. 3.1 degr
31、ee of permanence. dye: Colorant applied to or formed on a substrate, via the molecularly dispersed state, which exhibits some 3.2 migration: Movement of a chemical, dye or pigment between fibres, within a substrate or between substrates due to capillary forces. NOTE - Migration may occur in textile
32、processing, testing, storage and use. 3.3 pigment: Colorant in particulate form which is insoluble in a substrate, but which can be dispersed in the substrate to modify its colour. 3.4 pad: Impregnation of a substrate (usually fabric) with a liquor, followed by squeezing between rollers. 1 STD-BSI B
33、S EN IS0 105-ZOb-ENGL 2000 3624b67 0905b23 721 EN IS0 105-206:2000 4 Principle Fabric impregnated with test colorant alone, or with test colorant and migration inhibitor, is dried.while partially covered with a watch glass, permitting differential drying and therefore, migration to occur. The degree
34、 of migration is evaluated by visual examination or by reflectance measurements of the covered and uncovered areas. NOTES 1 When drying conditions are not constant and/or uniform, uneven migration may occur, causing shade variations during a run, or shade differences between the face and back, or be
35、tween the side and centre of the fabric. 2 The pad liquor composition may be modified by varying the amount or type of migration inhibitor and tested in the laboratory prior to the application on the range. The colorant concentration, the fabric and the wet pickup should be the same in the laborator
36、y as used on the range. It is then possible to correlate the test results with the improvement experienced in practice. Two procedures are described: Procedure A. The fabric assembly is allowed to dry at room temperature. The procedure is very simple, but time- consuming (overnight). Procedure B. Th
37、e fabric assembly is dried in a laboratory dryer or oven, either with, or without air circulation. This procedure is faster but somewhat more complicated than procedure A. 5 Apparatus and materials 5.1 Fabric pieces for dyeing. NOTE - For disperse dyes, vat dyes and pigments, generally the preferred
38、 fabric is a blend of 65 %:35 % (mh) polyester: cotton gabardine or heavy twill, heat set, bleached and mercerized. For soluble dyes with affinity to cellulose (e.g. reactive dyes), the preferred fabric is a bleached and mercerized 100 % cotton gabardine or heavy twill. However, any other fabric int
39、ended for use on a continuous dye range may be chosen. 5.2 Balance, capable of weighing to an accuracy of 1 mg. 5.3 Laboratory padder. 5.4 Glass plate, 350 mm x 600 mm, for procedure A. 5.5 Watch glasses, 90 mm diameter with 22 mm arch punch. 5.6 Laboratory pin frame, for procedure B. 5.7 Aluminium
40、rings, 110 mm outer diameter, 80 mm inner diameter, 1 mm thickness, for procedure B. 5.8 Clips, e.g. metal binder clips for procedure B. 5.9 Laboratory dryer or oven, for procedure B. 5.10 Grey scale for assessing change in colour, in accordance with IS0 105-A02. 5.11 Spectrophotometer, for reflecta
41、nce measurements. 6 Test specimen Colorant(s), migration inhibitor, thickening agent and other auxiliaries (e.g. electrolyte for reactive dyes) in desired concentration(s) to be tested as appropriate. STD-BSI BS EN IS0 LOS-ZOb-ENGL 2000 I1624669 0905624 668 EN IS0 105-206:2000 7 Procedure WARNING -
42、It is the users responsibility to use safe and proper techniques in handling materials in this test method and to follow good laboratory practices. Consult manufacturers for specific details, such as material safety data sheets and other manufacturers recommendations. Users should also comply with a
43、ny national and local safety regulations. 7.1 Procedure A Cut a 150 mm x 300 mm piece of fabric (5.1), weigh it using the balance (5.2) and then pad it using the laboratory padder (5.3) at (20 f 2) OC. If other padding temperatures are used, these shall be stated in the test report. Generally the we
44、t pickup is 60 % by mass, but may be adjusted to simulate wet pickup of a particular fabric to be run on a particular range. The pad bath contains colorants and usually, auxiliaries. NOTE - Observe padder safety. Normal safeguards on padders should not be removed. Ensure that there is an adequate gu
45、ard at the roller nip point. A foot-operated kick-off is recommended. Obtain the desired wet pickup by adjusting the pressure at the nip of the pad rolls. Calculate the percent wet pickup as the mass gained by the substrate after padding using the following equation: WP = 1 O0 x (% - I where WP ml m
46、o is the percent mass wet pickup; is the mass of the fabric after padding; is the mass of the fabric before padding. Immediately after padding place the fabric on a flat glass plate (5.4). Place the watch glass (5.5) on the fabric as shown in figure 1, and leave the fabric to dry at room temperature
47、. Remove the watch glass and determine the degree of migration in accordance with clause 8 by comparing the dye concentration in the area of the fabric which was covered by the watch glass to the dye concentration in the area of the fabric which was not covered. A 1 Fabric 2 AreaA 3 AreaB 4 Watch gl
48、ass 5 5 Glass plate Figure 1 - Layout of apparatus for inducing colorant migration using procedure A 3 STD*BSI ES EN IS0 105-ZOb-ENGL 2000 1b24bb9 0305625 5T4 EN IS0 105-206:2000 7.2 Procedure B Proceed as described in procedure A, using a piece of fabric sufficiently large (usually about 110 mm x 2
49、20 mm) to fit a Laboratory pin frame (5.6). Immediately after padding mount the fabric taut on the pin frame (5.6), sandwiched between two watch glasses (5.5), one on the fabric face and one directly underneath on the back of the fabric. Hold the watch glasses in place with two aluminium rings (5.7) and clips (5.8) as shown in figure 2. Dry the fabric assembly horizontally at (100 f 2) “C for approximately 7 min (or until dry) in a laboratory dryer or oven (5.9). Remove the watch glasses and remove the fabric from the pin frame. Determine the
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