GOST 31765-2012 Wines and wine materials Determination of synthetic dyes by capillary electrophoresis method《葡萄酒和葡萄酒原料 通过毛细管电泳法测定合成染料》.pdf

1、 , ()INTERSTATE COUNCIL FOR STANDARDIZATION, METROLOGY AND CERTIFICATION(ISC)317652012, - 1.092 . 1.22009 . -, . , , 1 - - ( )2 3 , ( 15 2012 . 42) : ( 3166) 00497 ( 3166) 00497 BYKZKGMDRUTJ -4 29 2012 . 1686- 317652012 - 1 2013 5 5315420086 ( ) - . , - . - , 2013 -, II 3176520121 .12 13 .24 , , 25

2、.26 .37 .37.1 37.2 38 39 39.1 .39.2 49.3 49.4 510 .511 .5 () .7 () 8 () .10III 317652012 . - , , , - . - .IV 317652012 Wines and wine materials.Determination of synthetic dyes by capillary electrophoresis method1 0,002 0,200/3.2 :5725-22002 ()-. 2. - 12.1.00776 . . 12.1.01979 . . - 177074 ( 104283,

3、478880) . -, , , . 311877 . . 365269 . . 395676 . 432877 . . 670972 . 1065273 . -N, N, N c162 ,Nc162- 2- ( ). 1491983 , . - 241042001 . 2533682 . , 2849890 . . 2922791 ( 835-181) . . 1. 317302012 . 1 317652012 20130701 - , 1 , , . (), (-) . , , , , .3 12.1.019. - 12.1.007. , - , .4 , , , 50 , 75 , ,

4、 - 254 200 300 - () ., , - 400 700 . 24104 - c177 0,0001 .40200- c177 1. 0 100 1 28498. 2- 1, 2, 5, 10 3 29227. 2-250-2, 2-100-2, 2-50-2, 2-25-2 1770. 25336. -14/8 25336. . 25336. 14919. 6000 /. ( ) 1,5 3. 6709. 3118. 4328. 3652. (N,N,N,N-tetramethylethylenediamine) - 99,5 %. 10652. 99 %. 3956. . ,.

5、5 31730.2 3176520126 -, . , 254 215 .7 7.1 0,002 0,200 /3.7.2 5725-2 - 1. 1 r,%,P = 0,9511 R,%,P=0,9515 c177 5 P=0,95, %188 (23 c177 5) , 87 107 , 80 %, (50 c177 0,4) , 220 .9 9.1 9.1.1 4 % 5060 3 4 . - 100 3. 2 .9.1.2 3,5 % 100 3 8,3 3 1,18 /3, . .9.1.3 0,05 /3 25 3 (0,240 c177 0,001) . 15 3 . ( )

6、25 3, , . .9.1.4 0,05 /3 25 3 (0,145 c177 0,001) . 10 3 ( 4 ) . ( - ) 25 3, , . .3 3176520129.1.5 0,05 /3 25 3 (0,465 c177 0,001) . 15 3 . ( ) 25 3, , - . 1 .9.1.6 9.1.3, 9.1.4, - 9.1.5 4:3:1:1. - 2 . - 0,8 3 4 6000 /.9.2 9.2.1 () - :- 254 215 ;- 25 ;- 30 5 0 ;- 12 ;- 25 . , 3,5 % (. 9.1.2) 3 , 3 , 4 %- (. 9.1.1) 3 , 3 (. 9.1.6) 3 . - . 2 . , , .9.2.2 - (30 , 5) - 12 . . . - . .9.3 9.3