EN ISO 13803-2014 en Paints and varnishes - Determination of haze on paint films at 20 degrees《色漆和清漆 20℃漆膜光泽度的测定(ISO 13803 2014)》.pdf

1、BSI Standards PublicationBS EN ISO 13803:2014Paints and varnishes Determination of haze on paintfilms at 20 degreesBS EN ISO 13803:2014 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN ISO13803:2014. It supersedes BS EN ISO 13803:2004 which is withdrawn.The UK pa

2、rticipation in its preparation was entrusted to TechnicalCommittee STI/10, Test methods for paints.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a contract. Users are respon

3、sible for its correctapplication. The British Standards Institution 2014. Published by BSI StandardsLimited 2014ISBN 978 0 580 71907 3ICS 87.040Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the authority of theStandards Poli

4、cy and Strategy Committee on 31 October 2014.Amendments issued since publicationDate Text affectedEUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 13803 October 2014 ICS 87.040 Supersedes EN ISO 13803:2004English Version Paints and varnishes - Determination of haze on paint films at 20 degre

5、es (ISO 13803:2014) Peintures et vernis - Dtermination du voile sur des feuils de peinture 20 degrs (ISO 13803:2014) Beschichtungsstoffe - Bestimmung des Schleiers von Beschichtungen bei 20 (ISO 13803:2014) This European Standard was approved by CEN on 24 August 2014. CEN members are bound to comply

6、 with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC M

7、anagement Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same

8、 status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg,

9、Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOMITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2014

10、 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 13803:2014 EBS EN ISO 13803:2014EN ISO 13803:2014 (E) 3 Foreword This document (EN ISO 13803:2014) has been prepared by Technical Committee ISO/TC 35 “Paints and varnishes” in co

11、llaboration with Technical Committee CEN/TC 139 “Peintures et vernis” the secretariat of which is held by DIN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by April 2015, and conflicting national

12、standards shall be withdrawn at the latest by April 2015. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shall not be held responsible for identifying any or all such patent rights. This document supersedes EN

13、ISO 13803:2004. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedo

14、nia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. Endorsement notice The text of ISO 13803:2014 has been approved by CEN

15、as EN ISO 13803:2014 without any modification. BS EN ISO 13803:2014ISO 13803:2014(E) ISO 2014 All rights reserved iiiContents PageForeword ivIntroduction v1 Scope . 12 Normative references 13 Terms and definitions . 14 Principle 15 Apparatus and materials25.1 Hazemeter . 25.2 Measurement standards (

16、certified reference material, working measurement standards) 66 Test panels 76.1 Substrate 76.2 Preparation and coating 76.3 Drying and conditioning . 76.4 Thickness of coating . 77 Calibration and adjustment of the hazemeter . 77.1 Preparation of the apparatus 77.2 Zero point check 77.3 Calibration

17、 and adjustment . 78 Procedure. 88.1 General . 88.2 Haze measurement of coatings from liquid paints and powder coating materials on glass plates 88.3 Haze measurement on other coated dry substrates . 89 Precision . 89.1 General . 89.2 Repeatability limit r 89.3 Reproducibility limit R 910 Test repor

18、t . 9Annex A (normative) Calculation of linear haze .10Bibliography .11BS EN ISO 13803:2014ISO 13803:2014(E)ForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO member bodies). The work of preparing International Standards is no

19、rmally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in

20、 the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those intended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular t

21、he different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).Attention is drawn to the possibility that some of the elements of this docu

22、ment may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document will be in the Introduction and/or on the ISO list of patent declarations received (see www.iso.or

23、g/patents).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the meaning of ISO specific terms and expressions related to conformity assessment, as well as information about ISOs adherence to the WTO pr

24、inciples in the Technical Barriers to Trade (TBT) see the following URL: Foreword - Supplementary information.The committee responsible for this document is ISO/TC 35, Paints and varnishes, Subcommittee SC 9, General test methods for paints and varnishes.This second edition cancels and replaces the

25、first edition (ISO 13803:2000), which has been technically revised. The main technical changes are:a) the symbols have been adapted to the revision of ISO 2813;b) an introduction and a principle clause have been added;c) the supplementary test conditions have been included in the test report;d) the

26、normative references have been updated.iv ISO 2014 All rights reservedBS EN ISO 13803:2014ISO 13803:2014(E)IntroductionHigh quality surfaces are expected to have a clear and brilliant appearance. Microstructures can cause a milky appearance. This effect is described as haze. A high gloss surface wit

27、h microscopic texture has diffused light with low intensity adjacent to the main direction of reflection. The majority of the incident light is reflected in the specular direction which will make the surface appear high glossy with image forming qualities, but with a milky haziness on top of it.The

28、phenomenon haze can be seen on high gloss surfaces only. Therefore, the 20 geometry is used like with a gloss meter. The aperture range of a 20 gloss meter is 1,8. Two additional sensors next to the gloss detector measure the intensity of the diffused light responsible for haze. Thus, the specularly

29、 reflected and the scattered light are measured simultaneously. In order to better correlate with the visual perception, haze is displayed in a logarithmic scale the lower the haze reading the better the surface. ISO 2014 All rights reserved vBS EN ISO 13803:2014BS EN ISO 13803:2014Paints and varnis

30、hes Determination of haze on paint films at 201 ScopeThis International Standard specifies a test method for determining the haze of coatings. The method is suitable for the haze measurement of non-textures coatings on plane, opaque substrates.The use of the 20 geometry means that the method is clos

31、ely related to the measurement of gloss at 20 in ISO 2813. The application of this method is intended to give improved differentiation between high-gloss surfaces, for example in the field of assessment of dispersion characteristics.2 Normative referencesThe following documents, in whole or in part,

32、 are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 1514, Paints and varnishes Standard panels for te

33、stingISO 2808, Paints and varnishes Determination of film thicknessISO 2813, Paints and varnishes Determination of gloss value at 20, 60and 853 Terms and definitionsFor the purposes of this document, the following terms and definitions apply.3.1hazemilky opalescence in high-gloss or clear coatingsSO

34、URCE: ISO 4618:2014, 2.1373.2geometryidentification of a method of haze measurement using a specified angle with assigned aperturesSOURCE: ISO 2813:2014, 3.2, modified the term “gloss” has been replaced with “haze”.3.3haze valueratio of the luminous flux reflected and diffusely scattered from an obj

35、ect adjacent to the specular direction for a specified source and receptor angle to the luminous flux reflected from glass with a refractive index of 1,567 in the specular direction, this glass being assigned the value of 100 on the linear haze scaleNote 1 to entry: The measurement of haze value is

36、related to the measurement of gloss in accordance with ISO 2813.4 PrincipleWith a reflectometric apparatus haze values are determined on coated surfaces, correlating with the visual haze perception.INTERNATIONAL STANDARD ISO 13803:2014(E) ISO 2014 All rights reserved 1BS EN ISO 13803:2014ISO 13803:2

37、014(E)The method of haze measurement is specified by the following parameters: measuring angles; field stop apertures; spectral adaptation; reference refractive index.5 Apparatus and materials5.1 Hazemeter5.1.1 GeneralThe hazemeter shall consist of a light source and a lens that directs a parallel b

38、eam of light onto the surface under test, plus a receptor housing containing a lens, a field stop and a photoelectric cell to receive the required cone of reflected light. The source of the hazemeter is shown in Figure 1.Key1 light source2 sensor3 gloss4 haze5 test surfaceFigure 1 Measuring angle of

39、 205.1.2 GeometriesThe axis of the incident beam shall be at an angle 1= (20,0 0,1) (see Figure 1) to the normal to the surface under test. With a flat piece of polished black glass or a front reflecting mirror instead of the test panel position, the source field stop shall be reproduced at the cent

40、re of the receptor field stop (see Figure 3).The optical axis of the receptor shall be coincident with the mirror image of the axis of the incident beam to within 0,1, i.e. the condition 1- 2 0,1 shall be fulfilled (see Figure 2).The dimensions of the source aperture and the receptor aperture and th

41、e permissible tolerances shall be as indicated in Table 1.In order to average out the entire surface, the width of the illuminated area on the test panel shall be significantly larger than possible surface irregularities: a generally accepted value is 10 mm.2 ISO 2014 All rights reservedBS EN ISO 13

42、803:2014ISO 13803:2014(E)The angular dimensions of the receptor field stop shall be measured from the receptor lens.There shall be no vignetting of rays that lie with the specified angular fields.The photoelectric cell shall give a reading proportional to the light flux passing the receptor field st

43、op, to a deviation within 1 % of the full-scale reading ISO 2014 All rights reserved 3BS EN ISO 13803:2014ISO 13803:2014(E)Key1 light source2 source image aperture3 source lens4 receptor lens5 test surface6 receptor area7 image of the source aperture in the receptor field stop1angle of the beam agai

44、nst surface normal2reflection angle of the beam refracted from medium 2 (against surface normal)1receptor aperture2central opaque zone of the receptor aperture3source image aperture angleFigure 2 Course of beam of the hazemeter4 ISO 2014 All rights reservedBS EN ISO 13803:2014ISO 13803:2014(E)Key1 p

45、lane of measurement2 plane perpendicular to plane of measurement3 receptor area4 receptor field stop5 image of the source aperture in the receptor field stopFigure 3 Receptor field stop5.1.3 Filtering at the receptorFiltering at the receptor shall be done in such a way that the transmittance of the

46、filter () is given by Formula 1:()=()()()()kVSLLCrelS(1)whereV() is the CIE photopic luminous efficiency;SC() is the spectral power distribution of CIE illuminant C;L()relis the relative spectral sensitivity of the receptor;LS() is the spectral power distribution of the light source;k is the calibra

47、tion constant. ISO 2014 All rights reserved 5BS EN ISO 13803:2014ISO 13803:2014(E)Table 1 Angles of source image aperture and receptor apertureAnglein parallel to plane of reflectionperpendicular to plane of reflectionSource image aperture 30,75 0,10 2,50 0,1Receptor aperture 15,50 0,25 5,50 0,25Cen

48、tral opaque part of receptor aperture 22,00 0,1 5,50 0,25NOTE 1 In Figure 3 the plane of reflection corresponds to the plane of illustration.NOTE 2 In Figure 3 only the aperture angles in parallel to the plane of reflection are illustrated.5.2 Measurement standards (certified reference material, wor

49、king measurement standards)1)5.2.1 High gloss standard A (working measurement standard)Plane black glass plate with the following properties: surface grinded and polished; gloss values 88 GU.Thickness, rear side, and edges shall be made in such a way that interfering light, scattered light, and reflected light from the edges and the rear side are avoided.The following specifications parameters shall be recorded on the standard: direction of measure