EN ISO 13383-1-2016 en Fine ceramics (advanced ceramics advanced technical ceramics) - Microstructural characterization - Part 1 Determination of grain size and size distribution《精.pdf

1、Fine ceramics (advancedceramics, advanced technicalceramics) MicrostructuralcharacterizationPart 1: Determination of grain size and sizedistributionBS EN ISO 13383-1:2016(ISO 13383-1:2012)BSI Standards PublicationBS EN ISO 13383-1:2016 BRITISH STANDARDNational forewordThis British Standard is the UK

2、 implementation of EN ISO 13383-1:2016. It is identical to ISO 13383-1:2012. It supersedes BS EN 623-3:2001 and BS ISO 13383-1:2012 which are withdrawn.The UK participation in its preparation was entrusted to Technical Committee RPI/13, Advanced technical ceramics.A list of organizations represented

3、 on this committee can be obtained on request to its secretary.This publication does not purport to include all the necessary provisions of a contract. Users are responsible for its correct application. The British Standards Institution 2016. Published by BSI Standards Limited 2016ISBN 978 0 580 911

4、72 9ICS 81.060.30Compliance with a British Standard cannot confer immunity from legal obligations.This British Standard was published under the authority of the Standards Policy and Strategy Committee on 30 September 2012.Amendments/corrigenda issued since publicationDate Text affected31 May 2016 Th

5、is corrigendum renumbers BS ISO 13383-1:2012 as BS EN ISO 13383-1:2016.g3g3g3g8g24g21g18g19g8g4g17g3g22g23g4g17g7g4g21g7g3g17g18g21g16g8g3g8g24g21g18g19g50g8g17g17g8g3g8g24g21g18g19g34g12g22g6g11g8g3g17g18g21g16g3EN ISO 13383-1 g3 g3g3 g4g146g148g139g142g3g884g882g883g888g3g12g6g22g3g890g883g484g882

6、g888g882g484g885g882g3 g22g151g146g135g148g149g135g134g135g149g3g8g17g3g888g884g885g486g885g483g884g882g882g883g8g144g137g142g139g149g138g3g25g135g148g149g139g145g144g3g3g9g139g144g135g3g133g135g148g131g143g139g133g149g3g523g131g134g152g131g144g133g135g134g3g133g135g148g131g143g139g133g149g481g3g131

7、g134g152g131g144g133g135g134g3g150g135g133g138g144g139g133g131g142g3g133g135g148g131g143g139g133g149g524g3g486g3g16g139g133g148g145g149g150g148g151g133g150g151g148g131g142g3g133g138g131g148g131g133g150g135g148g139g156g131g150g139g145g144g3g486g3g19g131g148g150g3g883g483g3g7g135g150g135g148g143g139g1

8、44g131g150g139g145g144g3g145g136g3g137g148g131g139g144g3g149g139g156g135g3g131g144g134g3g149g139g156g135g3g134g139g149g150g148g139g132g151g150g139g145g144g3g523g12g22g18g3g883g885g885g890g885g486g883g483g884g882g883g884g524g3g6g177g148g131g143g139g147g151g135g149g3g150g135g133g138g144g139g147g151g13

9、5g149g3g486g3g6g131g148g131g133g150g177g148g139g149g131g150g139g145g144g3g143g139g133g148g145g149g150g148g151g133g150g151g148g131g142g135g3g486g3g19g131g148g150g139g135g3g883g483g3g7g177g150g135g148g143g139g144g131g150g139g145g144g3g134g135g3g142g131g3g150g131g139g142g142g135g3g135g150g3g134g135g3g1

10、42g131g3g134g139g149g150g148g139g132g151g150g139g145g144g3g134g135g149g3g137g148g131g139g144g149g3g523g12g22g18g3g883g885g885g890g885g486g883g483g884g882g883g884g524g3g3 g11g145g133g138g142g135g139g149g150g151g144g137g149g141g135g148g131g143g139g141g3g486g3g16g139g141g148g145g149g150g148g151g141g150

11、g151g148g135g142g142g135g3g6g138g131g148g131g141g150g135g148g139g149g139g135g148g151g144g137g3g486g3g23g135g139g142g3g883g483g3g5g135g149g150g139g143g143g151g144g137g3g134g135g148g3g14g145g148g144g137g148g218g233g135g3g151g144g134g3g134g135g148g3g14g145g148g144g137g148g218g233g135g144g152g135g148g15

12、0g135g139g142g151g144g137g3g523g12g22g18g3g883g885g885g890g885g486g883g483g884g882g883g884g524g3g23g138g139g149g3g8g151g148g145g146g135g131g144g3g22g150g131g144g134g131g148g134g3g153g131g149g3g131g146g146g148g145g152g135g134g3g132g155g3g6g8g17g3g145g144g3g883g890g3g16g131g148g133g138g3g884g882g883g8

13、88g484g3g3g3g6g8g17g3g143g135g143g132g135g148g149g3g131g148g135g3g132g145g151g144g134g3g150g145g3g133g145g143g146g142g155g3g153g139g150g138g3g150g138g135g3g6g8g17g512g6g8g17g8g15g8g6g3g12g144g150g135g148g144g131g142g3g21g135g137g151g142g131g150g139g145g144g149g3g153g138g139g133g138g3g149g150g139g146

14、g151g142g131g150g135g3g150g138g135g3g133g145g144g134g139g150g139g145g144g149g3g136g145g148g3g137g139g152g139g144g137g3g150g138g139g149g3g8g151g148g145g146g135g131g144g3g22g150g131g144g134g131g148g134g3g150g138g135g3g149g150g131g150g151g149g3g145g136g3g131g3g144g131g150g139g145g144g131g142g3g149g150g

15、131g144g134g131g148g134g3g153g139g150g138g145g151g150g3g131g144g155g3g131g142g150g135g148g131g150g139g145g144g484g3g24g146g486g150g145g486g134g131g150g135g3g142g139g149g150g149g3g131g144g134g3g132g139g132g142g139g145g137g148g131g146g138g139g133g131g142g3g148g135g136g135g148g135g144g133g135g149g3g133

16、g145g144g133g135g148g144g139g144g137g3g149g151g133g138g3g144g131g150g139g145g144g131g142g3g149g150g131g144g134g131g148g134g149g3g143g131g155g3g132g135g3g145g132g150g131g139g144g135g134g3g145g144g3g131g146g146g142g139g133g131g150g139g145g144g3g150g145g3g150g138g135g3g6g8g17g486g6g8g17g8g15g8g6g3g16g1

17、31g144g131g137g135g143g135g144g150g3g6g135g144g150g148g135g3g145g148g3g150g145g3g131g144g155g3g6g8g17g3g143g135g143g132g135g148g484g3g3g23g138g139g149g3g8g151g148g145g146g135g131g144g3g22g150g131g144g134g131g148g134g3g135g154g139g149g150g149g3g139g144g3g150g138g148g135g135g3g145g136g136g139g133g139g

18、131g142g3g152g135g148g149g139g145g144g149g3g523g8g144g137g142g139g149g138g481g3g9g148g135g144g133g138g481g3g10g135g148g143g131g144g524g484g3g4g3g152g135g148g149g139g145g144g3g139g144g3g131g144g155g3g145g150g138g135g148g3g142g131g144g137g151g131g137g135g3g143g131g134g135g3g132g155g3g150g148g131g144g1

19、49g142g131g150g139g145g144g3g151g144g134g135g148g3g150g138g135g3g148g135g149g146g145g144g149g139g132g139g142g139g150g155g3g145g136g3g131g3g6g8g17g3g143g135g143g132g135g148g3g139g144g150g145g3g139g150g149g3g145g153g144g3g142g131g144g137g151g131g137g135g3g131g144g134g3g144g145g150g139g136g139g135g134g

20、3g150g145g3g150g138g135g3g6g8g17g486g6g8g17g8g15g8g6g3g16g131g144g131g137g135g143g135g144g150g3g6g135g144g150g148g135g3g138g131g149g3g150g138g135g3g149g131g143g135g3g149g150g131g150g151g149g3g131g149g3g150g138g135g3g145g136g136g139g133g139g131g142g3g152g135g148g149g139g145g144g149g484g3g3g6g8g17g3g1

21、43g135g143g132g135g148g149g3g131g148g135g3g150g138g135g3g144g131g150g139g145g144g131g142g3g149g150g131g144g134g131g148g134g149g3g132g145g134g139g135g149g3g145g136g3g4g151g149g150g148g139g131g481g3g5g135g142g137g139g151g143g481g3g5g151g142g137g131g148g139g131g481g3g6g148g145g131g150g139g131g481g3g6g1

22、55g146g148g151g149g481g3g6g156g135g133g138g3g21g135g146g151g132g142g139g133g481g3g7g135g144g143g131g148g141g481g3g8g149g150g145g144g139g131g481g3g9g139g144g142g131g144g134g481g3g9g145g148g143g135g148g3g28g151g137g145g149g142g131g152g3g21g135g146g151g132g142g139g133g3g145g136g3g16g131g133g135g134g145

23、g144g139g131g481g3g9g148g131g144g133g135g481g3g10g135g148g143g131g144g155g481g3g10g148g135g135g133g135g481g3g11g151g144g137g131g148g155g481g3g12g133g135g142g131g144g134g481g3g12g148g135g142g131g144g134g481g3g12g150g131g142g155g481g3g15g131g150g152g139g131g481g3g15g139g150g138g151g131g144g139g131g481

24、g3g15g151g154g135g143g132g145g151g148g137g481g3g16g131g142g150g131g481g3g17g135g150g138g135g148g142g131g144g134g149g481g3g17g145g148g153g131g155g481g3g19g145g142g131g144g134g481g3g19g145g148g150g151g137g131g142g481g3g21g145g143g131g144g139g131g481g3g22g142g145g152g131g141g139g131g481g3g22g142g145g15

25、2g135g144g139g131g481g3g22g146g131g139g144g481g3g22g153g135g134g135g144g481g3g22g153g139g150g156g135g148g142g131g144g134g481g3g23g151g148g141g135g155g3g131g144g134g24g144g139g150g135g134g3g14g139g144g137g134g145g143g484g3g3g3g3g3g8g24g21g18g19g8g4g17g3g6g18g16g16g12g23g23g8g8g3g9g18g21g3g22g23g4g17g

26、7g4g21g7g12g29g4g23g12g18g17g3g6g18g16g12g23g50g3g8g24g21g18g19g50g8g17g3g7g8g3g17g18g21g16g4g15g12g22g4g23g12g18g17g3g8g24g21g18g19g34g12g22g6g11g8g22g3g14g18g16g12g23g8g8g3g9g111g21g3g17g18g21g16g24g17g10g3g3g3g3CEN-CENELECg3Management Centre: Avenue Marnix 17, B-1000 Brussels g825g3g884g882g883g8

27、88g3g6g8g17g3 g4g142g142g3g148g139g137g138g150g149g3g145g136g3g135g154g146g142g145g139g150g131g150g139g145g144g3g139g144g3g131g144g155g3g136g145g148g143g3g131g144g134g3g132g155g3g131g144g155g3g143g135g131g144g149g3g148g135g149g135g148g152g135g134g3g153g145g148g142g134g153g139g134g135g3g136g145g148g3

28、g6g8g17g3g144g131g150g139g145g144g131g142g3g16g135g143g132g135g148g149g484g3g21g135g136g484g3g17g145g484g3g8g17g3g12g22g18g3g883g885g885g890g885g486g883g483g884g882g883g888g3g8European foreword The text of ISO 13383-1:2012 has been prepared by Technical Committee ISO/TC 206 “Fine ceramics” of the In

29、ternational Organization for Standardization (ISO) and has been taken over as EN ISO 13383-1:2016 by Technical Committee CEN/TC 184 “Advanced technical ceramics” the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of

30、 an identical text or by endorsement, at the latest by October 2016, and conflicting national standards shall be withdrawn at the latest by October 2016. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not

31、 be held responsible for identifying any or all such patent rights. This document supersedes EN 623-3:2001. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Cr

32、oatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

33、 the United Kingdom. Endorsement notice The text of ISO 13383-1:2012 has been approved by CEN as EN ISO 13383-1:2016 without any modification. BS EN ISO 13383-1:2016EN ISO 13383-1:2016 (E)BS ISO 13383-1:2012ISO 13383-1:2012(E) ISO 2012 All rights reserved iiiContents PageForeword iv1 Scope .12 Norma

34、tive references 1g885g3 g23g135g148g143g149g3g131g144g134g3g134g135g976g139g144g139g150g139g145g144g149 .1g886g3 g22g139g137g144g139g976g139g133g131g144g133g135g3g131g144g134g3g151g149g135 35 Apparatus .4g887g484g883g3 g22g135g133g150g139g145g144g139g144g137g3g135g147g151g139g146g143g135g144g150 .4g

35、887g484g884g3 g16g145g151g144g150g139g144g137g3g135g147g151g139g146g143g135g144g150 .4g887g484g885g3 g10g148g139g144g134g139g144g137g3g131g144g134g3g146g145g142g139g149g138g139g144g137g3g135g147g151g139g146g143g135g144g150 4g887g484g886g3 g8g150g133g138g139g144g137g3g135g147g151g139g146g143g135g144g

36、150.45.5 Microscope .45.6 Calibrated rule or scale 55.7 Circle template 56 Test piece preparation 56.1 Sampling .56.2 Cutting 56.3 Mounting 5g888g484g886g3 g10g148g139g144g134g139g144g137g3g131g144g134g3g146g145g142g139g149g138g139g144g137 .56.5 Etching .67 Photomicrography 6g889g484g883g3 g10g135g1

37、44g135g148g131g142g3g131g149g146g135g133g150g149 .6g889g484g884g3 g18g146g150g139g133g131g142g3g143g139g133g148g145g149g133g145g146g155 6g889g484g885g3 g22g133g131g144g144g139g144g137g3g135g142g135g133g150g148g145g144g3g143g139g133g148g145g149g133g145g146g155 .67.4 Calibration micrographs .78 Measur

38、ement of micrographs .7g890g484g883g3 g10g135g144g135g148g131g142 .78.2 Method A1 .88.3 Method A2 .88.4 Method B 8g890g484g887g3 g24g149g135g3g145g136g3g131g151g150g145g143g131g150g139g133g3g145g148g3g149g135g143g139g486g131g151g150g145g143g131g150g139g133g3g139g143g131g137g135g3g131g144g131g142g155

39、g149g139g149g3g136g145g148g3g143g135g150g138g145g134g149g3g4g3g131g144g134g3g5 .99 Calculation of results 109.1 Method A1 109.2 Method A2 109.3 Method B .1010 Interferences and uncertainties 1111 Test report 12Annex A (informative) Grinding and polishing procedures 14Annex B (informative) Etching pr

40、ocedures 16Annex C (informative) Setting Khler illumination in an optical microscope .18Annex D (informative)g3g21g145g151g144g134g486g148g145g132g139g144g3g152g135g148g139g976g139g133g131g150g139g145g144g3g145g136g3g16g135g150g138g145g134g3g4g88319Annex E (informative)g3g21g145g151g144g134g486g148g

41、145g132g139g144g3g152g135g148g139g976g139g133g131g150g139g145g144g3g145g136g3g16g135g150g138g145g134g3g5 20Annex F (informative) Grain size distribution measurement .21Annex G (informative) Results sheet: Grain size in accordance with ISO 13383-1 .22Bibliography .23BS EN ISO 13383-1:2016ISO 13383-1:

42、2012(E)BS ISO 13383-1:2012ISO 13383-1:2012(E)Forewordg12g22g18g3g523g150g138g135g3g12g144g150g135g148g144g131g150g139g145g144g131g142g3g18g148g137g131g144g139g156g131g150g139g145g144g3g136g145g148g3g22g150g131g144g134g131g148g134g139g156g131g150g139g145g144g524g3g139g149g3g131g3g153g145g148g142g134g

43、153g139g134g135g3g136g135g134g135g148g131g150g139g145g144g3g145g136g3g144g131g150g139g145g144g131g142g3g149g150g131g144g134g131g148g134g149g3g132g145g134g139g135g149g3g523g12g22g18g3g143g135g143g132g135g148g3g132g145g134g139g135g149g524g484g3g23g138g135g3g153g145g148g141g3g145g136g3g146g148g135g146g

44、131g148g139g144g137g3g12g144g150g135g148g144g131g150g139g145g144g131g142g3g22g150g131g144g134g131g148g134g149g3g139g149g3g144g145g148g143g131g142g142g155g3g133g131g148g148g139g135g134g3g145g151g150g3g150g138g148g145g151g137g138g3g12g22g18g3g150g135g133g138g144g139g133g131g142g3g133g145g143g143g139g1

45、50g150g135g135g149g484g3g8g131g133g138g3g143g135g143g132g135g148g3g132g145g134g155g3g139g144g150g135g148g135g149g150g135g134g3g139g144g3g131g3g149g151g132g140g135g133g150g3g136g145g148g3g153g138g139g133g138g3g131g3g150g135g133g138g144g139g133g131g142g3committee has been established has the right to

46、be represented on that committee. International g145g148g137g131g144g139g156g131g150g139g145g144g149g481g3g137g145g152g135g148g144g143g135g144g150g131g142g3g131g144g134g3g144g145g144g486g137g145g152g135g148g144g143g135g144g150g131g142g481g3g139g144g3g142g139g131g139g149g145g144g3g153g139g150g138g3g1

47、2g22g18g481g3g131g142g149g145g3g150g131g141g135g3g146g131g148g150g3g139g144g3g150g138g135g3g153g145g148g141g484g3g12g22g18g3g133g145g142g142g131g132g145g148g131g150g135g149g3g133g142g145g149g135g142g155g3g153g139g150g138g3g150g138g135g3g12g144g150g135g148g144g131g150g139g145g144g131g142g3g8g142g135g

48、133g150g148g145g150g135g133g138g144g139g133g131g142g3g6g145g143g143g139g149g149g139g145g144g3g523g12g8g6g524g3g145g144g3g131g142g142g3g143g131g150g150g135g148g149g3g145g136g3g135g142g135g133g150g148g145g150g135g133g138g144g139g133g131g142g3g149g150g131g144g134g131g148g134g139g156g131g150g139g145g144

49、g484g12g144g150g135g148g144g131g150g139g145g144g131g142g3g22g150g131g144g134g131g148g134g149g3g131g148g135g3g134g148g131g136g150g135g134g3g139g144g3g131g133g133g145g148g134g131g144g133g135g3g153g139g150g138g3g150g138g135g3g148g151g142g135g149g3g137g139g152g135g144g3g139g144g3g150g138g135g3g12g22g18g512g12g8g6g3g7g139g148g135g133g150g139g152g135g149g481g3g19g131g148g150g3g884g484The main task of technical committees is to prepare International Standards. Draft International g22g150g131g144g134g131g148g134g149g3g131g134g145g146g150g135g134g3g132g155g3g150g138g135g3g150g135g133g138g144g1