1、STDmBSI BS EN IS0 105-Z9-ENGL 1998 m 1b24bb7 Ob72580 474 m BRITISH STANDARD * * rn The European Standard EN IS0 105209 : 1997 has the status of a British Standard ICs 59.080.01 NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW BS EN IS0 105-ZO9 : 1998 Textiles - Tests for colour
2、 fastness Part 209. Determination of cold water solubility of water-soluble dyes (IS0 105-209 : 1995) STD-BSI BS EN IS0 105-ZOS-ENGL 1798 D lb24bb7 Ob72581 300 D AmdNo. BS EN IS0 105-209 : 1998 Date Text affected This British Standard, having been prepared under the direction of the Sector Board for
3、 Materiais and Chemicals, was published under the authority of the Standards Board and comes into effect on 15 January 1998 National foreword This British Standard is the English ianguage version of EN IS0 105209 : 1997. It is identical with IS0 105209 : 1995. The UK participation in its preparation
4、 was entrusted by Technical Committee TCI/25, Chemical properties, to Subcommittee TCI/25/J107 Colour fastness, which has the responsibility to: - aid enquirers to understand the text; - present to the responsible internationallEuropean committee any enquiries on the interpretation, or proposals for
5、 change, and keep the UK interests informed, - monitor related intedonal and European developments and promdgate theminthem A list of organizations represented on this subcommittee can be obtained on request to its secretary. Cross-references Attention is drawn to the fact that CEN and CENELEC stand
6、ards nonnally include an annex which lists normative references to international publications with their correspondmg European publications. The British Standards which implement these international or European publications may be found in the BSI Standards Catalogue under the section entitled ?Inte
7、rnational Standards Correspondence Index?, or by using the ?fid facility of the BSI Standards Elecmnic Catalogue. Compliance with a British Standard does not of itself confer immunity from legai obiigations. Summary of pages This document comprises a front cover, an inside front cover, the EN IS0 ti
8、tle page, the EN IS0 foreword page, the IS0 title page, page ii, pages 1 to 4, the annex ZA page, a blank page, an inside back cover and a back cover. Amendments issued since publication O BSI 1998 ISBN O 080 29453 6 STD.BS1 BS EN IS0 10!irZ9-ENGL 1778 D LbZLibb Ob72582 247 EUROPEAN STANDARD NORME E
9、UROPENNE EUROPISCHE NORM EN IS0 105-209 September 1997 ICs 59.080.1 O Descriptors: see IS0 document English version Textiles - Tests for colour fastness - Patt ZO9: Determination of cold water solubility of water-soluble dyes (IS0 105-209: 1 995) Textiles - Essais de solidit des leinlures - Partie Z
10、og: Dlerminatbn de ia solubilit dans leau froide des colorants solubles dans leau (IS0 105209:1995) Textilien - FaibecMheHsprufungen -Teil 209: Bestimmung der Kaltwrislichkeil von wasserlslichen Farbstoffen (IS0 105-209:1995) This European Standard was approved by CEN on 24 August 1997. CEN members
11、are bound lo comply with lhe CENKENELEC Internai Regulations which stipulate the condilions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographicai derences concerning such national standards may be obtained on applioation to l
12、he Central Secrelariat or to any CEN member. This European Standard exisls in three offciai versions (Engih, French, Geman). A version in any other language made by translation under lhe responsibility of a CEN member inlo ils own language and nolified to the Central Secretariat has lhe same slatus
13、as the official versions. CEN members are the nalionai standards bodies of Austria, Belgium. Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Nelherlands, Norway, Porhigai, Spain, Sweden, Switzerland and United Kingdom. EUROI“ COMMITTEE POR STANDARDQATI
14、ON COMITE EUROPEEN DE NORMALISATION EUROPISCHES KOMITEE FOR NORMUNG Central Secretariat: rue de Stasam, 36 B1050 Bruuel8 O 1997 CEN All rights of exploitation in any form and by any means resewed worldwide for GEN national Members. Ref. No. EN IS0 105-209:1997 E STD-BSI BS EN IS0 105-209-ENGL 1998 =
15、 Lb2LibbS Ob72583 183 = EN IS0 105-209 : 1998 Foreword The text of the International Standard from Technical Committee ISOTTC 38 “Textiles“ of the International Organization for Standardization (IS01 has been taken over as an European Standard by Technical Committee CENTTC 248 “Textiles and textile
16、products“, the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by month of March 1998, and conflicting national standards shall be withdrawn at the latest by Marc
17、h 1998. According to the CENKENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norw
18、ay, Portugal, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of the International Standard IS0 105-209: 1995 has been approved by CEN as a European Standard without any modification. NOTE: Normative references to International Standards are listed in annex ZA (normati
19、ve). STD.BSI BS EN IS0 LOS-ZOS-ENGL 1998 D lb2Llbb b72584 OLT R EN IS0 105-209 : 1998 I N T E R N AT I O NA L STANDARD IS0 105-209 First edition 1 995-06-1 5 Textiles - Tests for colour fastness - Part 209: Determination of cold water solubility of water-soluble dyes Textiles - Essais de solidit des
20、 teintures - Partie ZO9: Dtermination de la solubilit dans leau froide des colorants solubles dans leau Reference number IS0 105-Z09:1995(E) EN IS0 105-209 : 1998 Foreword IS0 (the International Organization for Standardization) is a worldwide federation of national standards bodies (IS0 member bodi
21、es). The work of preparing International Standards is normally carried out through IS0 technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and
22、nongovernmental, in liaison with ISO, also take part in the work. IS0 collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodie
23、s for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. International Standard IS0 105209 was prepared by Technical Committee ISO/TC 38, Textiles, Subcommittee SC 1, Tests for coloured textiles and colorants. IS0 105 was previous
24、ly published in thirteen “parts“, each designated by a letter (e.g. “Part A“), with publication dates between 1978 and 1985. Each part contained a series of “sections“, each designated by the re- spective part letter and by a twodigit serial number (e.g. “Section A01 “). These sections are now being
25、 republished as separate documents, them- selves designated “parts“ but retaining their earlier alphanumeric desig- nations. A complete list of these parts is given in IS0 105AO1. Annex A of this part of IS0 105 is for information only. 0.rcripton: textiles. dyeing. colour fastness, dyes. tests, col
26、our fastness tests, determination, solubili*/, cold water. i STD-BSI BS EN IS0 105-ZO9-ENGL 1998 = lb24bb9 Ob725b 772 llss EN IS0 105-209 : 1998 Textiles - Tests for colour fastness - Part ZO9: Determination of cold water solubility of water-soluble dyes 1 Scope This part of IS0 105 describes a meth
27、od for the de- termination of solubility of water-soluble dyes at 25 OC in aqueous solution without previous heating. The method is not intended to measure absolute sol- ubility. - - = _. - NOTE 1 are listed in annex A. Several factors which may influence test results - * VI * 2 Normative references
28、 The following standards contain provisions which, through reference in this text, constitute provisions of this part of IS0 105. At the time of publication, the editions indicated were valid. All standards are subject to revision, and parties to agreements based on this part of IS0 105 are encourag
29、ed to investigate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and IS0 maintain registers of currently valid International Standards. IS0 1773:1976, Laboratory glassware - Boiling flasks fnarrow-necked). IS0 381 9:1985, Laboratory glassware -
30、Beakers. IS0 3696: 1 987, Water for analytical laboratory use - Specification and test methods. 3 Principle Several solutions of known concentration, including the solubility limit, of the dye to be tested are pre- pared at 25 OC. The solutions are then filtered under suction at this temperature in
31、a heatable Nutsch filter and the cold water solubility limit determined by visual assessment of the filter residues and the measured flow-through time of the filtrate. 4 Apparatus and reagents 4.1 Glass beaker, capacity 400 mi, conforming to IS0 3819. 4.2 Heating bath, thermostatically controlled, t
32、o 25 “C 2 2 OC, with magnetic stirring bar 40 mm long by 6 mm diameter; speed of stirrer 500 r/min to 600 r/min. 4.3 Nutsch filter (Bchner funnel), heatable, of glass, stainless steel or porcelain; inner diameter 70 mm, capacity at least 200 ml, having more than 100 holes with a total surface area o
33、f holes (evenly distributed) of not less than 200 mm2. 4.4 Thermostatic device (optional), with circulation pump to adjust temperature of Nutsch filter. 4.5 Vacuum apparatus. 4.5.1 Suction bottle, capacity 1 litre to 2 litres. 4.5.2 Piston or membrane pump, of sufficiently high suction capacity to c
34、reate a full vacuum of at least 50 kPa under pressure. 4.5.3 Apparatus to adjust and maintain a given vacuum, preferably coupled with a manometer. 1 STD-BSI BS EN IS0 L05-ZU7-ENGL 1778 m Lb24bb7 b72587 827 m EN IS0 105-209 : 1998 4.6 Stopwatch, to measure flow-through time. 4.7 Filter paper, circula
35、r, 70 mm * 2 mm diam- eter. NOTE 2 Filter papers of the following characteristics have been found suitable: Two typical sets of values Gramrnage, g/m2 92 121 Air resistance, Gurley, s/lOO rnl 33 1 Wet burst strength, kPa I 4 Thickness, pm 210 330 Surface appearance smooth smooth See IS0 105-A01:1994
36、, clause 8, note 1 for information on sources of supply of suitable filter paper. The type of filter paper used and the manufacturer shall be listed in the test report. 4.8 Water, complying with grade 3 of IS0 3696, used as dye solvent. An amount of 200 ml is designated as normal. More water may be
37、added to the solution, but such addi- tions shall be reported together with the cold water solubility values. NOTE 3 No account is taken of changes in volume caused by the addition of dye. 5 Preparation of solutions 5.1 The concentrations at which the dye solutions are prepared shall be chosen consi
38、dering the ex- pected cold water solubility limit of the dye: Expecte limit to fall Stepwise increase in between dye concentration ap- proaching limit 1 g/l to 10 g/l 1 g/l 10 g/i to 50 g/i 5 911 50 g/l to 100 g/l 10 s/l above 100 g/i 20 911 5.2 Strew a known amount of the test dye into a glass beak
39、er (4.1) containing 200 ml water under agi- tation (4.8) at 25 OC * 2 “C (maximum strewing time 5 s) in the thermostatically controlled heating bath (4.2). Continue stirring for a maximum total stirring time of 2 min or 5 min. Filter the solution immediately (see clause 6). Stirring time shall be in
40、dicated in the test report along with cold water solubility limit. Repeat the process for each concentration of dye un- der test. 6 Filtering the solutions NOTE 4 In order to avoid any temperature shock effects, it is essential that heated solutions are filtered through equipment already brought to
41、the same temperature as the solution under test. Ideally this is best done using a jacketed filter funnel, but acceptable results can also be obtained using preheated funnels, either by immersion in a water bath or oven, or by passing water preheated to the test temperature through the equipment imm
42、ediately prior to carrying out the test. When using this latter technique, the amount of water should be determined locally in order that the filter funnel can be heated to the same temperature ir- respective of its geometry and the ambient conditions. In all cases when using preheating techniques r
43、ather than a jacketed funnel, the test solution should be passed through the test equipment immediately after removing it from its heating medium. 6.1 Bring the Nutsch filter (4.3) to the dissolving temperature of 25 “C (see 4.4) and maintain this temperature during the entire filtration operation.
44、6.2 Immediately before filtering, wet out two filter papers (4.7) in a double layer with at least 50 ml water at 25 OC in the Nutsch filter. 6.3 Adjust the vacuum (4.5) to between 3 kPa to 4 kPa, which is equivalent to 300 mm to 400 mm water column pressure. 6.4 Filter the dye solution (5.2) at 25 O
45、C f 2 OC and measure the flow-through time with the stopwatch (4.6). 6.5 If the solution does not filter within 2 min at a stabilized vacuum, filter it for an additional maximum 2 min under full vacuum (see 4.5.2). 2 STDSBSI BS EN IS0 LOS-ZOS-ENGL L778 LbZibbS b72588 7b5 Bs EN IS0 105-209 : 1998 6.6
46、 After the solution has flowed through, continue to extract the filter uniformly under full vacuum for 1 min. 6.7 Allow the filters to dry completely at room temperature before evaluation. 7 Evaluation 7.1 Compare visually the dried filters after filtration of the various dye solutions of known conc
47、entrations. The cold water solubility limit is taken as that con- centration at which filter residues are seen. Residues that are difficult to see may possibly be detected by gently rubbing the filter surface with a fingertip. 7.2 Flow-through time may be used as a further evaluation criterion. A su
48、dden sharp increase in flow- through time when moving up the range of solution concentrations indicates that the cold water solubility limit has been exceeded. 8 Test report The test report shall include the following information: number and year of publication of this part of IS0 105, .e. IS0 105-2
49、09:1995; full identification of the dyestuff under test; type of filter paper used and its manufacturer; stirring time (2 min or 5 min) used in preparation of dyestuff solutions (see 5.2); cold water (25 OC) solubility limit of the dyestuff, expressed in grams per litre; flow-through time, where applicable (see 7.2); any special observations during the test or evalu- ation procedure; any deviation, by agreement or otherwise, from the procedure specified (e.g. amounts of solvent other than 200 ml, etc.). 3 EN IS0 105-209 : 1998 Annex A (informative) Fact
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