FORD FLTM BO 117-2-2001 IMPACT TEST FOR PLASTICS (Replaces FLTM BO 017-02).pdf

1、 FORD LABORATORY TEST METHOD BO 117-02 Date Action Revisions 2001 03 28 Revised Editorial no technical change A. Cockman 1996 10 16 Printed copies are uncontrolled Page 1 of 11 Copyright 2001, Ford Global Technologies, Inc. IMPACT TEST FOR PLASTICS Application This method is used to determine the im

2、pact resistance of plastics. Apparatus Required Impact Test Stand The test fixture used for this test consists of a heavy metal base to which is mounted a sample support ring of 2 inches (50.8 mm) inside diameter. The inside perimeter of the sample support is cut to 1/4 inch (6.35 mm) radius. Mounte

3、d and centered over the support ring is a carrier which holds the impact dart. The dart is free to move in its carrier and rests on the sample under static conditions. The dart has 1/2 inch (12.7 mm) diameter with one end rounded to 1/4 inch (6.35 mm) radius; the other end has a 1 inch (25.4 mm) dia

4、meter flat impact head. The dart is long enough to protrude 3/4 inch (19.1 mm) below the sample plane into the support ring. Impact weights are 1 inch (25.4 mm) diameter metal rods and are dropped through a guide tube which is mounted and centered over the impact dart. The tube has 1 1/32 inch (26.2

5、 mm) diameter and is 50 inches (1270 mm) long. Its entire length is slotted and calibrated into 1 inch (25.4 mm) increments along the slot. The weights are lifted by a pin which protrudes through the slot in the guide tube. A wide selection of weights from pound (113 g) to 10 pounds (4.54 kg) should

6、 be available so that any force range can be maintained with a weight velocity at impact of 7 to 15 ft/s (2.1 to 4.6 m/s). Guide tube calibrations are clearly marked so that when the weight is raised to a specific height and dropped, it strikes the impact dart driving it against the sample with a sp

7、ecific impact force in inch pounds. Freezer In determining cold impact strength, a chest freezer or other cooling apparatus capable of maintaining the desired temperature within +/- 2 C should be used, such as Revco Cold Box - Model ULD 1234. Source: Revco Corporation Industrial Products Division De

8、erfield, Michigan 48238 or equivalent. Samples Impact test samples should be injection molded 4 x 4 inch (102 x 102 mm) plaques with smooth surfaces and be all of the same thickness, either 0.100 inch (2.54 mm) or 0.125 inch (3.18 mm). FORD LABORATORY TEST METHOD BO 117-02 Page 2 of 11 Copyright 200

9、1, Ford Global Technologies, Inc. Conditioning and Test Conditions All test values indicated herein are based on material conditioned in a controlled atmosphere of 23 +/- 2 C and 50 +/- 5 % relative humidity for not less than 24 h prior to testing and tested under the same conditions unless otherwis

10、e specified. Test Procedure 1. Place a test sample on the support ring letting the dart rest freely on the surface of the sample. 2. Choose a weight which will deliver an impact force when dropped from 25 inches that is in the range of the expected impact resistance of the material to be tested. 3.

11、After the appropriate weight is selected, the test force increment should be set at 5 % or less of the approximate impact resistance of the material. (For very low ranges, the force increment may be as high as 10 %.) 4. Impact a few plaques to verify that the weight chosen yields both passes and fai

12、lures in the desired height range. (If more than six or seven consecutive passes are encountered, increase the force impact and start test over. Conversely, if more than six or seven consecutive failures are encountered, decrease the force and start test over). 5. After this is verified, perform the

13、 test by the following method: (a) If the sample presently being impacted fails, the next sample will be impacted at a level one increment lower. (b) If the sample presently being impacted passes, the next sample will be impacted at a level one increment higher. Failure is defined as any evidence of

14、 cracking. A minimum of 20 samples should be tested. The weight should not be allowed to bounce and strike the sample a second time. The sample should be held firmly and flat on the support ring during the entire procedure. If impact resistance is being determined at a sub-ambient temperature, the s

15、ample should be held at the sub zero temperature for a minimum of 8 h and impacted within 5 s after removal from the freezer. 6. Record the data on a data sheet (example data sheet included) with force increments marked under column “F“ and failures and/or passes in the appropriate sample number box

16、 in the center of the page. Calculations: A computer program titled “STAIR“ is available for analysis of impact data. It is stored in corporate time sharing library, and can be accessed by any user from any time sharing console using the procedure described in Exhibit III of General Parts Division R

17、eliability Memo No. IV-12. The following procedure is given for manual analysis: FORD LABORATORY TEST METHOD BO 117-02 Page 3 of 11 Copyright 2001, Ford Global Technologies, Inc. 1. Count the number of passes and failures. Determine which occurred the least number of times. If the force range of the

18、 least frequent event is more than 20 % of the highest force value, the confidence of the test is decreased. (For very low ranges, a 30 % variation is allowable.) 2. Starting with “O“ for the lowest force increment at which the least frequent event (pass or fail) occurs, number the force increments

19、with ascending integers so that the highest integer corresponds to the highest force increment at which the least frequent event occurred. These numbers should be entered in Column “I“ of the work sheet. 3. Count the number of the least frequent events which occurred at each force level (horizontall

20、y). Enter these numbers in Column “N“. For each horizontal line, multiply I x N and I2 x N and enter results in the appropriate columns. 4. Add Columns N, (I x N) and (I2 x N) so that: A = N B = (I x N) C = (I2 x N) 5. Compute the force impact sample mean by the following equation: (Space is provide

21、d on the work sheet for calculations in Steps 5, 6, 7, and 8) x = Fo + d (B/A +/- 0.5) Where: x = Force Impact Sample Mean Fo = Lowest Force Value of Least Frequent Event d = Force Increment B/A = Mean of Force Impact Integer Value In the expression (B/A +/- 0.5) use + (plus) if the least frequent e

22、vent is pass; use - (minus) if the least frequent event is fail. 6. Compute Upper Limit by the following equation: U = (AC B2) A2 Where: U = Upper Limit A = N B = (I x N) C = (I2 x N) If “U“ is less than or equal to 0.3, the standard deviation cannot be estimated and the test should be repeated usin

23、g a smaller force increment. If “U“ is larger than 0.3, then continue to Step 7. FORD LABORATORY TEST METHOD BO 117-02 Page 4 of 11 Copyright 2001, Ford Global Technologies, Inc. 7. Compute the standard deviation by the following equation: S = 1.62 d x (AC B 2) 0.03) A2 Where: S = Standard Deviation

24、 1.62 = Constant (AC-B2)/A2 = Upper Limit 0.03 = Constant 8. The impact value, R, of the material is computed as follows: R = x - .84S Where: R = Impact Resistance of Material x = Sample Mean S = Standard Deviation The impact resistance of the material is defined to be the level at which 20 % of the

25、 samples would be expected to fail and 80 % pass. The 20 % failure level is chosen so that the material which has a high scatter of data will be penalized more than a very consistent material. 9. Report should contain: (a) Material description and identification (b) Sample number tested (c) Sample s

26、ize and thickness (d) Mean impact level (x) (e) Standard deviation (S) (f) Expected 20 % failure level (R) to the nearest inch pound. (g) Test conditions: temperature, painted or unpainted, side of plaque impacted, etc. Statistical methods are available for more detailed analysis. If more analysis i

27、s required, refer to General Parts Division Reliability Memo No. IV-12. Chemicals, materials, parts, and equipment referenced in this document must be used and handled properly. Each party is responsible for determining proper use and handling in its facilities. FORD LABORATORY TEST METHOD BO 117-02

28、 Page 5 of 11 Copyright 2001, Ford Global Technologies, Inc. IMPACT TEST FOR PLASTICS Sketch 1 FORD LABORATORY TEST METHOD BO 117-02 Page 6 of 11 Copyright 2001, Ford Global Technologies, Inc. IMPACT TEST FOR PLASTICS Sketch 2 FORD LABORATORY TEST METHOD BO 117-02 Page 7 of 11 Copyright 2001, Ford G

29、lobal Technologies, Inc. IMPACT TEST FOR PLASTICS Sketch 3 FORD LABORATORY TEST METHOD BO 117-02 Page 8 of 11 Copyright 2001, Ford Global Technologies, Inc. IMPACT TEST FOR PLASTICS Sketch 4 FORD LABORATORY TEST METHOD BO 117-02 Page 9 of 11 Copyright 2001, Ford Global Technologies, Inc. IMPACT TEST FOR PLASTICS Sketch 5 FORD LABORATORY TEST METHOD BO 117-02 Page 10 of 11 Copyright 2001, Ford Global Technologies, Inc. FORD LABORATORY TEST METHOD BO 117-02 Page 11 of 11 Copyright 2001, Ford Global Technologies, Inc.