1、 ENGINEERING MATERIAL SPECIFICATION Date Action Revisions Rev. 04 2017 06 27 Editorial Corrected footer A. Collins, NA 2016 07 05 Revised See Summary of revisions W. Janitschke, FoE 2002 07 31 Activated W. Janitschke, FoE Controlled document at www.MATS Copyright 2017, Ford Global Technologies, LLC
2、Page 1 of 8 PERFORMANCE SPRAYABLE COATING, ACOUSTIC, WSS-M99P30-A INTERIOR AND EXTERIOR, BODY PANELS 1. SCOPE This specification defines the performance requirements for solvent free material with good acoustical efficiency, which is applied to body panels either in body-in-white or in the paint sho
3、p. 2. APPLICATION This specification was originally released for materials to be sprayed on or applied with wide slit nozzle in visible or non-visible areas of roof, floor, side panel, rocker panel, doors, liftgate etc. where body panel damping, gravel noise reduction and/or panel stiffening is requ
4、ired. The material is applied onto oily surfaces or dry electrocoat. Type 1: The coating is applied to an oily metal surface prior to cleaning, phosphating and paint process. The material is hot applied and will set after cooling to room temperature without further bake process. Type 2: The coating
5、is applied to an oily metal surface prior to cleaning, phosphating and application of electrocoat. The material will cure during the electrocoat bake process. Type 3: The coating is applied to an electrocoated metal panel prior to application of primer surfacer and/or color coat. The material will c
6、ure through the primer surfacer and/or color coat bake process. 3. REQUIREMENTS 3.1 APPROVED SOURCES This specification requires the use of approved sources. Only the sources identified on the Ford Approved Source List (ASL) can be used when this specification is listed on the drawing, CAD file, or
7、other documents. The list of approved sources is located within Ford at or available externally through a Ford Materials Engineer. Part producers must use a process control plan which has been approved by STA and/or the relevant Materials Activity. 3.2 FILM THICKNESS, Dry As specified on Engineerin
8、g Drawing 3.3 ABRASION RESISTANCE (ASTM D968, only applicable for materials used as underbody coating, see Engineering Drawing) There shall be no exposed metal area showing after 370 L gravel impact. No loss of adhesion on and around the area of stone impact. ENGINEERING MATERIAL SPECIFICATION WSS-M
9、99P30-A Copyright 2017, Ford Global Technologies, LLC Page 2 of 8 Test Method: Prepare the test panels as follows: 3.3.1 Test panels of 300 x 100 mm prepared according to FLTM BI 120-01 shall be coated by material under test centrally 10 mm away from the edges to produce the min required dry thickne
10、ss which is required to fulfill acoustical requirements. Panels with Type 1 and Type 2 materials shall be baked separately for the min and max curing cycles acc. to FLTM BV 150-05, for the applicable region, and Type 3 materials acc. to FLTM BV 150-05 for the applicable region. 3.3.2 After condition
11、ing for 24 h at 23 +/- 2 C determine the abrasion resistance according to ASTM D 968, except I.D. of tube 25 mm and at a gravel through put rate of 30 - 40 L/h. For each specimen 5 L of fresh gravel shall be used. GRAVEL: Type “GABBRO“ grain size 5 - 8 mm or equivalent SUPPLY SOURCE: ODENWALDER HART
12、STEIN INDUSTRIE GMBH Erbacher Strasse 62 D-6101 Rossdorf or equivalent 3.4 CORROSION RESISTANCE, LABORATORY CYCLIC CORROSION TEST CETP 00.00-L-467 The material shall protect the test panel from corrosion. Under the material and at the border line of material edges it shall be seen no corrosion, no f
13、laking or any evidence of loss of adhesion of the material. Test Method: Prepare test specimens in accordance to the test method described in para 3.3.1. Panels shall be cured for the min and max cycle times as stated in FLTM BV 150-05, for the applicable region. After conditioning for 24 h at 23 +/
14、- 2 C, expose samples to CETP 00.00-L-467 as follows: Samples applied to BIW surfaces: 6 weeks Samples applied to e-coated surfaces: 12 weeks Examine for corrosion resistance. Disregard the area 10 mm from the edges of test panel. 3.5 CORROSION RESISTANCE, PROVING GROUND (CETP 00.00-R-343) New mater
15、ial technologies require total vehicle corrosion testing prior to approval and their introduction. Test details including film thickness, method of application, number of test cycles, etc. for the individual cars are defined by Materials Engineering, PV steel see Table 1 according to DIN EN 10083, h
16、ardness code CK75, panel size 240 x (+/-0,3) 10(+/-0,3) x 1 (+/-0.02) mm, material size 216 x 10 mm) Preparation and Curing of Specimens: Test panels shall be coated by material under test to produce the necessary dry thickness which is required to fulfill acoustical requirements. For panels with Ty
17、pe 1 materials no baking is required. Panels with Type 2 materials shall be baked for 10 min at 190 C (reference curing). Panels with Type 3 materials shall be baked for 10 min at 175 C (reference curing). 3.13.1 Original (24 h after application) 3.13.2 After Environmental Cycling Test Method: Sampl
18、es must be exposed 16 times to the following cycle in the sequence indicated below: 16 h at 38 +/- 2 C and 98 +/- 2% RH Review latest WCR 4 h at - 40 +/- 1 C Environmental 4 h at 80 +/- 2 C Requirements After each four cycles specimens to be stored at 23 +/- 2 C for 72 h before continuing or testing
19、. After ageing no deviation from original. 3.14 ACOUSTIC EFFICIENCY (GRAVEL NOISE REDUCTION) For min requirement (FLTM BV160-03, material under test is facing see Fig.1 to the noise source chamber in the equipment) 3.15 BODY PANEL REINFORCEMENT For min requirement (Only if required on Engineering Dr
20、awing see Table 1 DIN EN63, except body steel panel 140 (+/- 0.1) x 80 (+/- 0.1) x 0.75 mm (tolerance see Engs. Drawing);calculation: max. bending power for panel laminated with material under test minus max. power for virgin panel at 3 mm bending) Preparation and Curing of Specimens: ENGINEERING MA
21、TERIAL SPECIFICATION WSS-M99P30-A Copyright 2017, Ford Global Technologies, LLC Page 5 of 8 Test panels shall be coated by material under test to produce the necessary dry thickness which is required to fulfill acoustical and stiffening requirements (Tables 1 and 2 of spec.). Panels with Type 2 mate
22、rials shall be baked separately for the min and max curing cycles acc. to FLTM BV 150-05, for the applicable region and Type 3 acc. to FLTM BV 150-05, for the applicable region. 3.15.1 Original (24 h after application) 3.15.2 After Aging (14 d at 90 +/-2 C, 24 h 23 +/-2 C) 3.16 ODOR Rating 3 max (FL
23、TM BO 131-03, cured material per min cycle as in FLTM BV 150-05, for the individual region, for interior application only) 3.17 FOGGING 2000 ppm max (for European use and for interior applied materials only, VDA 278 (Thermodesorption), cured material per min cycle time as in FLTM BV 150-05, Table 2,
24、 Spray Primer) 3.18 VOLATILE ORGANIC CONTENT 1500 ppm max (for European use and for interior applied materials only, VDA 278 (Thermodesorption), cured material per min cycle time as in FLTM BV 150-05, Table 2, Spray Primer) 3.19 ALCANE RESTRICTION, (for European use and for interior applied material
25、s only) VDA 278 (Thermodesorption) The supplied material shall not contain Alcanes (n-Aliphates as C10H22 thru C16H34) based on VOC test method and requirements (para 3.18). 4. GENERAL INFORMATION The information given below is provided for clarification and assistance in meeting the requirements of
26、 this specification. Contact for questions concerning Engineering Material Specifications. 4.1 APPROVAL OF MATERIALS Suppliers desiring approval of their materials shall first obtain an expression of interest from Purchasing, Design or Product Development, and Materials Engineering. The supplier sh
27、all submit a completed copy of their laboratory test reports, signed by a qualified and authorized representative of the test facility, demonstrating full compliance with all the requirements of the Material Specification. Tested material samples must be available for review upon request and kept fo
28、r a minimum of one year. Upon request, the supplier will review the associated quality control documents (Process Failure Mode and Effects Analysis, Control Plans, Certification testing) with Ford. 4.2 SUPPLIERS ONGOING RESPONSIBILITY All materials must be equivalent in all characteristics to the ma
29、terial upon which approval was originally granted. Prior to making any changes to the material originally approved, whether or not such changes affect the materials ability to meet the specification requirements, the supplier shall notify the affected Supplier Technical Assistance (STA), Purchasing,
30、 and Materials Engineering ENGINEERING MATERIAL SPECIFICATION WSS-M99P30-A Copyright 2017, Ford Global Technologies, LLC Page 6 of 8 activities of the proposed changes (with reasons) by submission of a completed Suppliers Request for Engineering Approval, SREA. For parts and components using Ford En
31、gineering Material Specifications, all samples tested to the specifications for Design Verification (DV), Production Verification (PV) and Production Part Approval Process (PPAP) sign off must be kept until Job 1. 4.3 RESTRICTED SUBSTANCE MANAGEMENT STANDARD Substance restrictions imposed by regulat
32、ions or Company direction applies to the materials addressed by this document. The restrictions are identified in the Restricted Substance Management Standard WSS-M99P9999-A1 which is updated yearly. It is the suppliers responsibility to comply with this standard on a continuing basis through IMDS a
33、nd or GMAP reporting. 5. SUMMARY OF REVISIONS 2016 07 05 Updated Corrosion Resistance Requirements (3.4). Removed WSS-M99P1111-A and moved those requirements directly into this spec. 2011 06 01 Revised Odor Requirements 2004 03 25 Revised 3.3, 3.13, 3.16, 3.17, added 3.18, 3.19 ENGINEERING MATERIAL
34、SPECIFICATION WSS-M99P30-A Copyright 2017, Ford Global Technologies, LLC Page 7 of 8 LOST FACTORS (OBERST) Table 1 Test Temperature 1.5 2.0 2.5 3.0 3.5 4.0 kg/m - 20 C 0.02 0.02 0.02 0.02 0.03 0.04 0 C 0.05 0.06 0.06 0.06 0.07 0.09 20 C 0.06 0.08 0.10 0.12 0.14 0.16 40 C 0.03 0.03 0.03 0.03 0.06 0.0
35、9 60 C 0.02 0.02 0.02 0.02 0.02 0.02 ENGINEERING MATERIAL SPECIFICATION WSS-M99P30-A Copyright 2017, Ford Global Technologies, LLC Page 8 of 8 Fig. 1 Min. Requirements of Acoustical Performance Min requirements for cured material related to 1.5kg/m of mass of deadener to mass of metal, original and after aging
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