EN ISO 1833-24-2011 en Textiles - Quantitative chemical analysis - Part 24 Mixtures of polyester and certain other fibres (method using phenol and tetrachloroethane)《纺织品 定量化学分析 第24.pdf

1、raising standards worldwideNO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAWBSI Standards PublicationBS EN ISO 1833-24:2011Textiles Quantitativechemical analysisPart 24: Mixtures of polyester and certainother fibres (method using phenol andtetrachloroethane) (ISO 1833-24:2010)BS

2、 EN ISO 1833-24:2011 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN ISO 1833-24:2011. It is identical to ISO 1833-24:2010.The UK participation in its preparation was entrusted to T e c h n i c a l Committee TCI/80, Chemical testing of textiles.A list of organiz

3、ations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are responsible for its correctapplication. BSI 2011 ISBN 978 0 580 72143 4 ICS 59.060.01 Compliance with a British Standard c

4、annot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Policy and Strategy Committee on 28 February 2011. Amendments issued since publicationDate T e x t a f f e c t e dEUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 1833-24 Febru

5、ary 2011 ICS 59.060.01 English Version Textiles - Quantitative chemical analysis - Part 24: Mixtures of polyester and certain other fibres (method using phenol and tetrachloroethane) (ISO 1833-24:2010) Textiles - Analyse chimique quantitative - Partie 24: Mlanges de polyester et de certaines autres

6、fibres (mthode au phnol et au ttrachlorthane) (ISO 1833-24:2010) Textilien - Quantitative chemische Analysen - Teil 24: Mischungen aus Polyester und bestimmten anderen Fasern (Phenol-/Tetrachlorethan-Verfahren) (ISO 1833-24:2010) This European Standard was approved by CEN on 2 January 2011. CEN memb

7、ers are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on applicati

8、on to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Managem

9、ent Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlan

10、ds, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2011 CEN All rights of exploitation in a

11、ny form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 1833-24:2011: EBS EN ISO 1833-24:2011 EN ISO 1833-24:2011 (E) 3 Foreword The text of ISO 1833-24:2010 has been prepared by Technical Committee ISO/TC 38 “Textiles” of the International Organization for Standardizat

12、ion (ISO) and has been taken over as EN ISO 1833-24:2011 by Technical Committee CEN/TC 248 “Textiles and textile products” the secretariat of which is held by BSI. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, a

13、t the latest by August 2011, and conflicting national standards shall be withdrawn at the latest by August 2011. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any

14、or all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece

15、, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 1833-24:2010 has been approved by CEN as a EN ISO 1833-24:2011 without a

16、ny modification. BS EN ISO 1833-24:2011ISO 1833-24:2010(E) ISO 2010 All rights reserved iiiForeword ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried o

17、ut through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO c

18、ollaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2. The main task of technical committees is to prepare International

19、 Standards. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elemen

20、ts of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. ISO 1833-24 was prepared by Technical Committee ISO/TC 38, Textiles. This first edition, together with ISO 1833-1 to ISO 1833-23, cancels and replaces ISO 1833:19

21、77, which has been technically revised. ISO 1833 consists of the following parts, under the general title Textiles Quantitative chemical analysis: Part 1: General principles of testing Part 2: Ternary fibre mixtures Part 3: Mixtures of acetate and certain other fibres (method using acetone) Part 4:

22、Mixtures of certain protein and certain other fibres (method using hypochlorite) Part 5: Mixtures of viscose, cupro or modal and cotton fibres (method using sodium zincate) Part 6: Mixtures of viscose or certain types of cupro or modal or lyocell and cotton fibres (method using formic acid and zinc

23、chloride) Part 7: Mixtures of polyamide and certain other fibres (method using formic acid) Part 8: Mixtures of acetate and triacetate fibres (method using acetone) Part 9: Mixtures of acetate and triacetate fibres (method using benzyl alcohol) Part 10: Mixtures of triacetate or polylactide and cert

24、ain other fibres (method using dichloromethane) Part 11: Mixtures of cellulose and polyester fibres (method using sulfuric acid) Part 12: Mixtures of acrylic, certain modacrylics, certain chlorofibres, certain elastanes and certain other fibres (method using dimethylformamide) Part 13: Mixtures of c

25、ertain chlorofibres and certain other fibres (method using carbon disulfide /acetone) BS EN ISO 1833-24:2011ISO 1833-24:2010(E) iv ISO 2010 All rights reserved Part 14: Mixtures of acetate and certain chlorofibres (method using acetic acid) Part 15: Mixtures of jute and certain animal fibres (method

26、 by determining nitrogen content) Part 16: Mixtures of polypropylene fibres and certain other fibres (method using xylene) Part 17: Mixtures of chlorofibres (homopolymers of vinyl chloride) and certain other fibres (method using sulfuric acid) Part 18: Mixtures of silk and wool or hair (method using

27、 sulfuric acid) Part 19: Mixtures of cellulose fibres and asbestos (method by heating) Part 20: Mixtures of elastane and certain other fibres (method using dimethylacetamide) Part 21: Mixtures of chlorofibres, certain modacrylics, certain elastanes, acetates, triacetates and certain other fibres (me

28、thod using cyclohexanone) Part 24: Mixtures of polyester and certain other fibres (method using phenol and tetrachloroethane) The following parts are under preparation: Part 22: Mixtures of viscose or certain types of cupro or modal or lyocell and flax fibres (method using formic acid and zinc chlor

29、ide) Part 25: Mixtures of polyester and some other fibres (method using trichloracetic acid and chloroform) Part 23 of ISO 1833, Mixtures of polyethylene and polypropylene (method using cyclohexanone) has been withdrawn by Technical Committee ISO/TC 38. BS EN ISO 1833-24:2011INTERNATIONAL STANDARD I

30、SO 1833-24:2010(E) ISO 2010 All rights reserved 1Textiles Quantitative chemical analysis Part 24: Mixtures of polyester and certain other fibres (method using phenol and tetrachloroethane) WARNING This part of ISO 1833 calls for the use of substances/procedures that may be injurious to the health/en

31、vironment if appropriate conditions are not observed. It refers only to technical suitability and does not absolve the user from legal obligations relating to health and safety/environment at any stage. 1 Scope This part of ISO 1833 specifies a method using phenol and tetrachloroethane to determine

32、the percentage of polyester after removal of non-fibrous matter, in textiles made of binary mixtures of certain polyester fibres with acrylic, polypropylene or aramid fibres. This method is not applicable to coated fabrics. 2 Normative references The following referenced documents are indispensable

33、for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. ISO 1833-1:2006, Textiles Quantitative chemical analysis Part 1: General principles of testing 3 Princ

34、iple The polyester fibre is dissolved out from a known dry mass of the mixture, with a reagent composed of phenol and tetrachloroethane. The residue is collected, washed, dried and weighed; its mass, corrected if necessary, is expressed as a percentage of the dry mass of the mixture. The percentage

35、of polyester is found by difference. 4 Reagents and apparatus Use the reagents described in ISO 1833-1, together with those specified in 4.1 and 4.2. 4.1 Phenol and tetrachloroethane mixture: the reagent mass ratio is 6:4. SAFETY PRECAUTIONS The harmful effects of this reagent shall be borne in mind

36、, and full precautions shall be taken during use. The treatment with this reagent shall be carried out in fume cabinet or hood. 4.2 Ethanol. BS EN ISO 1833-24:2011ISO 1833-24:2010(E) 2 ISO 2010 All rights reserved5 Apparatus 5.1 Conical flask, of minimum capacity 250 ml, glass stoppered. 5.2 Heating

37、 apparatus, suitable for maintaining the temperature of the conical flask at (50 2) C (for example, water bath with thermostat). 6 Test procedure Follow the general procedure described in ISO 1833-1, and then proceed as follows. Place the specimen in the conical flask. Add 100 ml of phenol and tetra

38、chloroethane mixture (4.1) per gram of specimen. Shake the conical flask for 10 min at (50 2) C, then decant the liquid through the weighed filter crucible using suction. Add a further 100 ml of phenol and tetrachloroethane mixture, warmed up to (50 2) C, and decant the liquid through the filter cru

39、cible. Filter the contents of the conical flask through the weighed filter crucible (ISO 1833-1:2006, 6.1) and transfer any residual fibres to the crucible by washing out the residue from the conical flask with 100 ml of ethanol. Repeat the same washing operation with 100 ml of ethanol. Drain the cr

40、ucible under suction and wash the residue on the filter once with water. Do not apply suction again until the washing liquor has drained under gravity. Finally, drain the crucible under suction, dry the crucible and residue, then cool and weigh them. 7 Calculation and expression of results Calculate

41、 the results as described in the instructions in Clause 10 of ISO 1833-1:2006. The value of d is 1,00. BS EN ISO 1833-24:2011ISO 1833-24:2010(E) ISO 2010 All rights reserved 3Bibliography 1 ISO 2076, Textiles Man-made fibres Generic names This page deliberately left blankThis page deliberately left

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