EN ISO 15701-2015 en Leather - Tests for colour fastness - Colour fastness to migration into polymeric material《皮革 色牢度测试 聚合材料的色牢度(ISO 15701 2015)》.pdf

1、BSI Standards PublicationBS EN ISO 15701:2015Leather Tests for colourfastness Colour fastnessto migration into polymericmaterialBS EN ISO 15701:2015 BRITISH STANDARDNational forewordThis British Standard is the UK implementation of EN ISO15701:2015. It supersedes BS EN ISO 15701:1999 which is withdr

2、awn.The UK participation in its preparation was entrusted to TechnicalCommittee TCI/69, Footwear, leather and coated fabrics.A list of organizations represented on this committee can beobtained on request to its secretary.This publication does not purport to include all the necessaryprovisions of a

3、contract. Users are responsible for its correctapplication. The British Standards Institution 2015. Published by BSI StandardsLimited 2015ISBN 978 0 580 78789 8ICS 59.140.30Compliance with a British Standard cannot confer immunity fromlegal obligations.This British Standard was published under the a

4、uthority of theStandards Policy and Strategy Committee on 30 April 2015.Amendments issued since publicationDate Text affectedEUROPEAN STANDARD NORME EUROPENNE EUROPISCHE NORM EN ISO 15701 April 2015 ICS 59.140.30 Supersedes EN ISO 15701:1999English Version Leather - Tests for colour fastness - Colou

5、r fastness to migration into polymeric material (ISO 15701:2015) Cuir - Essais de solidit des coloris - Solidit des coloris la migration dans les matriaux polymres (ISO 15701:2015) Leder - Farbechtheitsprfungen - Bestimmung der Migrationsechtheit gegenber Polymerwerkstoff (ISO 15701:2015) This Europ

6、ean Standard was approved by CEN on 21 February 2015. CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references c

7、oncerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member

8、 into its own language and notified to the CEN-CENELEC Management Centre has the same status as the official versions. CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, Franc

9、e, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United Kingdom. EUROPEAN COMMITTEE FOR STANDARDIZATION COMIT EUROPEN DE NORMALISATION EUROPISCHES KOM

10、ITEE FR NORMUNG CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels 2015 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN ISO 15701:2015 EBS EN ISO 15701:2015EN ISO 15701:2015 (E) 3 Foreword This document (EN ISO 15701:

11、2015) has been prepared by IULTCS “International Union of Leather Technologists and Chemists Societies“ in collaboration with Technical Committee CEN/TC 289 “Leather” the secretariat of which is held by UNI. This European Standard shall be given the status of a national standard, either by publicati

12、on of an identical text or by endorsement, at the latest by October 2015, and conflicting national standards shall be withdrawn at the latest by October 2015. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN and/or CENELEC shal

13、l not be held responsible for identifying any or all such patent rights. This document supersedes EN 15701:1999. According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgari

14、a, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turke

15、y and the United Kingdom. Endorsement notice The text of ISO 15701:2015 has been approved by CEN as EN ISO 15701:2015 without any modification. BS EN ISO 15701:2015ISO 15701:2015(E)IULTCS/IUF 442:2015(E) ISO 2015 All rights reserved iiiContents PageForeword iv1 Scope . 12 Normative references 13 Pri

16、nciple 14 Apparatus and materials 15 Test specimens 26 Procedure. 37 Precision . 48 Test report . 4Annex A (informative) Commercial sources for apparatus and materials 5BS EN ISO 15701:2015ISO 15701:2015(E)ForewordISO (the International Organization for Standardization) is a worldwide federation of

17、national standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Each member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. Inte

18、rnational organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.The procedures used to develop this document and those int

19、ended for its further maintenance are described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the different types of ISO documents should be noted. This document was drafted in accordance with the editorial rules of the ISO/IEC Directives, Part 2 (see ww

20、w.iso.org/directives).Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of any patent rights identified during the development of the document

21、will be in the Introduction and/or on the ISO list of patent declarations received (see www.iso.org/patents).Any trade name used in this document is information given for the convenience of users and does not constitute an endorsement.For an explanation on the meaning of ISO specific terms and expre

22、ssions related to conformity assessment, as well as information about ISOs adherence to the WTO principles in the Technical Barriers to Trade (TBT) see the following URL: Foreword - Supplementary informationISO 15701 was prepared by the Fastness Tests Commission of the International Union of Leather

23、 Technologists and Chemists Societies (IUF Commission, IULTCS) in collaboration with the European Committee for Standardization (CEN) Technical Committee CEN/TC 289, Leather, the secretariat of which is held by UNI, in accordance with the Agreement on technical cooperation between ISO and CEN (Vienn

24、a Agreement).It is based on IUF 442 published in J. Sec. Leather Tech. Chem., 56, pp. 395-400 (1972) with a minor amendment in 65, p. 128 (1981), and declared an official method of the IULTCS in 1973 and reconfirmed in 1989.IULTCS, originally formed in 1897, is a world-wide organization of professio

25、nal leather societies to further the advancement of leather science and technology. IULTCS has three Commissions, which are responsible for establishing international methods for the sampling and testing of leather. ISO recognizes IULTCS as an international standardizing body for the preparation of

26、test methods for leather.This second edition cancels and replaces the first edition (ISO 15701:1998), which has been technically revised with the following changes: use of polymeric test materials other than poly(vinyl chloride) is allowed; change in title to reflect the use of polymeric test materi

27、als; technical update of the procedures; revision of the loading in 4.1 and 6.1; inclusion of precision information as Clause 7.Annex A is for information only.IULTCS/IUF 442:2015(E)iv ISO 2015 All rights reservedBS EN ISO 15701:2015INTERNATIONAL STANDARD ISO 15701:2015(E)Leather Tests for colour fa

28、stness Colour fastness to migration into polymeric material1 ScopeThis International Standard specifies a method for assessing the propensity of dyes and pigments to migrate from leather to a synthetic substrate by determining the transfer of colour from the leather to white plasticized poly(vinyl c

29、hloride) in contact with it.This method is suitable for leather of all kinds at any stage of processing.NOTE Tests to determine the transfer of colour from the leather using other polymeric materials (e.g. thermoplastic polyurethane) are also possible.2 Normative referencesThe following documents, i

30、n whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.ISO 105-A01, Textiles Tests for co

31、lour fastness Part A01: General principles of testingISO 105-A03, Textiles Tests for colour fastness Part A03: Grey scale for assessing stainingISO 105-A04, Textiles Tests for colour fastness Part A04: Method for the instrumental assessment of the degree of staining of adjacent fabricsISO 2418, Leat

32、her Chemical, physical and mechanical and fastness tests Sampling location3 PrincipleThe side under test of the leather specimen is placed on a polymeric sheet, for example a white-pigmented sheet of plasticized poly(vinyl chloride), and the resultant composite specimen is exposed to heat under pres

33、sure in a suitable apparatus. The transfer of colour from the leather to the white sheet is assessed with the standard grey scale for assessing staining and, if applicable, any change in hue of the staining is also assessed.The use of standard sheets of plasticized poly(vinyl chloride) makes it poss

34、ible to determine the tendency of colour to migrate from the leather to synthetic materials used in conjunction with the leather.If the leather has a finish, the test may be carried out with the finish intact or broken.The general colour fastness testing principles used are in accordance with those

35、described in ISO 105-A01, taking into account the differences between textile substrates and leather.4 Apparatus and materialsNormal laboratory apparatus and:4.1 Test apparatus, in which the composite specimen can be subjected, between glass plates, to a uniform pressure of (81,7 4,0) kPa using an a

36、pproximately 5 kg load weight. The pressure tolerance includes a maximal supplementary mass due to the glass plates of 250 g. The construction of the test apparatus shall ensure that the pressure is constant during the whole test. ISO 2015 All rights reserved 1BS EN ISO 15701:2015ISO 15701:2015(E)NO

37、TE 1 The 81,7 kPa pressure from a 5 kg load weight is equivalent to 833 g/cm2on the (30 20) mm leather specimen.NOTE 2 A test apparatus that allows removal of the load weight after fixing the composite specimens is not suitable for this test.NOTE 3 Examples of suitable apparatus available commercial

38、ly are given in Annex A.4.2 Oven, maintained at (50 2) C.4.3 Sheet of suitable polymeric material, preferably pigmented white.If no additional information is provided, use plasticized poly(vinyl chloride), pigmented white, (0,5 0,1) mm thick, measuring approximately 50 mm 30 mm.NOTE Examples of suit

39、able commercial sources for the prepared sheets of polyvinyl chloride and the specifications are given in Annex A.4.4 If the finish is to be broken, fine-grained abrasive paper, grade P180, as defined in the P-series grain size standard published by the Federation of European Producers of Abrasive P

40、roducts (FEPA).NOTE FEPA Standard (43-1-2006), obtainable from FEPA (Federation of European Producers of Abrasives), 20 Avenue Reille, 75014 Paris, France. www.fepa-abrasives.org4.5 Press knife, the inner wall of which is a rectangle (30 1) mm (20 1) mm.4.6 Grey scale for assessing staining, complyi

41、ng with ISO 105-A03 or an instrumental system for assessing staining, complying with ISO 105-A04.5 Test specimens5.1 If the piece of leather available for testing is a whole hide or skin, then first take a sample in accordance with ISO 2418.5.2 If the leather has no finish, or if it has a finish but

42、 is to be tested with the finish intact, or the reverse side of the leather is to be tested, with the press knife (4.5) simply cut out a representative test specimen measuring 30 mm 20 mm.In case of a differing load weight, it is possible to realize the pressure stated in 4.1 either by adding a supp

43、lementary load (only possible for lower load weights) or by adjusting the dimensions of the specimen. The second possibility is restricted by the dimensions of the plasticized poly(vinyl chloride) sheet that has to exceed the dimensions of the test specimen.IULTCS/IUF 442:2015(E)2 ISO 2015 All right

44、s reservedBS EN ISO 15701:2015ISO 15701:2015(E)A modality to recalculate the specimen area is given below.AmAm1100=()whereA0is the area of the specimen stated by this International Standard;A1is the recalculated area of the specimen;m0is the load weight stated by this International Standard;m1is the

45、 load weight existing in the laboratory.EXAMPLE If the available load weight m1is 4,5 kg, additional loading pieces of 0,5 kg are permitted to be added or a specimen with a different area is allowed to be used. The new area would be in this case of 5,4 cm2(27 mm 20 mm) instead of 6 cm2.5.3 If the le

46、ather has a finish and is to be tested with the finish broken, prepare the test specimen as follows:Cut out a piece of leather measuring approximately 80 mm 60 mm and lay it out, finish side down, on a sheet of abrasive paper (4.4), measuring about 150 mm 200 mm, held flat on a work surface. Load th

47、e upper side of the piece of leather uniformly with a 1 kg weight. Move the piece of leather 100 mm to-and-fro on the abrasive paper, carrying out 10 to-and-fro cycles.NOTE With practice, it is possible to achieve the same roughening effect holding the abrasive paper in the hand.Brush the roughened

48、area thoroughly to remove all dust. From the roughened area of the leather, use the press knife (4.5) to cut out a test specimen measuring 30 mm 20 mm.The fact that the finish has been broken shall be mentioned in the test report.5.4 Make up a composite specimen by placing the test specimen, with th

49、e side to be tested face down, in the centre of an approximately (50 30) mm piece of the plasticized poly(vinyl chloride) sheet (4.3).6 Procedure6.1 The load weight shall be preheated in the oven (4.2) at (50 2) C for at least 2 h. Place the composite specimen between two glass plates, place the plates in the apparatus (4.1) and load with an approximately 5 kg load weight corresponding to a pressure of (81,7 4,0) kPa on the leather.It is possible to test several composite specimens simultaneousl