EN ISO 8130-1-2010 en Coating powders - Part 1 Determination of particle size distribution by sieving《粉末涂料 第1部分 用筛选法测定粒度分布》.pdf

1、BRITISH STANDARDBS EN ISO 8130-1:2010Coating powders Part 1: Determinationof particle size distribution by sieving (ISO 8130-1:1992) Incorporating corrigendum April 2011ICS 87.040National forewordThis British Standard is the UK implementation of EN ISO 8130-1:2010. It is identical to ISO 8130-1:1992

2、. It supersedes BS 3900-J2:1993 which is withdrawn.The UK participation in its preparation was entrusted to Technical Committee STI/10, Test methods for paints.A list of organizations represented on this committee can be obtained on request to its secretary.This publication does not purport to inclu

3、de all the necessary provisions of a contract. Users are responsible for its correct application.Compliance with a British Standard cannot confer immunity from legal obligations.BS EN ISO 8130-1:2010This British Standard, having been prepared under the direction of the Pigments, Paints and Varnishes

4、 Standards Policy Committee, was published under the authority ofthe Standards Board and comesin to effect on 15 April 1993 BSI 2011First published January 1987 Second edition April 1993The following BSI references relate to the work on this standard: Committee reference PVC/10 Draft for comment 87/

5、54850 DCAmendments/corrigenda issued since publicationDate Comments 30 April 2011 This corigendum renumbers BS 390-J2:193 as BS EN ISO 8130-1:2010ISBN 978 0 580 72109 0EUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 8130-1 November 2010 ICS 87.040 English Version Coating powders - Part 1: D

6、etermination of particle size distribution by sieving (ISO 8130-1:1992) Poudres pour revtement - Partie 1: Dtermination de la distribution granulomtrique par tamisage (ISO 8130-1:1992) Pulverlacke - Teil 1: Bestimmung der Teilchengrenverteilung durch Sieben (ISO 8130-1:1992)This European Standard wa

7、s approved by CEN on 16 October 2010. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such n

8、ational standards may be obtained on application to the CEN Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language a

9、nd notified to the CEN Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania

10、, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG Management Centre: Avenue Marnix 17, B-1000 Brussels 2010 CEN A

11、ll rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 8130-1:2010: EEN ISO 8130-1:2010 (E) Foreword The text of ISO 8130-1:1992 has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes” of the International Organization fo

12、r Standardization (ISO) and has been taken over as EN ISO 8130-1:2010 by Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsemen

13、t, at the latest by May 2011, and conflicting national standards shall be withdrawn at the latest by May 2011. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or

14、 all such patent rights. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece,

15、Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. Endorsement notice The text of ISO 8130-1:1992 has been approved by CEN as a EN ISO 8130-1:2010 without any m

16、odification. BS EN ISO 8130-1:2010 BSI 2011 11 ScopeThis part of ISO8130specifies a method for the determination of particle size distribution by sieving. It discriminates between particles in the size range from324m to3004m.The method can also be used as an abbreviated procedure, i.e. for the deter

17、mination of the residue on one single sieve only (“go”/“no go” test).2 Normative referencesThe following standards contain provisions which, through reference in this text, constitute provisions of this part of ISO8130. At the time of publication, the editions indicated were valid. All standards are

18、subject to revision, and parties to agreements based on this part of ISO8130are encouraged to investigate the possibility of applying the most recent editions of the standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards.ISO 565:1990, Test sie

19、ves Metal wire cloth, perforated metal plate and electroformed sheet Nominal sizes of openings. ISO 842:1984, Raw materials for paints and varnishes Sampling. 3 Apparatus3.1 Test sieves, circular with a sieving area having a diameter of200mm. The frame and the mesh of the test sieves shall be of met

20、al. The range of nominal mesh apertures shall be between324m and3004m and shall comply with the requirements of ISO565for supplementary sizes (see Annex A). The test sieve shall be covered with a transparent lid.The choice of mesh apertures (see Annex A) will depend on the circumstances. If the appr

21、oximate particle size distribution of a sample is known, it is necessary to use only those test sieves that are appropriate to that particle size range. It is also permissible to restrict the choice of test sieves to those that give sufficient data for a specific purpose. Appropriate details shall b

22、e agreed on between the interested parties.3.2 Air-jet sieve apparatus (see Figure 1), consisting of a cylindrical casing which contains the test sieve(3.1). In the base of the casing shall be an outlet (to which an extractor fan is connected), and an air inlet to permit the injection of air.The air

23、 inlet is connected to a jet rotating at20r/min to25r/min and consisting of a slot-shaped nozzle arranged radially beneath and very close to the sieve mesh. When the jet rotates, it blows air continuously through the mesh, preventing the coating powder particles from blocking the test sieve. The air

24、 is extracted through the outlet, drawing the finer particles through the sieve.The flow of air is controlled by adjusting a slot at the outlet.3.3 Timer (e.g. stopwatch), recording to the nearest1s or better. It may be with a switch fordisconnecting the motor from the sieve apparatus (3.2).3.4 Bala

25、nce, capable of weighing to0,01g.3.5 Mallet, of light construction, with plastics head, suitable for tapping the apparatus to dislodge deposited powder.3.6 Magnifying glass, of magnification at least 5.3.7 Ultrasonic cleaning bath4 SamplingTake a representative sample of the product to be tested, as

26、 described in ISO842.5 Preparation of the test sieves5.1 Using the magnifying glass (3.6), check that the test sieve is clean and undamaged and is not blocked by material used in a previous determination.5.2 If it is necessary to clean the test sieve, clean it using the ultrasonic system (3.7).6 Pro

27、cedureCarry out the determination in duplicate.6.1 Weigh, to the nearest0,01g, the test sieve (3.1) with its transparent lid.6.2 Weigh, to the nearest0,01g, a20g test portion of the sample, except when using a test sieve of mesh aperture less than904m where a10g test portion is taken.6.3 Secure the

28、selected test sieve in position in the sieve apparatus (3.2) and transfer the test portion to the test sieve. Secure the transparent lid, reduce the pressure in the apparatus by (2 0,3) kPa1) and initiate the rotation of the nozzle. Unless otherwise specified, operate the apparatus for (300 15) s.1)

29、 100kPa = 1barBS EN ISO 8130-1:2010EN ISO 8130-1:2010 (E)2 BSI 2011If it can be demonstrated that all the sub-size powder passes through the test sieve within(180 15) s, then it is permissible to use this shorter sieving time, ensuring that the alternative time is noted in the test report. If any ma

30、terial becomes attached to the frame and/or the transparent lid, lightly tap either or both with the mallet (3.5) to dislodge the attached powder.NOTE 1Difficulties may be experienced in sieving extremely fine materials. The addition of a suitable, extremely fine sieving aid (pyrogenic silica or pyr

31、ogenic alumina may be suitable) to the sample at the level of0,2%(based on the initial mass of the test portion) should aid the process. No correction is required for the mass of this additional material as it will pass through the sieve.6.4 At the end of the test period, allow the air pressure to s

32、lowly equalize with that of the room. Remove the lid and the test sieve together with the retained material and weigh to the nearest0,01g.6.5 To determine the particle size distribution by mass determine the mass retained on the test sieve of the smallest aperture chosen as described in the introduc

33、tion. Repeat the procedure described in6.1 to6.4 using a fresh test portion for each size of test sieve, in ascending order, in the range (see3.1) to be reported.NOTEThis diagram illustrates the functioning of the apparatus and is schematic only.Figure 1 Air-jet sieve apparatusBS EN ISO 8130-1:2010E

34、N ISO 8130-1:2010 (E) BSI 2011 37 Expression of results7.1 CalculationFor each test sieve used, calculate the percentage of material retained, R, expressed as a percentage by mass using the equation:where If the two determinations differ by more than3%(absolute), repeat the procedure described in cl

35、ause6.Calculate the mean of two valid determinations and report the result to the nearest integer. Report results from a series of determinations using test sieves of different aperture sizes either in tabular form or graphically.NOTE 2For the graphical representation of results, plotting the data a

36、s a Rosin-Rammler-Sperling-Bennett diagram (RRSBdiagram) is recommended. Extrapolation of data to lower or higher particle sizes may lead to doubtful results. (The RRSB method is one of several ways of representing particle size distribution. Further information may be found in various technical pap

37、ers related to particle size analysis.)7.2 PrecisionNo precision data are currently available.8 Test reportThe test report shall contain at least the following information:a) all details necessary to identify the product tested;b) a reference to this part of ISO8130 (ISO8130-1);c) the result for eac

38、h test sieve as indicated in clause7;d) any deviation from the test method specified;e) the date of the test.m0 is the mass, in grams, of the test sieve and transparent lid;m1 is the mass, in grams, of the test portion;m2 is the mass, in grams, of the test sieve and transparent lid plus the retained

39、 material after the sieving operation.R m2 m0m1- 100=BS EN ISO 8130-1:2010EN ISO 8130-1:2010 (E)4 BSI 2011Annex A (normative) Nominal sizes of test sieves(Extracted from ISO565:1990, Table2)Table A.1 Supplementary sizes (4m)Series R 40/330025021218015012510690756353453832BS EN ISO 8130-1:2010EN ISO

40、8130-1:2010 (E) BSI List of referencesSee national foreword.BS EN ISO 8130-1:2010EN ISO 8130-1:2010 (E)2011BSI GroupHeadquarters 389 Chiswick High Road, London, W4 4AL, UK Tel +44 (0)20 8996 9001 Fax +44 (0)20 8996 7001 standardsBSI - British Standards InstitutionBSI is the independent national bod

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