1、BRITISH STANDARD Plastics Unsaturated-polyester resins (UP-R) Part 2: Preparation of test specimens and determination of properties The European Standard EN IS0 3672-2:2001 has the status of a British Standard ICs 83.080.10 BS EN IS0 3 672-2 1200 1 Incovorating Amendment No. I to (renumbers the BS I
2、S0 as BS EN IS0 3672-2:2001) and Corrigendum No. I BS IS0 3672-2:2000 WkNb A%“ U- rn% E rn NO COPYING WITHOUT BSI PERMISSION EXCEPT AS PERMITTED BY COPYRIGHT LAW $ present to the responsible international/European committee any enquiries on the interpretation, or proposals for change, and keep the U
3、K interests informed; monitor related international and European developments and promulgate them in the UK. - A list of organizations represented on this committee can be obtained on request to its secretary. Cross-references The British Standards which implement international or European publicati
4、ons referred to in this document may be found in the BSI Standards Catalogue under the section entitled “International Standards Correspondence Index”, or by using the “Find” facility of the BSI Standards Electronic Catalogue. A British Standard does not purport to include all the necessary provisio
5、ns of a contract. Users of British Standards are responsible for their correct application. Compliance with a British Standard does not ofitself confer immunity from legal obligations. Summary of pages This document comprises a front cover, an inside front cover, the EN IS0 title page, the EN IS0 fo
6、reword page, the IS0 title page, pages ii tov, a blank page, pages 1 to 9, the Annex ZA pages (2 pages) and a back cover. The BSI copyright date displayed in this document indicates when the document was last issued. OBSI 14 May 2002 13326 105 October 2001 Ilmplementation of the European Standard I
7、I ISBN O 580 36679 O EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN IS0 3672-2 August 2001 ICs 83.080.10 English version Plastics - Unsaturated-polyester resins (UP-R) - Part 2: Preparation of test specimens and determination of properties (IS0 3672-212000) Plastiques - Rsines de polyesters no
8、n saturs (UP-R) - Partie 2: Prparation des prouvettes et dtermination des proprits (IS0 3672-2:2000) Kunststoffe - Ungesttigte Polyesterharze (UP-R) - Teil 2: Herstellung von Probekrpern und Bestimmung von Eigenschaften (IS0 3672-2:2000) This European Standard was approved by CEN on 17 June 2001. CE
9、N members are bound to comply with the CENKENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on appl
10、ication to the Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the Management Centre has the
11、same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FO
12、R STANDARDIZATION EUROPISCHES KOMITEE FR NORMUNG COMIT EUROPEN DE NORMALISATION Management Centre: rue de Stassart, 36 B-1050 Brussels O 2001 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN IS0 3672-2:2001 E EN IS0 3672-22001 I COR
13、RECTED 2002-04-17 I Foreword The text of the International Standard from Technical Committee ISO/TC 61 “Plastics“ of the International Organization for Standardization (ISO) has been taken over as a European Standard by Technical Committee CEN/TC 249 “Plastics“, the secretariat of which is held by I
14、BN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by February 2002, and conflicting national standards shall be withdrawn at the latest by February 2002. According to the CENKENELEC Internal Regula
15、tions, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the Un
16、ited Kingdom. Endorsement notice The text of the International Standard IS0 3672-2:2000 has been approved by CEN as a European Standard without any modifications. NOTE Normative references to International Standards are listed in annex ZA (normative). EN IS0 3672-22001 INTERNATIONAL STANDARD IS0 367
17、2-2 First edition 2000-07-1 5 Plastics - Unsaturated-polyester resins Part 2: Preparation of test specimens and determination of properties (UP-R) - Plasfiques - Rsines de polyesfers non safurs (UP-R) - Partie 2: Prparafion des prouveffes ef dferminafion des proprifs Reference number IS0 3672-2:2000
18、(E) os1 0002 II 7 egaP EN IS0 3672-22001 Contents Page Foreword . iv Introduction . v 1 2 3 3.1 3.2 3.3 3.4 4 5 Scope 1 Normative references 1 Preparation of test specimens . 3 General 3 Pretreatment of materials . 3 Preparation of the sheets 4 Cutting out test specimens . 6 Conditioning of test spe
19、cimens . 6 Determination of properties 6 O IS0 0002 -All rights rsedevre . 111 8 egaP EN IS0 3672-22001 Foreword IS0 (the International Organization for Standardization) is a worldwide federation of national standards bodies (IS0 member bodies). The work of preparing International Standards is norma
20、lly carried out through IS0 technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in th
21、e work. IS0 collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. International Standards are drafted in accordance with the rules given in the ISOAEC Directives, Part 3. Draft International Standards adopted by the technica
22、l committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. Attention is drawn to the possibility that some of the elements of this part of IS0 3672 may be the subject of patent rights.
23、IS0 shall not be held responsible for identifying any or all such patent rights. International Standard IS0 3672-2 was prepared by Technical Committee ISO/TC 61, Plasfics, Subcommittee SC 12, Thermoseffing maferials. IS0 3672 consists of the following parts, under the general title Plasfics - Unsafu
24、rafed-polyesfer resins (UP-R): - Par 1: Designafion sysfem - Par 2: Preparafion of fesf specimens and deferminafion of properies iv O IS0 0002 -All rights rsedevre 9 egaP EN IS0 3672-22001 I nt rod u cti on The purpose of this part of IS0 3672 is to designate procedures for the determination of intr
25、insic properties of unsaturated-polyester (UP) resins. It specifies procedures and conditions for the preparation of test specimens of unsaturated-polyester resins in a specified state, and methods for measuring their properties. Those properties and test methods which are suitable and necessary for
26、 characterizing unsaturated-polyester resins are listed. Because of the specificity of thermosetting resins like unsaturated-polyester resins, contrary to other plastic products, a distinction is made between the presentation of the properties before crosslinking (characteristics which are useful fo
27、r processing) and after crosslinking (intrinsic characteristics). O IS0 0002 -All rights rsedevre V EN IS0 3672-22001 Plastics - Unsaturated-polyester resins (UP-R) - Part 2: Preparation of test specimens and determination of properties WARNING - Persons using this part of IS0 3672 should be familia
28、r with normal laboratory practice. This part of IS0 3672 does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions
29、. 1 Scope This part of IS0 3672 specifies the methods of preparation of test specimens and the test methods to be used in determining the properties of unsaturated-polyester resins. Requirements for handling test material and for conditioning both the test material before moulding and the specimens
30、before testing are given here. The properties of crosslinked unsaturated-polyester resins have been selected from the general test methods in IS0 10350-1. Other test methods in wide use for, or of particular significance to, unsaturated-polyester resins (particularly properties useful for the proces
31、sing of non-crosslinked resins) are also included in this part of IS0 3672. In order to obtain reproducible and comparable test results, it is necessary to use the test methods, sample preparation and conditioning procedures, and specimen dimensions specified herein. Values determined will not neces
32、sarily be identical to those obtained using specimens of different dimensions or prepared using different procedures. Other standards exist concerning the determination of properties and preparation of test specimens for unsaturated-polyester-based products, to which reference will be made, if requi
33、red. 2 Normative references The following normative documents contain provisions which, through reference in this text, constitute provisions of this part of IS0 3672. For dated references, subsequent amendments to, or revisions of, any of these publications do not apply. However, parties to agreeme
34、nts based on this part of IS0 3672 are encouraged to investigate the possibility of applying the most recent editions of the normative documents indicated below. For undated references, the latest edition of the normative document referred to applies. Members of IS0 and IEC maintain registers of cur
35、rently valid International Standards. IS0 62:1999, Plasfics - Deferminafion of wafer absorpfion. IS0 75-2:1993, Plasfics - Deferminafion of femperafure of deflecfion under load - Par 2: Plasfics and ebonife. IS0 178:1993, Plasfics - Deferminafion of flexural properies. IS0 179-1 :-I), Plasfics - Def
36、erminafion of Charpy impacf properies - Par 1: Non-insfrumenfed impacf fest 1) To be published. (Revision of IS0 179:1993) 1 EN IS0 3672-22001 IS0 291 :I 997, Plasfics - Sfandard afmospheres for condifioning and fesfing. IS0 527-1 : 1993, Plasfics - Deferminafion of fensile properies - Par 1: Genera
37、l principles. IS0 527-2:1993, Plasfics - Deferminafion of fensile properies - Par 2: Tesf condifions for moulding and exfrusion plasfics. IS0 604: 1993, Plasfics - Deferminafion of compressive properies. IS0 760: 1978, Deferminafion of wafer - Karl Fischer mefhod (General mefhod). IS0 1523: 1983, Pa
38、infs, varnishes, pefroleum and relafed producfs - Deferminafion of flashpoinf - Closed cup equilibrium mefhod. IS0 1675: 1985, Plasfics - Liquid resins- Deferminafion of densify by fhe pyknomefer mefhod. IS0 21 14:-2) , Plasfics (polyesfer resins) and painfs and varnishes (binders) - Deferminafion o
39、f parfial acid value and fofal acid value. IS0 25351:-), Plasfics - Unsafurafed-polyesfer resins - Measuremenf of gel fime af ambienf femperafure. IS0 2554: 1997, Plasfics - Unsafurafed polyesfer resins - Deferminafion of hydroxyl value. IS0 2577: 1984, Plasfics - Thermoseffing moulding maferials -
40、Deferminafion of shrinkage. IS0 271 9:-4), Deferminafion of flash poinf - Pensky-Marens closed cup mefhod. IS0 281 8: 1994, Plasfics - Preparafion of fesf specimens by machining. IS0 31 67:1993, Plasfics - Mulfipurpose fesf specimens. IS0 321 9: 1993, Plasfics - Polymerslresins in fhe liquid sfafe o
41、r as emulsions or dispersions - Deferminafion of viscosify using a rofafional viscomefer wifh defined shear rafe. IS0 3521 : 1997, Plasfics - Unsafurafed polyesfer and epoxy resins - Deferminafion of overall volume shrinkage. IS0 3672-1 :2000, Plasfics - Unsafurafed-polyesfer resins (UP-R) - Par 1:
42、Designafion sysfem. IS0 4589-2: 1996, Plasfics - Deferminafion of burning behaviour by oxygen index - Par 2: Ambienf-femperafure fesf. IS0 461 5: 1979, Plasfics - Unsafurafed polyesfers and epoxide resins - Deferminafion of fofal chlorine confenf. IS0 4630:1997, Binders for painfs and varnishes - Es
43、fimafion of colour of clear liquids by fhe Gardner colour scale. IS0 4901 : 1985, Reinforced plasfics based on unsafurafed polyesfer resins - Deferminafion of residual styrene monomer confenf. IS0 6271 :I 997, Clear liquids - Esfimafion of colour by fhe plafinum-cobalf scale. IS0 6603-2:-5), Plasfic
44、s - Deferminafion of puncfure impacf behaviour of rigid plasfics - Par 2: Insfrumenfed impacf fesfing. IS0 8256: 1990, Plasfics - Deferminafion of fensile-impacf sfrengfh. 2) To be published. (Revision of IS0 2114:1996) 3) To be published. (Revision of IS0 25351997) 4) To be published. (Revision of
45、IS0 2719:1988) 5) To be published. (Revision of IS0 6603-2:1989) 2 EN IS0 3672-22001 IS0 10350-1 :I 998, Plasfics - Acquisifion and presenfafion of comparable single-poinf dafa - Par 1: Moulding maferials. IS0 11 357-2: 1999, Plasfics - Differenfial scanning calorimefry (DSC) - Par 2: Deferminafion
46、of glass fransifion femperafure. IS0 11 359-2: 1999, Plasfics - Thermomechanical analysis (TMA) - Par 2: Deferminafion of coefficienf of linear fhermal expansion and glass fransifion femperafure. IS0 14848: 1998, Plasfics - Unsafurafed-polyesfer resins - Deferminafion of reacfivify af 130 “C. I EC 6
47、0093: 1 980, Mefhods of fesf for volume resisfivify and surface resisfivify of solid elecfrical insulafing maferials. IEC 601 12:1979, Mefhods for defermining fhe comparafive and fhe proof fracking indices of solid insulafing maferials under moisf condifions. IEC 60243-1:1998, Elecfrical sfrengfh of
48、 insulafing maferials - Tesf mefhods - Par 1: Tesfs af power frequencies. I EC 60250: 1 969, Recommended mefhods for fhe deferminafion of fhe permiffivify and dielecfric dissipafion facfor of elecfrical insulafing maferials af power, audio and radio frequencies including mefre wavelengfhs. I EC 6029
49、6: 1 982, Specificafion for unused mineral insulafing oils for fransformers and swifchgear. IEC 60695-11-10:1999, Fire hazard fesfing - Par 11-10: Tesf flames - 50 W horizonfal and vertical flame fesf mefhods. IEC 60695-1 1-20:1999, Fire hazard fesfing - Par 11-20: Tesf flames - 500 W flame fesf mefhods. EN 59:1977, Glass reinforced plasfics - Measuremenf of hardness by means of a Barco1 impressor. 3 Preparation of test specimens 3.1 General This procedure shall be used for the preparation of specimens for the determinati
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